Liquid crystalline compound and use thereof

ABSTRACT

A process for producing a liquid crystalline compound represented by the following general formula (A): ##STR1##

BACKGROUND OF THE INVENTION

The present invention relates to a liquid crystalline compound and use thereof. More particularly, the present invention relates to a process for producing a novel liquid crystalline compound, which exhibits liquid crystallinity and, in addition, photoconductivity and fluorescence, and use of the liquid crystalline compound in a liquid crystalline charge transport material.

Liquid crystalline compounds having various structures are known in the art and have been extensively used as a liquid crystal display material.

Materials, wherein a charge transport molecule which serves as a charge transport site are dissolved or dispersed in a matrix material, such as a polycarbonate resin, or materials, wherein a charge transport molecule structure pends as a pendant on a polymer backbone, such as polyvinyl carbazole, are known in the art. These materials have been extensively used as materials for photoconductors in copying machines, printers and the like.

For the above conventional charge transport materials, in the case of dispersive charge transport materials, that the charge transport molecule has high solubility in the polymer as a matrix is preferred from the viewpoint of improving the charge transport capability. In fact, however, bringing the charge transport molecule to a high concentration in the matrix leads to crystallization of the charge transport molecule in the matrix, and, for this reason, the upper limit of the concentration of the charge transport molecule is generally 20 to 50% by weight although it varies depending upon the kind of the charge transport molecule. This means that the matrix not having charge transport capability occupies not less than 50% by weight of the whole material. This in turn raises a new problem that the charge transport capability and response speed of a film formed from the material are limited by the excess matrix present in the material.

On the other hand, in the case of the pendant type charge transport polymer, the proportion of the pendant having charge transport capability can be increased. This polymer, however, involves many practical problems associated with mechanical strength, environmental stability and durability of the formed film, film-forming properties and the like. In this type of charge transport material, the charge transport pendants are locally located in close proximity, and the local proximity portion serves as a stable site in hopping of charges and functions as a kind of trap, unfavorably resulting in lowered charge mobility.

For all the above charge transport materials, electrical properties of such amorphous materials raise a problem that, unlike crystalline materials, the hopping site fluctuates in terms of space, as well as in terms of energy. For this reason, the charge transport depends greatly upon the concentration of the charge transport site, and the mobility is generally about 10⁻⁶ to 10⁻⁵ cm² /vs which is much smaller than that of the molecular crystal, 0.1 to 1 cm² /vs. Further, the amorphous materials have an additional problem that the charge transport properties depend greatly upon temperature and field strength. This is greatly different from the crystalline charge transport materials.

A polycrystalline charge transport material is a promissing material in applications where a charge transport layer having a large area is necessary, because it can form an even charge transport film having a large area can be evenly formed. The polycrystalline material, however, is inherently an uneven material from the microscopic viewpoint and involves a problem that a defect formed in the interface of particles should be inhibited.

Accordingly, the present invention aims to solve the above problems of the prior art and to provide a novel charge transport material which simultaneously realizes advantages of the amorphous materials, that is, structural flexibility and evenness in a large area, and advantages of the crystalline materials having molecular orientation and is excellent in high-quality charge transport capability, thin film-forming properties, various types of durability and the like.

DISCLOSURE OF INVENTION

An object of the present invention is to provide a novel liquid crystalline compound which exhibits liquid crystallinity and, in addition, photoconductivity and fluorescence and a process for producing the same.

Another object of the present invention is to provide a novel charge transport material which simultaneously realizes advantages of the amorphous materials, that is, structural flexibility and evenness in a large area, and advantages of the crystalline materials having molecular orientation and is excellent in high-quality charge transport capability, thin film-forming properties, various types of durability and the like.

According to one aspect of the present invention, there is provided a process for producing a liquid crystalline compound represented by the general formula (A) described below, comprising the steps of: reacting a compound represented by the general formula (1), described below, with a compound represented by the general formula (2) described below, brominating the reaction product to give a compound represented by the general formula (3) described below; and substituting the bromine atom with an R₂ group.

According to another aspect of the present invention, there is provided a process for producing a liquid crystalline compound represented by the general formula (B) described below, comprising the step of: reacting a compound represented by the general formula (4), described below, with a compound represented by the general formula (5) described below.

According to a further aspect of the present invention, there is provided a process for producing a liquid crystalline compound represented by the general formula (C) described below, comprising the step of: reacting two moles of a compound represented by the general formula (6), described below, with one mole of a compound represented by the general formula (7) described below.

According to a yet further aspect of the present invention, there is provided a process for producing a liquid crystalline compound represented by the general formula (D) described below, comprising the step of: reacting two moles of a compound represented by the general formula (8), described below, with one mole of a compound represented by the general formula (9) described below.

According to a yet further aspect of the present invention, there is provided a liquid crystalline charge transport material which exhibits smectic liquid crystallinity and has a reduction potential relative to a standard reference electrode (SCE) in the range of from -0.3 to -0.6 (Vvs. SEC).

According to a yet further aspect of the present invention, there is provided a liquid crystalline charge transport material which exhibits smectic liquid crystallinity and has an oxidation potential relative to a standard reference electrode (SCE) in the range of from 0.2 to 1.3 (Vvs. SEC).

BRIEF DESCRIPTION OF THE DRAWINGS

FIGS. 1, 2, 3 and 4 are cross-sectional views of embodiments where the crystalline charge transport material according to the present invention has been applied to a charge transport layer in an image recording device;

FIG. 5 is a cross-sectional view of an embodiment where the liquid crystalline charge transport material has been applied to a space light modulating device; and

FIG. 6 is a cross-sectional view of an embodiment where the liquid crystalline charge transport material according to the present invention has been applied to a thin film transistor.

BEST MODE FOR CARRYING OUT THE INVENTION

Process for producing liquid crystalline compound

The first invention relates to a process for producing a liquid crystalline compound represented by the general formula (A), comprising the steps of: reacting a compound represented by the general formula (1) with a compound represented by the general formula (2); brominating the reaction product to give a compound represented by the general formula (3); and substituting the bromine atom of the compound (3) with an R₂ group: ##STR2## wherein R₁ and R₂ represent (a) a cyano group, (b) a nitro group, (c) a fluorine atom, or (d) a C₁ -C₂₂ straight-chain or branched, saturated or unsaturated, alkyl or alkoxy group attached to the aromatic ring through an oxygen atom, or a sulfur atom, provided that at least one of R₁ and R₂ represents said alkyl or alkoxy group.

The second invention relates to a process for producing a liquid crystalline compound represented by the general formula (B), comprising the step of: reacting a compound represented by the general formula (4) with a compound represented by the general formula (5): ##STR3## wherein R₁ and R₂ represent a C₁ -C₂₂ straight-chain or branched saturated or unsaturated alkyl or alkoxy group attached to the aromatic ring through a cyano group, a nitro group, a fluorine atom, an oxygen atom, or a sulfur atom, provided that at least one of R₁ and R₂ represents said alkyl or alkoxy group; and X and Y are respectively groups which are reacted with each other to form a --COO--, --OCO--, --N═N--, --CH═N--, --N═N--, --CH₂ S--, --CH═CH--, or acetylene group.

The third invention relates to a process for producing a liquid crystalline compound represented by the general formula (C), comprising the step of: reacting 2 moles of a compound represented by the general formula (6) with one mole of a compound represented by the general formula (7): ##STR4## wherein R₁ is a C₁ -C₂₂ straight-chain or branched saturated or unsaturated alkyl or alkoxy group attached to the aromatic ring through an oxygen or sulfur atom.

The fourth invention relates to a process for producing a liquid crystalline compound represented by the general formula (D), comprising the step of: reacting two moles of a compound represented by the general formula (8) with one mole of a compound represented by the general formula (9): ##STR5## wherein R₁ is a C₁ -C₂₂ straight-chain or branched saturated or unsaturated alkyl or alkoxy group attached to the aromatic ring through an oxygen or sulfur atom; and X and Y are respectively groups which are reacted with each other to form a --COO--, --OCO--, --N═N--, --CH═N--, --N═N--, --CH₂ S--, --CH═CH--, or acetylene group.

According to a specific one embodiment of the present invention, there is provided a process for producing a liquid crystalline compound represented by the following general formula (I), comprising the steps of: reacting a 4-alkoxybenzaldehyde with o-aminobenzenethiol to synthesize a 2-(4'-alkoxyphenyl)benzothiazole; brominating the 2-(4'-alkoxyphenyl)benzothiazole to synthesize a 2-(4'-alkoxyphenyl)-6-bromobenzothiazole; and reacting the resultant bromide with an alkanethiol: ##STR6## wherein R represents a C₄ -C₂₀ alkyl group; and R' represents a C₄ -C₂₀ alkyl group, provided that the total number of carbon atoms contained in R and R' is 10 or more.

A further preferred embodiment of the production process will be described.

According to the present invention, a 4-alkoxybenzaldehyde is reacted with 1 mole or more, preferably 1.1 to 1.5 moles or more, based on one mole of the 4-alkoxybenzaldehyde, of o-aminobenzenethiol in a solvent suitable for a dehydration reaction (oxidative cyclization), preferably dimethylsulfoxide, at a temperature of 100° C. or above, preferably 120° to 160° C., for about 30 min to 2 hr.

In this reaction, the aldehyde group, the amino group, and the thiol group are combined together to form a thiazole ring, thus giving a 2-(4'-alkoxyphenyl)benzothiazole as an intermediate. This reaction can be easily achieved, and the intermediate is produced in a high yield of not less than 90%. The intermediate may be purified before use in the subsequent step or alternatively used in the subsequent step without purification.

The 2-(4'-alkoxyphenyl)benzothiazole is then brominated. In the bromination, the 2-(4'-alkoxyphenyl)benzothiazole is dissolved in a suitable solvent, such as glacial acetic acid, and bromine in an equimolar or slightly excessive molar amount is dropwise added thereto. In this reaction, bromine is easily substituted in the 6-position of the benzothiazole ring to give a 2-(4'-alkoxyphenyl)-6-bromobenzothiazole, and the reaction under mild conditions with heating can give the bromide in a yield of not less than 60%. When this intermediate contains a dibromination product and/or a substance remaining unreacted as impurities, it is preferably purified by recrystallization before use in the subsequent step.

Finally, the above bromide is reacted with an alkanethiol to give a liquid crystalline compound according to the present invention. Since this reaction is an aromatic nucleophilic displacement reaction by taking advantage of a thiolate anion, it is preferably performed in an alkaline atmosphere. For example, a liquid crystalline compound represented by the general formula (I) is produced by suspending an oil dispersion of sodium hydride in an ether, dropwise adding a corresponding alkanethiol to the suspension to produce a sodium salt of the alkanethiol, and reacting the sodium salt with the above bromide in a suitable solvent at a temperature of about 30° to 100° C. for 30 min to 2 hr.

According to the process of the present invention, the number of carbon atoms of the alkyl group in the 4-alkoxybenzaldehyde and the alkanethiol is important, and the number of carbon atoms of the alkyl group is preferably not less than 4, preferably 4 to 20 from the viewpoint of developing excellent liquid crystallinity. For the alkanethiol, the number of carbon atoms of the alkyl group is 4 or more, preferably 4 to 20. These alkyl groups may be somewhat branched. However, in order to develop excellent liquid crystallinity, the alkyl group is more preferably linear with the total number of carbon atoms of R and R' being 10 or more, preferably 12 to 40.

Further, liquid crystalline compounds represented by the following general formula (II) also fall within the scope of the present invention: ##STR7## wherein R represents C₇ H₁₅ and R' represents C₆ H₁₃, C₈ H₁₇, C₁₀ H₂₁ or C₁₂ H₂₅.

The above liquid crystalline compounds according to the present invention can be produced in a high yield from a p-alkoxybenzaldehyde, for example, by the following reaction scheme: ##STR8## wherein R and R' are as defined above and DMI represents N,N'-dimethylimidazolidinone.

The present invention provides a novel liquid crystalline compound which exhibits liquid crystallinity and, in addition, photoconductivity and fluorescence. The novel liquid crystalline compound is useful as a material for a liquid crystal display, a photosensitive material for electrophotography and the like. In particular, the liquid crystalline compound of the present invention has strong fluorescence and, hence, when used as a material for a color liquid crystal display or used in combination with a dichroic dye, can effectively utilize an ultraviolet portion in a backlight source, offering a display image having excellent sharpness and brightness.

Liquid crystalline charge transport material

According to a further aspect of the present invention, there is provided a liquid crystalline charge transport material which exhibits smectic liquid crystallinity and has a reduction potential relative to a standard reference electrode (SCE) in the range of from -0.3 to -0.6 (Vvs. SEC). According to a further aspect of the present invention, there is provided a liquid crystalline charge transport material which exhibits smectic liquid crystallinity and has an oxidation potential relative to a standard reference electrode (SCE) in the range of from 0.2 to 1.3 (Vvs. SEC).

A liquid crystalline molecule, by virtue of its molecular structure, has self-orientation, and, in the case of charge transport utilizing this molecule as a hopping site, unlike the above molecule dispersive material, the spacial and energy scattering of the hopping site is inhibited, enabling a band-like transport property such as found in a molecular crystal to be realized. This enables a mobility of about 10⁻³ to 10⁻² cm² /vs, that is, a larger mobility than that in the conventional molecular dispersive material, to be realized, and, in addition, the charge transport properties do not depend upon electric field.

In order that the material serves as a hole transport material, the molecule should have a low ionization potential, and, hence, the oxidation potential should be in the range of from 0.2 to 1.3 (Vvs. SEC) relative to a standard reference electrode (SCE). Further, in order that the material serves as an electron transport material, the molecule should have high electron affinity, and, hence, the reduction potential should be in the range of from -0.3 to -0.6 (Vvs.SEC). The above requirements are the same as the well known requirements for a charge transport molecule used in the conventional molecule dispersive material.

Preferred liquid crystalline charge transport materials of the present invention will be listed in Tables 1 to 71. Among the charge transport materials listed in these tables, more preferred materials are those which satisfy the above requirements, have (aromatic ring of 6 π electron system) n (wherein n is an integer of 1 to 4) cores and exhibit smectic liquid crystallinity, those wherein the aromatic ring of 6 π a electron system is linked through a carbon-carbon double bond or a carbon-carbon triple bond, and those which has a core of a benzothiazole ring, a benzoxazole ring, a benzimidazole ring, a naphthalene ring, or other aromatic ring of 10 π electron system and exhibit smectic liquid crystallinity.

The liquid crystalline charge transport materials according to the present invention are useful for various applications such as photosensors, electroluminescence devices, photoconductors, space modulating devices, and thin film transistors.

The liquid crystalline charge transfer materials according to the present invention can realize high-speed mobility and inhibition of the creation of structural traps. Therefore, high-speed response photosensors may be mentioned as the first application thereof. Next, by virtue of excellent charge transport properties, the liquid crystalline charge transfer materials according to the present invention can be used as a charge transfer layer in electroluminescence devices. Further, since electric field orientation and photoconductivity can be simultaneously switched, they can be used in image display devices.

The application to image display devices will be described as a representative example. In an image display device, when a device comprising a transparent substrate, such as glass, a transparent electrode, such as ITO (indium-tin-oxide), a charge generating layer capable of generating carriers according to exposure, the liquid crystalline charge transport material of the present invention, and a counter electrode (such as a gold electrode) laminated in that order is subjected to imagewise exposure (input image) through the bottom of the device as shown in the schematic diagram, the liquid crystalline charge transport material is aligned according to the exposure, resulting in flow of carriers in the counter electrode (gold electrode). The input image can be reproduced by optical reading of the alignment of the liquid crystal. The larger the smectic properties of the liquid crystal, the longer the storage time of the alignment of the liquid crystal and the longer the storage time of the input information.

FIGS. 1 to 3 are explanatory diagrams of embodiments where the liquid crystalline charge transport material according to the present invention has been applied to a charge transport layer in an image recording device. FIG. 1 is a schematic view of a photosensor, an embodiment where the liquid crystalline charge transport material according to the present invention has been applied to a charge transport layer. Use of the photosensor will be described in more detail. As shown in FIG. 3, the device is subjected to pattern exposure from the direction of the above in the drawing while applying a voltage across the upper and lower electrodes 15. Carriers are generated in a pattern form in 14', and charges transported by a charge transport layer 14" are discharged in a space 19 and reach the surface of an information recording layer 11.

The information recording layer is, for example, a liquid crystal/polymer composite layer formed of a composite of a smectic liquid crystal and a polymer. The liquid crystal is aligned in a pattern form in an electric field of accumulated charges and accumulated, enabling optical recording to be performed.

In the embodiment shown in FIG. 4, exposure with a voltage being applied may be carried out in the same manner as described above in connection with the embodiment shown in FIG. 3. The generated charges (image) are accumulated on the top surface of a dielectric layer 20, and the liquid crystal is aligned in a pattern form in an electric field of charges accumulated in the same manner as described above in connection with the embodiment shown in FIG. 3 and accumulated, enabling optical reading to be performed.

Further, the liquid crystalline charge transport material according to the present invention can be used also in a pace optical light modulating device schematically shown in FIG. 5. Furthermore, the liquid crystalline charge transport materials of the present invention can also be used as an active layer of a thin film transistor. For example, as shown in FIG. 6, the liquid crystalline material may be disposed on a substrate having thereon source, drain, and gate electrodes.

Thus, the liquid crystalline charge transport materials according to the present invention are useful for various applications such as photosensors, electroluminescence devices, photoconductors, space modulating devices, and thin film transistors.

                                      TABLE 1                                      __________________________________________________________________________      ##STR9##                                                                      No L            R             Cr  LC                                           __________________________________________________________________________     7109                                                                              O.sub.2 N    COC.sub.10 H.sub.20Si.sub.4 O.sub.4 Me.sub.7 -cy                                             K?  A58 I                                        7122                                                                              NCCHCH       C.sub.4 H.sub.9                                                                              K61.1                                                                              A57.7 N113.8 I                               7123                                                                              NCCHCH       C.sub.5 H.sub.11                                                                             K61.8                                                                              A93.3 N122.2 I                               7124                                                                              NCCHCH       C.sub.6 H.sub.13                                                                             K79.7                                                                              A113 N120.6 I                                7125                                                                              NCCHCH       C.sub.7 H.sub.15                                                                             K70.2                                                                              A125 I                                       7126                                                                              NCCHCH       C.sub.8 H.sub.17                                                                             K59.3                                                                              A127.4 I                                     7127                                                                              NCCHCH       C.sub.9 H.sub.19                                                                             K55 A131 I                                       7130                                                                              C.sub.5 H.sub.13                                                                            C.sub.9 H.sub.19                                                                             K42.5                                                                              B65.5 I                                      7131                                                                              C.sub.7 H.sub.16                                                                            C.sub.7 H.sub.15                                                                             K52.5                                                                              B68 I                                        7132                                                                              C.sub.2 H.sub.5OOCCHCH                                                                      C.sub.4 H.sub.9                                                                              K96.3                                                                              S104 S153.9 I                                7133                                                                              C.sub.2 H.sub.5OOCCHCH                                                                      C.sub.5 H.sub.11                                                                             K88.8                                                                              S88.5 S149.1 I                               7134                                                                              C.sub.2 H.sub.5OOCCHCH                                                                      C.sub.6 H.sub.13                                                                             K74.2                                                                              S81 S146.2 I                                 7135                                                                              C.sub.2 H.sub.5OOCCHCH                                                                      C.sub.7 H.sub.15                                                                             K61 S74 S142.5 I                                 7136                                                                              C.sub.2 H.sub.5OOCCHCH                                                                      C.sub.8 H.sub.17                                                                             K62 S75 S143 I                                   7137                                                                              C.sub.2 H.sub.5OOCCHCH                                                                      C.sub.9 H.sub.19                                                                             K60 S73 S141.4 I                                 7138                                                                              CH.sub.3O    C.sub.3 H.sub.7                                                                              K51.9                                                                              S27.9 A33.6 I                                7139                                                                              CH.sub.3O    C.sub.4 H.sub.9                                                                              K38.7                                                                              S26.2 A36.7 I                                7140                                                                              CH.sub.3O    C.sub.5 H.sub.11                                                                             K38 S23.5 A31.2 I                                7141                                                                              CH.sub.3O    C.sub.6 H.sub.13                                                                             K31.6                                                                              S14 A28.7 I                                  7142                                                                              CH.sub.3O    C.sub.7 H.sub.15                                                                             K36.1                                                                              S23.8 A27.7 N33.6 I                          7148                                                                              C.sub.2 H.sub.5O                                                                            C.sub.4 H.sub.9                                                                              K49.3                                                                              A67.1 I                                      7149                                                                              C.sub.4 H.sub.9O                                                                            C.sub.4 H.sub.9                                                                              K7.4                                                                               S76 A96.2 I                                  7150                                                                              C.sub.4 H.sub.9O                                                                            C.sub.5 H.sub.11                                                                             K11.3                                                                              S53.4 I                                      7151                                                                              C.sub.4 H.sub.9O                                                                            C.sub.6 H.sub.13                                                                             K20.8                                                                              S54.5 A83.4 I                                7152                                                                              C.sub.5 H.sub.11O                                                                           C.sub.3 H.sub.7                                                                              K36.5                                                                              S74 S76.5 I                                  7153                                                                              C.sub.5 H.sub.11O                                                                           C.sub.4 H.sub.9                                                                              K59.5                                                                              S61.5 S81.2 I                                7154                                                                              C.sub.5 H.sub.11O                                                                           C.sub.5 H.sub.11                                                                             K39.5                                                                              S54 S84.8 I                                  7155                                                                              C.sub.5 H.sub.11O                                                                           C.sub.6 H.sub.13                                                                             K40.5                                                                              S46.5 S85.5 I                                __________________________________________________________________________

                  TABLE 2                                                          ______________________________________                                          ##STR10##                                                                     No    L          R        Cr     LC                                            ______________________________________                                         7156  C.sub.5 H.sub.11 O                                                                        C.sub.7 H.sub.15                                                                        K35.4  S84.8    I                                    7157  C.sub.5 H.sub.11 O                                                                        C.sub.8 H.sub.17                                                                        K39.5  S84      I                                    7158  C.sub.5 H.sub.11 O                                                                        C.sub.9 H.sub.19                                                                        K42.5  S82.5    I                                    7159  C.sub.6 H.sub.13 O                                                                        C.sub.4 H.sub.9                                                                         K18.2  S43.4 A74.1                                                                             I                                    7160  C.sub.6 H.sub.13 O                                                                        C.sub.9 H.sub.19                                                                        K35    B87      I                                    7161  C.sub.7 H.sub.15 O                                                                        C.sub.3 H.sub.7                                                                         K47    B72      I                                    7162  C.sub.7 H.sub.15 O                                                                        C.sub.7 H.sub.15                                                                        K53.5  B85.5    I                                    7163  C.sub.5 H.sub.11 CO                                                                       C.sub.5 H.sub.11                                                                        K75.5  S104.5   I                                    7164  C.sub.5 H.sub.11 CO                                                                       C.sub.6 H.sub.13                                                                        K80.5  S102 S103                                                                               I                                    7165  C.sub.5 H.sub.11 CO                                                                       C.sub.7 H.sub.15                                                                        K71    S95 S101 I                                    7166  C.sub.5 H.sub.11 CO                                                                       C.sub.8 H.sub.17                                                                        K87    S95.3 S98                                                                               I                                    7167  C.sub.5 H.sub.11 CO                                                                       C.sub.9 H.sub.19                                                                        K84.5  S93.8 S99.6                                                                             I                                    7168  C.sub.6 H.sub.13 CO                                                                       C.sub.8 H.sub.17                                                                        K72    S101.8 S105.8                                                                           I                                    7169  C.sub.7 H.sub.15 CO                                                                       C.sub.8 H.sub.17                                                                        K86.6  S97 S104.5                                                                              I                                    ______________________________________                                    

                  TABLE 3                                                          ______________________________________                                          ##STR11##                                                                     No    L          R           Cr    LC                                          ______________________________________                                         26206 C.sub.3 H.sub.7                                                                           C.sub.3 H.sub.7                                                                            K90   P120 P190                                                                              I                                   26207 C.sub.4 H.sub.9                                                                           C.sub.4 H.sub.9                                                                            K57   P119 P190                                                                              I                                   26208 C.sub.5 H.sub.11                                                                          C.sub.5 H.sub.11                                                                           K41   P114 P190                                                                              I                                   26209 C.sub.6 H.sub.13                                                                          C.sub.6 H.sub.13                                                                           K55   P184    I                                   26210 C.sub.7 H.sub.15                                                                          C.sub.7 H.sub.15                                                                           K28   P180    I                                   26211 C.sub.8 H.sub.17                                                                          C.sub.8 H.sub.17                                                                           K39   P173    I                                   26212 C.sub.9 H.sub.19                                                                          C.sub.9 H.sub.19                                                                           K45   P165    I                                   26213 C.sub.10 H.sub.21                                                                         C.sub.10 H.sub.21                                                                          K62   P160    I                                   26217 C.sub.2 H.sub.5                                                                           OC.sub.2 H.sub.5                                                                           K166  S182    I                                   26221 C.sub.3 H.sub.7 O                                                                         OC.sub.3 H.sub.7                                                                           K210  P215    I                                   26222 C.sub.4 H.sub.9 O                                                                         OC.sub.4 H.sub.9                                                                           K197  P227    I                                   26223 C.sub.5 H.sub.11 O                                                                        OC.sub.5 H.sub.11                                                                          K185  P218    I                                   26224 C.sub.6 H.sub.13 O                                                                        OC.sub.6 H.sub.13                                                                          K172  P218    I                                   26225 C.sub.7 H.sub.15 O                                                                        OC.sub.7 H.sub.15                                                                          K166  P209    I                                   26226 C.sub.8 H.sub.17 O                                                                        OC.sub.8 H.sub.17                                                                          K163  P203    I                                   26227 C.sub.9 H.sub.19 O                                                                        OC.sub.9 H.sub.19                                                                          K162  P194    I                                   26228 C.sub.10 H.sub.21O                                                                        OC.sub.10 H.sub.24                                                                         K161  P189    I                                   26230 CH.sub.3 O OOCC.sub.2 H.sub.5                                                                         K148  S155 N193                                                                              I                                   ______________________________________                                          ##STR12##                                                                     No    L        R        Cr    LC                                               ______________________________________                                         28692 C.sub.3 H.sub.7                                                                         C.sub.3 H.sub.7                                                                         K163.3                                                                               B171.5      I                                    28693 C.sub.4 H.sub.9                                                                         C.sub.4 H.sub.9                                                                         K36.3 E106.9 S113.4 B179.5                                                                       I                                    28694 C.sub.5 H.sub.11                                                                        C.sub.5 H.sub.11                                                                        K50   B155.9      U                                    28695 C.sub.6 H.sub.13                                                                        C.sub.6 H.sub.13                                                                        K30   E76.7 S107.9 B182.8                                                                        I                                    28696 C.sub.7 H.sub.15                                                                        C.sub.7 H.sub.15                                                                        K27.7 E82 S100.4 B175.5                                                                          I                                    28697 C.sub.8 H.sub.17                                                                        C.sub.8 H.sub.17                                                                        K58.1 E64.5 S93.4 B178.3                                                                         I                                    28698 C.sub.9 H.sub.19                                                                        C.sub.9 H.sub.19                                                                        K52.6 E75.3 S87.3 B174.1                                                                         I                                    ______________________________________                                    

                                      TABLE 4                                      __________________________________________________________________________      ##STR13##                                                                     No  L             R        Cr  LC                                              __________________________________________________________________________     22075                                                                              C.sub.6 H.sub.13 CHMeOOC                                                                     OC.sub.10 H.sub.21                                                                    1 K?  A? I                                            22076                                                                              C.sub.2 H.sub.5 CHMeCH.sub.2 OOC                                                             OC.sub.10 H.sub.21                                                                    1 K22 A48                                                                               I                                            22077                                                                              C.sub.6 H.sub.13 CHCF.sub.3 OOC                                                              OC.sub.10 H.sub.21                                                                    1 K-13                                                                               A-6                                                                               I                                            __________________________________________________________________________      ##STR14##                                                                     No     L       R     Cr  LC                                                    __________________________________________________________________________     8085   C.sub.8 H.sub.17 O                                                                     C.sub.5 H.sub.11                                                                     K36 C44.5 A75 N83.5                                                                         I                                            __________________________________________________________________________

                                      TABLE 5                                      __________________________________________________________________________      ##STR15##                                                                     No  L      R      Cr   LC                                                      __________________________________________________________________________     22305                                                                              C.sub.7 H.sub.15                                                                      C.sub.7 H.sub.15                                                                      K83.1                                                                               C58 N109.5 I                                            22307                                                                              C.sub.6 H.sub.13 O                                                                    C.sub.5 H.sub.11                                                                      K81  A85 N120   I                                            22309                                                                              C.sub.8 H.sub.17 O                                                                    C.sub.7 H.sub.15                                                                      K73  A106.1 N111.3                                                                             I                                            22317                                                                              C.sub.7 H.sub.15                                                                      OC.sub.7 H.sub.15                                                                     K83.1                                                                               C58 N109.5 I                                            22318                                                                              C.sub.8 H.sub.17                                                                      OC.sub.6 H.sub.13                                                                     K70  C73 N109   I                                            22320                                                                              C.sub.6 H.sub.13 O                                                                    OC.sub.7 H.sub.15                                                                     K82  C88.4 N133.4                                                                              I                                            22321                                                                              C.sub.6 H.sub.13 O                                                                    OC.sub.8 H.sub.17                                                                     K85.1                                                                               C89.1 N133.3                                                                              I                                            22322                                                                              C.sub.7 H.sub.15 O                                                                    OC.sub.7 H.sub.15                                                                     K88.9                                                                               C94.7 A105.5 N129.8                                                                       I                                            22323                                                                              C.sub.7 H.sub.15 O                                                                    OC.sub.8 H.sub.17                                                                     K82.5                                                                               C103.8 A110.7 N132.2                                                                      I                                            22324                                                                              C.sub.7 H.sub.15 O                                                                    OC.sub.9 H.sub.19                                                                     K90.4                                                                               C103 A113.8 N128                                                                          I                                            22325                                                                              C.sub.8 H.sub.17 O                                                                    OC.sub.7 H.sub.15                                                                     K84.7                                                                               C93.8 A115.7 N129.7                                                                       I                                            22326                                                                              C.sub.8 H.sub.17 O                                                                    OC.sub.8 H.sub.17                                                                     K85.5                                                                               C101.8 A119.8 N131                                                                        I                                            22327                                                                              C.sub.8 H.sub.17 O                                                                    OC.sub.9 H.sub.19                                                                     K90  C104.2 A122.4 N131.8                                                                      I                                            __________________________________________________________________________

                                      TABLE 6                                      __________________________________________________________________________      ##STR16##                                                                     No  L      R                  Cr  LC                                           __________________________________________________________________________     22328                                                                              C.sub.9 H.sub.19 O                                                                    OC.sub.8 H.sub.17  K87 C106.3 A122.5 N129.8                                                                      I                                 22329                                                                              C.sub.9 H.sub.19 O                                                                    OC.sub.9 H.sub.19  K89.4                                                                              C115.5 A125.7 N128.4                                                                      I                                 22333                                                                              C.sub.4 H.sub.9                                                                       COC.sub.4 H.sub.9  K116                                                                               S120 N130  I                                 22334                                                                              C.sub.10 H.sub.21 O                                                                   COOCH(C.sub.3 H.sub.6 /C.sub.2 H.sub.5).sub.2                                                   R K<30                                                                               A25        I                                 22337                                                                              C.sub.8 H.sub.17 O                                                                    COOCHMeC.sub.6 H.sub.13                                                                         R K69.3                                                                              A62.1      I                                 22338                                                                              C.sub.10 H.sub.21 O                                                                   COOCHMeC.sub.6 H.sub.13                                                                         R K60 A20        U                                 22341                                                                              C.sub.10 H.sub.21 O                                                                   COOCH.sub.2 CHMeC.sub.2 H.sub.5                                                                 1 K85.2                                                                              A103.6     I                                 22342                                                                              C.sub.9 H.sub.19 O                                                                    CHCHCOOCHCF.sub.3 C.sub.6 H.sub.13                                                              R K51 CA63 A69   I                                 22343                                                                              C.sub.10 H.sub.21 O                                                                   CHCHCOOCHCF.sub.3 C.sub.6 H.sub.13                                                              R K50 CA56 A66   I                                 22344                                                                              C.sub.11 H.sub.23 O                                                                   CHCHCOOCHCF.sub.3 C.sub.6 H.sub.13                                                              R K45 CA52 A61   I                                 22345                                                                              C.sub.10 H.sub.21 O                                                                   COOCHCF.sub.3 C.sub.6 H.sub.13                                                                  1 K<-30                                                                              A25        I                                 22346                                                                              C.sub.10 H.sub.21 O                                                                   COOCHCF.sub.3 C.sub.8 H.sub.17                                                                  1 K?  S6 A13.3   I                                 22347                                                                              C.sub.10 H.sub.21 O                                                                   COOCHCF.sub.3 C.sub.6 H.sub.13                                                                  2 K52 A61        I                                 __________________________________________________________________________

                                      TABLE 7                                      __________________________________________________________________________      ##STR17##                                                                     No  L           R                Cr  LC                                        __________________________________________________________________________     35478                                                                              C.sub.4 H.sub.9 O                                                                          CN               K158                                                                               N>300         Z                           35479                                                                              C.sub.7 H.sub.15 O                                                                         CN               K132                                                                               N292          Z                           35481                                                                              C.sub.8 H.sub.17 O                                                                         CHMeCOSC.sub.6 H.sub.13                                                                       1 K89.2                                                                              C*120 A140.7  I                           35482                                                                              C.sub.9 H.sub.19 O                                                                         CHMeCOSC.sub.6 H.sub.13                                                                       1 K86.7                                                                              C*125.3 A135.7                                                                               I                           35483                                                                              C.sub.10 H.sub.21 O                                                                        CHMeCOSC.sub.6 H.sub.13                                                                       1 K85.4                                                                              C*127.5 A133.6                                                                               I                           35484                                                                              C.sub.11 H.sub.23 O                                                                        CHMeCOSC.sub.6 H.sub.13                                                                       1 K83.3                                                                              S112.8 C*128.2 A131.1                                                                        I                           35485                                                                              C.sub.12 H.sub.25 O                                                                        CHMeCOSC.sub.6 H.sub.13                                                                       1 K86.9                                                                              S104.8 C*128.6 A129.1                                                                        I                           35486                                                                              C.sub.13 H.sub.27 O                                                                        CHMeCOSC.sub.6 H.sub.13                                                                       1 K81.9                                                                              S102.6 C*128.8                                                                               I                           35487                                                                              C.sub.14 H.sub.29 O                                                                        CHMeCOSC.sub.6 H.sub.13                                                                       1 K77.4                                                                              S103 C*124.4  I                           35488                                                                              C.sub.7 H.sub.15 O                                                                         CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K98 C*100.8 A141.8 N*151                                                                         I                           35489                                                                              C.sub.8 H.sub.17 O                                                                         CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K94.1                                                                              C*101.6 A139.1 N*147.9                                                                       I                           35490                                                                              C.sub.9 H.sub.19 O                                                                         CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K79.1                                                                              C*105.9 A134.1 A#? N*142.8                                                                   I                           35491                                                                              C.sub.10 H.sub.21 O                                                                        CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K66.9                                                                              C*108.4 A#138.6 N*147.9                                                                      I                           35492                                                                              C.sub.11 H.sub.23 O                                                                        CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K73.3                                                                              C*114.1 A#127.5 N*134.3                                                                      I                           35493                                                                              C.sub.12 H.sub.25 O                                                                        CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K69 C*113.4 A#126.4 N*132.6                                                                      I                           35494                                                                              C.sub.13 H.sub.27 O                                                                        CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K68.6                                                                              C*119.7 A#133.7 N*138.5                                                                      I                           35495                                                                              C.sub.14 H.sub.29 O                                                                        CHMeCOOCHMeC.sub.3 H.sub.7                                                                    5 K71.7                                                                              C*119.4 A#132.8 N*136.5                                                                      I                           35496                                                                              C.sub.8 H.sub.17 O                                                                         COOCHCF.sub.3 C.sub.6 H.sub.13                                                                1 K93.5                                                                              S147.4 C*150.7 A176.4                                                                        I                           35497                                                                              C.sub.8 H.sub.17 O                                                                         COOCHCF.sub.3 C.sub.8 H.sub.17                                                                1 K84 S133 C*135.6 A163.8                                                                          I                           35498                                                                              C.sub.6 H.sub.13 CHCF.sub.3 OOC                                                            OC.sub.10 H.sub.21                                                                            1 K?  S10 S75 C*106 A150.5                                                                         I                           __________________________________________________________________________

                                      TABLE 8                                      __________________________________________________________________________      ##STR18##                                                                     No       L         R         Cr LC                                             __________________________________________________________________________     46421    C.sub.8 H.sub.17                                                                         C.sub.5 H.sub.11                                                                         K54                                                                               S142.5 N178                                                                               I                                   __________________________________________________________________________      ##STR19##                                                                     No  L              R             Cr  LC                                        __________________________________________________________________________     35500                                                                              C.sub.7 H.sub.15                                                                              F             K114.9                                                                             S187.9 N229.7                                                                             I                              35501                                                                              C.sub.7 H.sub.15 O                                                                            CN            K136                                                                               N304       Z                              35502                                                                              H.sub.2 CCHCOOC.sub.5 H.sub.12 O                                                              NO.sub.2      K134                                                                               S>180      Z                              35503                                                                              C.sub.6 H.sub.13 CHCF.sub.3 OOC                                                               C.sub.10 H.sub.21                                                                          1 K49.5                                                                              A127.7     I                              35504                                                                              C.sub.6 H.sub.13 CHCF.sub.3 OOC                                                               OC.sub.10 H.sub.21                                                                         1 K35 S100.4 C*124.5 A152.5                                                                     I                              35505                                                                              C.sub.6 H.sub.13 CHCF.sub.3 OOC                                                               COOC.sub.10 H.sub.21                                                                       1 K40 S96 C*97.7 A123.7                                                                         I                              35506                                                                              C.sub.6 H.sub.13 CHCF.sub.3 OOC                                                               OOCC.sub.10 H.sub.21                                                                       1 K75 S120 C*156.9 A184.2                                                                       I                              35507                                                                              C.sub.10 H.sub.21 O                                                                           COOCHCF.sub.3 C.sub.6 H.sub.13                                                             1 K?  S97 C*120 A151.9                                                                          I                              35508                                                                              C.sub.8 H.sub.17 OOC                                                                          COOCHCF.sub.3 C.sub.6 H.sub.13                                                             1 K?  S64.1 C*66 A108.4                                                                         I                              __________________________________________________________________________      ##STR20##                                                                     No     L          R                  Cr                                                                               LC                                      __________________________________________________________________________     22447  C.sub.5 F.sub.11 CH.sub.2 O                                                               OC.sub.8 H.sub.17  K?                                                                               A92    I                                22448  C.sub.5 F.sub.11 CH.sub.2 O                                                               OC.sub.3 H.sub.6 CHMeC.sub.2 H.sub.5                                                          1   K?                                                                               C*37 A80                                                                              I                                __________________________________________________________________________

                                      TABLE 9                                      __________________________________________________________________________      ##STR21##                                                                     No  L            R         Cr  LC                                              __________________________________________________________________________     7534                                                                               C.sub.8 H.sub.17                                                                            C.sub.6 H.sub.13                                                                         K39.9                                                                              C23 A25.5                                                                             I                                        7538                                                                               C.sub.6 H.sub.13 O                                                                          C.sub.4 H.sub.9                                                                          K68.7                                                                              C45.1 A55.8                                                                           I                                        7539                                                                               C.sub.10 H.sub.21 O                                                                         C.sub.8 H.sub.17                                                                         K57.7                                                                              C71.5 A77.3                                                                           I                                        7542                                                                               C.sub.10 H.sub.21 O                                                                         OC.sub.8 H.sub.17                                                                        K60.1                                                                              C81.7 A89.1                                                                           I                                        7543                                                                               C.sub.8 H.sub.17 O                                                                          COC.sub.10 H.sub.21                                                                      K106.9                                                                             C103.8 A120.4                                                                         I                                        7545                                                                               C.sub.10 H.sub.21 O                                                                         COOC.sub.8 H.sub.17                                                                      K103.6                                                                             A88.2  I                                        7548                                                                               C.sub.6 H.sub.13 COO                                                                        C.sub.8 H.sub.17                                                                         K51.8                                                                              A64.3 N49.8                                                                           U                                        7549                                                                               C.sub.6 H.sub.13 CHFCH.sub.2 O                                                              C.sub.8 H.sub.17                                                                       1 K77.9                                                                              A69.6  I                                        __________________________________________________________________________      ##STR22##                                                                     No     L         R      Cr  LC                                                 __________________________________________________________________________     8788   C.sub.10 H.sub.21 O                                                                      C.sub.4 H.sub.9                                                                       K90.1                                                                              A109.9 I                                           __________________________________________________________________________      ##STR23##                                                                     No     L       R       Cr  LC                                                  __________________________________________________________________________     27629  C.sub.8 H.sub.17                                                                       C.sub.12 H.sub.25                                                                      K76.6                                                                              C99.4 N128.2                                                                            I                                          __________________________________________________________________________

                                      TABLE 10                                     __________________________________________________________________________      ##STR24##                                                                     No    L      R      Cr  LC                                                     __________________________________________________________________________     28106 C.sub.8 H.sub.17                                                                      C.sub.8 H.sub.17                                                                      K77.8                                                                              C101.4 N121.8                                                                           I                                             __________________________________________________________________________      ##STR25##                                                                     No   L     R      Cr   LC                                                      __________________________________________________________________________     26603                                                                               C.sub.10 H.sub.21                                                                    C.sub.8 H.sub.17                                                                      K77.5                                                                               C114.9 N123.8                                                                             I                                            26604                                                                               C.sub.10 H.sub.21                                                                    OC.sub.10 H.sub.21                                                                    K92.2                                                                               C132.8 A135.9 N143.4                                                                      I                                            __________________________________________________________________________      ##STR26##                                                                     No     L      R       Cr LC                                                    __________________________________________________________________________     8726   C.sub.4 H.sub.9                                                                       C.sub.6 H.sub.13                                                                       K90                                                                               A96 N106                                                                              I                                              __________________________________________________________________________

                  TABLE 11                                                         ______________________________________                                          ##STR27##                                                                     No     L       R           Cr    LC                                            ______________________________________                                         27356  H       OC.sub.4 H.sub.9                                                                           K211  A207 N240                                                                               I                                    27357  H       OC.sub.6 H.sub.13                                                                          K183  B225 A228                                                                               U                                    ______________________________________                                          ##STR28##                                                                     No     L          R       Cr    LC                                             ______________________________________                                         27633  C.sub.4 H.sub.9                                                                           H       K75   S96       I                                    27634  C.sub.5 H.sub.11                                                                          H       K65   S106      I                                    27635  C.sub.6 H.sub.13                                                                          H       K55   S103      I                                    27636  C.sub.7 H.sub.15                                                                          H       K48   S100 S103 S107                                                                           I                                    27637  C.sub.8 H.sub.17                                                                          H       K42   S102      I                                    27638  C.sub.4 H.sub.9 O                                                                         H       K106  S136      I                                    27639  C.sub.5 H.sub.11 O                                                                        H       K62   S133      I                                    27640  C.sub.6 H.sub.13 O                                                                        H       K76   S133      I                                    27641  C.sub.7 H.sub.15 O                                                                        H       K63   S136      I                                    27642  C.sub.8 H.sub.17 O                                                                        H       K54   S137      I                                    ______________________________________                                          ##STR29##                                                                     No     L          R           Cr    LC                                         ______________________________________                                         8268   C.sub.4 H.sub.9 S                                                                         Br          K?          I                                    8269   C.sub.4 H.sub.9 S                                                                         CN          K30.3 N-63  E                                    8270   C.sub.7 H.sub.15                                                                          C.sub.7 H.sub.15                                                                           K56         I                                    8278   C.sub.7 H.sub.15                                                                          COOC.sub.2 H.sub.5                                                                         K84   S47   I                                    8279   C.sub.4 H.sub.9 O                                                                         COOC.sub.2 H.sub.5                                                                         K87   S86   I                                    8280   C.sub.5 H.sub.11 O                                                                        COOC.sub.2 H.sub.5                                                                         K72   S90   I                                    8281   C.sub.6 H.sub.13 O                                                                        COOC.sub.2 H.sub.5                                                                         K60   S82   I                                    8282   C.sub.7 H.sub.15 O                                                                        COOC.sub.2 H.sub.5                                                                         K86   S82   I                                    8283   C.sub.8 H.sub.17 O                                                                        COOC.sub.2 H.sub.5                                                                         K72   S84   I                                    ______________________________________                                    

                                      TABLE 12                                     __________________________________________________________________________      ##STR30##                                                                     No    L      R       Cr  LC                                                    __________________________________________________________________________     29065 C.sub.3 H.sub.7                                                                       C.sub.3 H.sub.7                                                                        K50 S74     I                                             29066 C.sub.4 H.sub.9                                                                       C.sub.4 H.sub.9                                                                        K50 S75     I                                             29067 C.sub.5 H.sub.11                                                                      C.sub.5 H.sub.11                                                                       K53 S77     I                                             29068 C.sub.6 H.sub.13                                                                      C.sub.6 H.sub.13                                                                       K51 S82     I                                             29069 C.sub.7 H.sub.15                                                                      C.sub.7 H.sub.15                                                                       K55 G78 F83 C89                                                                            I                                             29070 C.sub.8 H.sub.17                                                                      C.sub.8 H.sub.17                                                                       K65 G72 F87 C91                                                                            I                                             29071 C.sub.9 H.sub.19                                                                      C.sub.9 H.sub.12                                                                       K64 G62 F91 C95                                                                            I                                             29072 C.sub.10 H.sub.21                                                                     C.sub.10 H.sub.21                                                                      K71 F95 C96 I                                             29074 C.sub.4 H.sub.9                                                                       COC.sub.3 H.sub.7                                                                      K148.3                                                                             A155.7  I                                             29075 C.sub.5 H.sub.11                                                                      COC.sub.4 H.sub.9                                                                      K137.2                                                                             A163    I                                             29076 C.sub.6 H.sub.13                                                                      COC.sub.5 H.sub.11                                                                     K138.4                                                                             A162    I                                             29077 C.sub.7 H.sub.15                                                                      COC.sub.6 H.sub.13                                                                     K132                                                                               C138.9 A161.8                                         29078 C.sub.8 H.sub.17                                                                      COC.sub.7 H.sub.15                                                                     K133                                                                               C151 A159.7                                                                            I                                             29079 C.sub.9 H.sub.19                                                                      COC.sub.8 H.sub.17                                                                     K129.4                                                                             C154.2 A158.7                                                                          I                                             29080 C.sub.10 H.sub.21                                                                     COC.sub.9 H.sub.19                                                                     K127                                                                               C152    I                                             __________________________________________________________________________      ##STR31##                                                                     No  L           R      Cr  LC                                                  __________________________________________________________________________     5713                                                                               Br          COC.sub.7 H.sub.15                                                                    K116.1                                                                             A123.8 I                                            5719                                                                               NC          C.sub.8 H.sub.17                                                                      K49.9                                                                              A20.8 N22.2                                                                           I                                            5723                                                                               NC          SC.sub.4 H.sub.9                                                                      K32.6                                                                              N-52   E                                            5727                                                                               C.sub.4 H.sub.9 SiMe.sub.2 C.sub.3 H.sub.6 O                                               C.sub.10 H.sub.21                                                                     K57 S43    I                                            5730                                                                               C.sub.4 H.sub.9 S                                                                          CN     K55.7                                                                              N5     E                                            5732                                                                               C.sub.2 H.sub.5 O                                                                          COC.sub.7 H.sub.15                                                                    K120.8                                                                             A123.1 I                                            5733                                                                               C.sub.3 H.sub.7 O                                                                          COC.sub.7 H.sub.15                                                                    K124.4                                                                             A122.8 I                                            5734                                                                               C.sub.4 H.sub.9 O                                                                          COC.sub.7 H.sub.15                                                                    K127.6                                                                             A130.9 I                                            5735                                                                               C.sub.5 H.sub.11 O                                                                         COC.sub.7 H.sub.15                                                                    K120.5                                                                             A127.4 I                                            5736                                                                               C.sub.6 H.sub.13 O                                                                         COC.sub.7 H.sub.15                                                                    K120                                                                               A129.8 I                                            5737                                                                               C.sub.7 H.sub.15 O                                                                         COC.sub.7 H.sub.15                                                                    K113                                                                               A127.4 I                                            5738                                                                               C.sub.8 H.sub.17 O                                                                         COC.sub.7 H.sub.15                                                                    K109.5                                                                             A126.2 I                                            5739                                                                               C.sub.9 H.sub.19 O                                                                         COC.sub.7 H.sub.15                                                                    K107.5                                                                             A123.8 I                                            5740                                                                               C.sub.12 H.sub.25 O                                                                        COC.sub.7 H.sub.15                                                                    K100.6                                                                             S93.8 A122.2                                                                          I                                            __________________________________________________________________________

                  TABLE 13                                                         ______________________________________                                          ##STR32##                                                                     No     L         R         Cr     LC                                           ______________________________________                                         36004  C.sub.5 H.sub.11                                                                         C.sub.5 H.sub.11                                                                         K21.5  B88.4 A96.7                                                                             I                                   36005  C.sub.6 H.sub.13                                                                         C.sub.5 H.sub.11                                                                         K22.5  B94.7 A97.2                                                                             I                                   36006  C.sub.7 H.sub.15                                                                         C.sub.5 H.sub.11                                                                         K20.5  B96.2 A99.8                                                                             I                                   36007  C.sub.8 H.sub.17                                                                         C.sub.5 H.sub.11                                                                         K21    B96.8 A99.1                                                                             I                                   36008  C.sub.9 H.sub.19                                                                         C.sub.5 H.sub.11                                                                         K23.7  B97.2 A100.1                                                                            I                                   36009  C.sub.10 H.sub.21                                                                        C.sub.5 H.sub.11                                                                         K55    B98.4    I                                   ______________________________________                                          ##STR33##                                                                     No      L           R         Cr   LC                                          ______________________________________                                         27648   C.sub.4 H.sub.9 O                                                                          H         K128 S150  I                                     27649   C.sub.6 H.sub.13                                                                           C.sub.2 H.sub.5                                                                          K56  S155  I                                     27650   C.sub.4 H.sub.9 O                                                                          C.sub.2 H.sub.5                                                                          K102 S180  I                                     27651   C.sub.4 H.sub.9 O                                                                          C.sub.5 H.sub.11                                                                         K61  S176  I                                     ______________________________________                                          ##STR34##                                                                     No    L        R          Cr    LC                                             ______________________________________                                         27643 C.sub.5 H.sub.11                                                                        C.sub.5 H.sub.11                                                                          K42.4 C47.9 A62 N97.8                                                                          I                                    27644 C.sub.5 H.sub.11                                                                        COC.sub.4 H.sub.9                                                                         K74.9 A186.8    I                                    ______________________________________                                    

                                      TABLE 14                                     __________________________________________________________________________      ##STR35##                                                                     No     L      R         Cr LC                                                  __________________________________________________________________________     25783  C.sub.6 H.sub.3                                                                       OC.sub.6 H.sub.13                                                                        K148                                                                              A152 N155                                                                               I                                          __________________________________________________________________________      ##STR36##                                                                     No  L           R           Cr  LC                                             __________________________________________________________________________     25800                                                                              C.sub.6 H.sub.13 O                                                                         OC.sub.6 H.sub.13                                                                          K110.8                                                                             C130.6 N161                                                                           I                                       25801                                                                              C.sub.7 H.sub.15 O                                                                         OC.sub.7 H.sub.15                                                                          K109.8                                                                             C139.4 N155.8                                                                         I                                       25802                                                                              C.sub.8 H.sub.17 O                                                                         OC.sub.8 H.sub.17                                                                          K107.3                                                                             C149 N157.3                                                                           I                                       25803                                                                              C.sub.10 H.sub.21 O                                                                        OC.sub.10 H.sub.21                                                                         K98.6                                                                              C147.4 I                                       25805                                                                              H.sub.2 CCHC.sub.4 H.sub.8 O                                                               OC.sub.4 H.sub.8 CHCH.sub.2                                                                K99 A114 N144                                                                             I                                       25806                                                                              H.sub.2 CCHC.sub.9 H.sub.18 O                                                              OC.sub.9 H.sub.18 CHCH.sub.2                                                               K92 A145   I                                       __________________________________________________________________________      ##STR37##                                                                     No  L             R      Cr  LC                                                __________________________________________________________________________     25816                                                                              Me.sub.3 SiC.sub.3 H.sub.6 O                                                                 C.sub.6 H.sub.13                                                                      K96 C109     I                                        25817                                                                              C.sub.4 H.sub.9 SiMe.sub.2 C.sub.3 H.sub.6 COO                                               C.sub.6 H.sub.13                                                                      K51 C90      I                                        25818                                                                              C.sub.6 H.sub.13                                                                             C.sub.6 H.sub.13                                                                      K68.8                                                                              A116.5 N120.1                                                                           I                                        25819                                                                              C.sub.9 H.sub.19                                                                             C.sub.6 H.sub.13                                                                      K61 C72.2 A126.8                                                                            I                                        25828                                                                              C.sub.3 H.sub.7 O                                                                            C.sub.6 H.sub.13                                                                      K79 C70 A101 N147.5                                                                         I                                        25841                                                                              C.sub.3 H.sub.7 O                                                                            OC.sub.8 H.sub.17                                                                     K78 C98 N161 I                                        25842                                                                              C.sub.4 H.sub.9 COO                                                                          C.sub.6 H.sub.13                                                                      K101.9                                                                             C128.5 N149.4                                                                           I                                        __________________________________________________________________________

                                      TABLE 15                                     __________________________________________________________________________      ##STR38##                                                                     No   L       R     Cr   LC                                                     __________________________________________________________________________     25843                                                                               C.sub.6 H.sub.13 COO                                                                   C.sub.6 H.sub.13                                                                     K73.1                                                                               S83.2 C139.3 N148.7                                                                      I                                            25844                                                                               C.sub.8 H.sub.17 COO                                                                   C.sub.6 H.sub.13                                                                     K58  S75.8 C146.4 N148.1                                                                      I                                            25845                                                                               C.sub.8 H.sub.17 COO                                                                   C.sub.8 H.sub.17                                                                     K59.4                                                                               S74.5 S78.5 C148.5                                                                       I                                            25846                                                                               C.sub.10 H.sub.21 COO                                                                  C.sub.6 H.sub.13                                                                     K74.9                                                                               S86.2 C147                                                                               I                                            __________________________________________________________________________      ##STR39##                                                                     No    L      R      Cr  LC                                                     __________________________________________________________________________     26979 C.sub.6 H.sub.13                                                                      C.sub.9 H.sub.19                                                                      K134.2                                                                             S166.3 S167.3                                                                           I                                             __________________________________________________________________________      ##STR40##                                                                     No     L      R       Cr LC                                                    __________________________________________________________________________     26980  C.sub.4 H.sub.9                                                                       C.sub.7 H.sub.15                                                                       K76                                                                               S130 N137                                                                              I                                             __________________________________________________________________________      ##STR41##                                                                     No   L     R       Cr  LC                                                      __________________________________________________________________________     25848                                                                               C.sub.10 H.sub.21                                                                    OCH.sub.3                                                                              K95 N154       U                                            25849                                                                               C.sub.10 H.sub.21                                                                    OC.sub.6 H.sub.13                                                                      K43 C53 A142   U                                            25850                                                                               C.sub.10 H.sub.21                                                                    OC.sub.7 H.sub.15                                                                      K54 B64 C110 A143                                                                             U                                            25851                                                                               C.sub.10 H.sub.21                                                                    OC.sub.8 H.sub.17                                                                      K59 B73 C120 A146                                                                             U                                            25852                                                                               C.sub.10 H.sub.21                                                                    OC.sub.10 H.sub.21                                                                     K66 B84 C137 A144.6                                                                           I                                            __________________________________________________________________________

                                      TABLE 16                                     __________________________________________________________________________      ##STR42##                                                                     No   L    R            Cr  LC                                                  __________________________________________________________________________     7226 NC   C.sub.8 H.sub.17                                                                            K48 A91.5 N113                                                                            I                                            7227 NC   C.sub.9 H.sub.19                                                                            K44 A95 N104                                                                              I                                            7235 NC   OC.sub.8 H.sub.17                                                                           K85 A94 N140                                                                              I                                            7243 NC   OOCCHCHCH.sub.3                                                                             K139                                                                               N259   Z                                            7244 NC   OOCCHCHC.sub.2 H.sub.5                                                                      K113                                                                               N229   Z                                            __________________________________________________________________________      ##STR43##                                                                     No   L      R      Cr   LC                                                     __________________________________________________________________________     8776 C.sub.5 H.sub.11                                                                      C.sub.5 H.sub.11                                                                      K146.5                                                                              E145.5 A163.5 N171.5                                                                      I                                           8777 C.sub.6 H.sub.13                                                                      C.sub.6 H.sub.13                                                                      K138 E135.5 A156.5                                                                             I                                           8778 C.sub.7 H.sub.15                                                                      C.sub.7 H.sub.15                                                                      K125.5                                                                              E135.5 A163                                                                               I                                           8779 C.sub.8 H.sub.17                                                                      C.sub.8 H.sub.17                                                                      K123 E129 A156.5                                                                               I                                           8780 C.sub.9 H.sub.19                                                                      C.sub.9 H.sub.19                                                                      K113.5                                                                              E110 A148  I                                           8783 C.sub.3 H.sub.7 O                                                                     OC.sub.3 H.sub.7                                                                      K194 A237 N278  I                                           8784 C.sub.4 H.sub.9 O                                                                     OC.sub.4 H.sub.9                                                                      K136 E190 A241 N256                                                                            I                                           8785 C.sub.5 H.sub.11 O                                                                    OC.sub.9 H.sub.11                                                                     K136 E178 A236 N244                                                                            I                                           8786 C.sub.6 H.sub.13 O                                                                    OC.sub.6 H.sub.13                                                                     K141 E170 A229  I                                           8787 C.sub.7 H.sub.15 O                                                                    OC.sub.7 H.sub.15                                                                     K130 E163 N225  I                                           __________________________________________________________________________

                                      TABLE 17                                     __________________________________________________________________________      ##STR44##                                                                     No         L       R         Cr     LC                                         __________________________________________________________________________     22138      NC      OC.sub.8 H.sub.17                                                                        K128   A122 N156 I                                22139      NC      OC.sub.9 H.sub.19                                                                        K125   A140 N152 I                                22140      NC      OC.sub.10 H.sub.21                                                                       K125   A146 N149 I                                22141      NC      OC.sub.11 H.sub.23                                                                       K122.5 A149 I                                     22142      NC      OC.sub.12 H.sub.25                                                                       K123   A151 I                                     22146      O.sub.2 N                                                                              OC.sub.8 H.sub.17                                                                        K98    A109 N136 I                                22147      O.sub.2 N                                                                              OC.sub.9 H.sub.19                                                                        K94    A127.5 N135 I                              22148      O.sub.2 N                                                                              OC.sub.10 H.sub.21                                                                       K93    A135 N135.5 I                              22149      O.sub.2 N                                                                              OC.sub.11 H.sub.23                                                                       K92    A136.5 I                                   22150      O.sub.2 N                                                                              OC.sub.12 H.sub.25                                                                       K92    A136.5 I                                   22161      C.sub.9 H.sub.19                                                                       CN        K74    A105.9 N131.11                             __________________________________________________________________________      ##STR45##                                                                     No  L             R                Cr  LC                                      __________________________________________________________________________     22168                                                                              C.sub.10 H.sub.21O                                                                           CN               K78 R72 A139 N152 I                         22169                                                                              C.sub.11 H.sub.23O                                                                           CN               K79 A146 N149.5 I                           22172                                                                              C.sub.8 H.sub.17S                                                                            CN               K99 A109.5 N129.5 I                         22173                                                                              C.sub.9 H.sub..sub.19S                                                                       CN               K107                                                                               A122 N127 I                             22174                                                                              C.sub.10 H.sub.21S                                                                           CN               K100                                                                               A128.5 I                                22175                                                                              C.sub.11 H.sub.23S                                                                           CN               K100                                                                               A130.5 I                                22176                                                                              C.sub.12 H.sub.25S                                                                           CN               K104                                                                               A133 I                                  22181                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                         CN             S K80 A122 N*135 I                            22182                                                                              C.sub.9 H.sub..sub.19O                                                                       COOC.sub.3 H.sub.6SiMe.sub.2 C.sub.4 H.sub.9                                                    K48 C67 A81 I                               22184                                                                              C.sub.6 H.sub.13O                                                                            C.sub.5 H.sub.11 K81 A84.9 N120 I                            22185                                                                              C.sub.8 H.sub.17O                                                                            C.sub.7 H.sub.15 K73 A106.1 N111.3 I                         22186                                                                              C.sub.10 H.sub.21O                                                                           C.sub.4 H.sub.9CHMeOOCC.sub.2 H.sub.5                                                         1 K22.1                                                                              A9.1 I                                  22187                                                                              C.sub.10 H.sub.21O                                                                           OC.sub.2 H.sub.4OC.sub.4 H.sub.9                                                                K63 C72.3 N98.3 I                           22188                                                                              C.sub.10 H.sub.21O                                                                           OCH.sub.2CHMeOC.sub.2 H.sub.5                                                                 1 K49 C*59 A64 N*73 I                         __________________________________________________________________________

                                      TABLE 18                                     __________________________________________________________________________      ##STR46##                                                                     No       L         R        Cr     LC                                          __________________________________________________________________________     22305    C.sub.7 H.sub.15                                                                         C.sub.7 H.sub.15                                                                        K83.1  C58 N109.5 I                                22307    C.sub.6 H.sub.13O                                                                        C.sub.5 H.sub.11                                                                        K81    A85 N120 I                                  22309    C.sub.8 H.sub.17O                                                                        C.sub.7 H.sub.15                                                                        K73    A106.1 N111.3 I                             22317    C.sub.7 H.sub.15                                                                         OC.sub.7 H.sub.15                                                                       K83.1  C58 N109.5 I                                22318    C.sub.8 H.sub.17                                                                         OC.sub.6 H.sub.13                                                                       K70    C73 N109 I                                  22320    C.sub.6 H.sub.13O                                                                        OC.sub.7 H.sub.15                                                                       K82    C88.4 N133.4 I                              22321    C.sub.6 H.sub.13O                                                                        OC.sub.8 H.sub.17                                                                       K85.1  C89.1 N133.3 I                              22322    C.sub.7 H.sub.15O                                                                        OC.sub.7 H.sub.15                                                                       K88.9  C94.7 A105.5 N129.8 I                       22323    C.sub.7 H.sub.15O                                                                        OC.sub.8 H.sub.17                                                                       K82.5  C103.8 A110.7 N132.2 I                      22324    C.sub.7 H.sub.15O                                                                        OC.sub.9 H.sub.19                                                                       K90.4  C103 A113.8 N128 I                          22325    C.sub.8 H.sub.17O                                                                        OC.sub.7 H.sub.15                                                                       K84.7  C93.8 A115.7 N129.7 I                       22326    C.sub.8 H.sub.17O                                                                        OC.sub.8 H.sub.17                                                                       K85.5  C101.8 A119.8 N131 I                        22327    C.sub.8 H.sub.17O                                                                        OC.sub.9 H.sub.19                                                                       K90    C104.2 A122.4 N131.8                        __________________________________________________________________________                                        I                                            ##STR47##                                                                     No  L              R             Cr  LC                                        __________________________________________________________________________     35500                                                                              C.sub.7 H.sub.15                                                                              F             K114.9                                                                             S187.9 N229.7 I                           35502                                                                              H.sub.2 CCHCOOC.sub.6 H.sub.12O                                                               NO.sub.2      K134                                                                               S>180 Z                                   35503                                                                              C.sub.6 H.sub.13CHCF.sub.3OOC                                                                 C.sub.10 H.sub.21                                                                          1 K49.5                                                                              A127.7 I                                  35504                                                                              C.sub.6 H.sub.13CHCF.sub.3OOC                                                                 OC.sub.10 H.sub.21                                                                         1 K35 S100.4 C*24.5 A152.5 I                    35505                                                                              C.sub.6 H.sub.13CHCF.sub.3OOC                                                                 COOC.sub.10 H.sub.21                                                                       1 K40 S96 C*97.7 A123.7 I                       35506                                                                              C.sub.6 H.sub.13CHCF.sub.3OOC                                                                 OOCC.sub.10 H.sub.21                                                                       1 K75 S120 C*156.9 A184.2 I                     35507                                                                              C.sub.10 H.sub.21O                                                                            COOCHCF.sub.3C.sub.6 H.sub.13                                                              1 K?  S97 C*120 A151.9 I                        35508                                                                              C.sub.8 H.sub.17OOC                                                                           COOCHCF.sub.3C.sub.6 H.sub.13                                                              1 K?  S64.1 C*66 A108.4 I                       __________________________________________________________________________

                  TABLE 19                                                         ______________________________________                                          ##STR48##                                                                     No      L         R         Cr     LC                                          ______________________________________                                         24420   C.sub.8 H.sub.17                                                                         C.sub.5 H.sub.11                                                                         K44.5  S65 N84 I                                   24421   C.sub.8 H.sub.17                                                                         C.sub.6 H.sub.13                                                                         K46.5  S36.5 N69.5 I                               ______________________________________                                          ##STR49##                                                                     No    L         R           Cr     LC                                          ______________________________________                                         8289  C.sub.6 H.sub.13                                                                         OC.sub.6 H.sub.13                                                                          K107.4 C114.1 I                                    8290  C.sub.6 H.sub.13                                                                         CC.sub.10 H.sub.21                                                                         K92.8  C116.5 I                                    8291  C.sub.6 H.sub.13                                                                         OOCC.sub.6 H.sub.13                                                                        K81.7  C106.7 A110.9 I                             ______________________________________                                          ##STR50##                                                                     No    L         R           Cr     LC                                          ______________________________________                                         28262 C.sub.6 H.sub.13                                                                         OC.sub.4 H.sub.9                                                                           K79.5  C155.1 N230.7 I                             28263 C.sub.10 H.sub.21                                                                        OC.sub.10 H.sub.21                                                                         K80.3  C198.2 I                                    28265 C.sub.6 H.sub.13                                                                         OOCC.sub.6 H.sub.13                                                                        K82.3  C199.4 N225.2 I                             ______________________________________                                    

                  TABLE 20                                                         ______________________________________                                          ##STR51##                                                                     No    L         R         Cr     LC                                            ______________________________________                                         8292  C.sub.6 H.sub.13                                                                         C.sub.8 H.sub.17                                                                         K87.3  S118.6 A186.4 I                               8293  C.sub.8 H.sub.17                                                                         C.sub.8 H.sub.17                                                                         K82.4  S92.7 C149 A181.2 I                           ______________________________________                                          ##STR52##                                                                     No    L         R         Cr     LC                                            ______________________________________                                         8294  C.sub.6 H.sub.13                                                                         C.sub.8 H.sub.17                                                                         K84.6  S119.5 A147.5 I                               8295  C.sub.8 H.sub.17                                                                         C.sub.8 H.sub.17                                                                         K34.8  S117.5 A155.2 I                               ______________________________________                                    

                                      TABLE 21                                     __________________________________________________________________________      ##STR53##                                                                     No   L       R            Cr   LC                                              __________________________________________________________________________     25914                                                                               C.sub.5 H.sub.11                                                                       H            K76  N56 U                                           25915                                                                               C.sub.6 H.sub.13                                                                       H            K75  S60 N80 I                                       25916                                                                               C.sub.7 H.sub.15                                                                       H            K79  S64 N86 I                                       25917                                                                               C.sub.12 H.sub.25                                                                      H            K84  A95 I                                           25918                                                                               C.sub.2 H.sub.5O                                                                       H            K120 N165 U                                          25919                                                                               C.sub.3 H.sub.7O                                                                       H            K110 N101 U                                          25920                                                                               C.sub.4 H.sub.9O                                                                       H            K84  N140 U                                          25921                                                                               C.sub.5 H.sub.11O                                                                      H            K80  N134 U                                          25922                                                                               C.sub.6 H.sub.13O                                                                      H            K80.5                                                                               N134 U                                          25923                                                                               C.sub.7 H.sub.15O                                                                      H            K73.5                                                                               N149.5 U                                        25924                                                                               C.sub.8 H.sub.17O                                                                      H            K83  N142.5 U                                        25925                                                                               C.sub.9 H.sub.19O                                                                      H            K96  A126 I                                          25926                                                                               C.sub.10 H.sub.21O                                                                     H            K99  A126 I                                          25931                                                                               C.sub.6 H.sub.13O                                                                      F            K97  A198 I                                          25932                                                                               C.sub.6 H.sub.13O                                                                      Cl           K132 A244 I                                          25933                                                                               C.sub.6 H.sub.13O                                                                      Br           K135 A239 I                                          25934                                                                               C.sub.6 H.sub.13                                                                       CN           K118 A220 N233 I                                     25935                                                                               C.sub.5 H.sub.11O                                                                      CN           K142 A246 N265 I                                     25936                                                                               C.sub.6 H.sub.13O                                                                      CN           K146 A258 N264 I                                     25937                                                                               C.sub.6 H.sub.13O                                                                      NO.sub.2     K123 A241 I                                          25938                                                                               C.sub.10 H.sub.21                                                                      OC.sub.4 H.sub.6SiMe.sub.2 C.sub.4 H.sub.9                                                  K46  C122 E                                          25943                                                                               C.sub.5 H.sub.11                                                                       C.sub.5 H.sub.11                                                                            K93  C123 N164 I                                     25944                                                                               C.sub.6 H.sub.13                                                                       C.sub.6 H.sub.13                                                                            K89  C137 N154 B                                     25945                                                                               C.sub.6 H.sub.13                                                                       C.sub.10 H.sub.21                                                                           K66  C168 N172.9 I                                   25946                                                                               C.sub.7 H.sub.15                                                                       C.sub.7 H.sub.15                                                                            K81  C149 N158 I                                     25947                                                                               C.sub.8 H.sub.17                                                                       C.sub.8 H.sub.17                                                                            K78  C151 N152 B                                     __________________________________________________________________________

                                      TABLE 22                                     __________________________________________________________________________      ##STR54##                                                                     No  L     R               Cr  LC                                               __________________________________________________________________________     25949                                                                              C.sub.2 H.sub.5                                                                      OC.sub.7 H.sub.15                                                                              K67 A142 N178 I                                      25952                                                                              C.sub.5 H.sub.11                                                                     CC.sub.6 H.sub.13                                                                              K55 C158 N186 I                                      25953                                                                              C.sub.5 H.sub.11                                                                     OC.sub.8 H.sub.17                                                                              K80 C167 N182 I                                      25954                                                                              C.sub.6 H.sub.13                                                                     OC.sub.4 H.sub.9                                                                               K80.6                                                                              C141 N183.5 I                                    25955                                                                              C.sub.6 H.sub.13                                                                     OC.sub.7 H.sub.15                                                                              K69 A166 N179 I                                      25956                                                                              C.sub.6 H.sub.13                                                                     OC.sub.9 H.sub.19                                                                              K77 C171 N175 I                                      25957                                                                              C.sub.7 H.sub.15                                                                     OC.sub.8 H.sub.17                                                                              K79 C174 N178 I                                      25958                                                                              C.sub.8 H.sub.17                                                                     OC.sub.7 H.sub.15                                                                              K72 A170 N177 I                                      25960                                                                              C.sub.10 H.sub.21                                                                    OC.sub.7 H.sub.15                                                                              K76 C171 N181 B                                      25961                                                                              C.sub.10 H.sub.21                                                                    OC.sub.6 H.sub.17                                                                              K79 C173 I                                           25962                                                                              C.sub.10 H.sub.21                                                                    OC.sub.10 H.sub.21                                                                             K78 A154 I                                           25963                                                                              C.sub.12 H.sub.25                                                                    OC.sub.9 H.sub.19                                                                              K74 C169 I                                           25965                                                                              C.sub.10 H.sub.21                                                                    COOCH.sub.3     K140                                                                               A224 I                                           25966                                                                              C.sub.6 H.sub.13                                                                     OOCC.sub.8 H.sub.17                                                                            K58.2                                                                              S68.1 C172.6 N176.1 I                            25967                                                                              C.sub.10 H.sub.21                                                                    OOCCH.sub.3     K117                                                                               C134 N183 I                                      25968                                                                              C.sub.10 H.sub.21                                                                    OOCC.sub.2 H.sub.5                                                                             K107                                                                               C153 N181 I                                      25969                                                                              C.sub.10 H.sub.21                                                                    OOCCHMeCCH.sub.3                                                                             1 K108                                                                               C*139 N*140 I                                    25970                                                                              C.sub.10 H.sub.21                                                                    OOCCHMeCC.sub.6 H.sub.13                                                                     1 K110                                                                               C*121 I                                          25971                                                                              C.sub.10 H.sub.21                                                                    OCOOC.sub.4 H.sub.9                                                                            K64 C146 A147 N166 I                                 25972                                                                              C.sub.10 H.sub.21                                                                    OCOOC.sub.7 H.sub.15                                                                           K80 C153 N157 I                                      25974                                                                              CH.sub.3O                                                                            CC.sub.6 H.sub.13                                                                              K93 A109 N215 I                                      25977                                                                              C.sub.4 H.sub.9O                                                                     CC.sub.4 H.sub.9                                                                               K145                                                                               A156 N222 I                                      __________________________________________________________________________

                                      TABLE 23                                     __________________________________________________________________________      ##STR55##                                                                     No  L              R      Cr  LC                                               __________________________________________________________________________     27803                                                                              NC             C.sub.6 H.sub.13                                                                      K128                                                                               A169 N199 I                                      27804                                                                              C.sub.4 H.sub.9                                                                               C.sub.3 H.sub.7                                                                       K76 A96 N150 I                                       27805                                                                              C.sub.4 H.sub.9                                                                               C.sub.4 H.sub.9                                                                       K71 A120 N146 I                                      27806                                                                              C.sub.4 H.sub.9                                                                               C.sub.5 H.sub.11                                                                      K52 A115 N138 I                                      27807                                                                              C.sub.4 H.sub.9                                                                               C.sub.6 H.sub.13                                                                      K58 A117 N151 I                                      27808                                                                              C.sub.6 H.sub.13                                                                              C.sub.2 H.sub.5                                                                       K50 A77 N115 I                                       27809                                                                              C.sub.6 H.sub.13                                                                              C.sub.3 H.sub.7                                                                       K61 A126 N146 I                                      27810                                                                              C.sub.6 H.sub.13                                                                              C.sub.4 H.sub.9                                                                       K47 A133 N139 I                                      27811                                                                              C.sub.6 H.sub.13                                                                              C.sub.5 H.sub.11                                                                      K50 A148 N150 I                                      27812                                                                              C.sub.6 H.sub.13                                                                              C.sub.6 H.sub.13                                                                      K50 A145 I                                           27815                                                                              C.sub.9 H.sub.19O                                                                             C.sub.4 H.sub.9                                                                       K111                                                                               A166 N167 I                                      27816                                                                              C.sub.9 H.sub.19O                                                                             C.sub.6 H.sub.13                                                                      K108                                                                               C130 N169 I                                      27817                                                                              C.sub.10 H.sub.21O                                                                            C.sub.6 H.sub.13                                                                      K105                                                                               C122 N165 I                                      27818                                                                              C.sub.10 H.sub.21O                                                                            C.sub.7 H.sub.15                                                                      K87 C143 A169 I                                      27819                                                                              C.sub.12 H.sub.25O                                                                            C.sub.6 H.sub.13                                                                      K58 C136 A146 I                                      27820                                                                              C.sub.4 H.sub.9CMe.sub.2C.sub.4 H.sub.9O                                                      C.sub.6 H.sub.13                                                                      K93 C101 A111 N112 I                                 27821                                                                              C.sub.4 H.sub.9CMe.sub.2C.sub.6 H.sub.12O                                                     C.sub.6 H.sub.13                                                                      K90 C117 A129 N129 I                                 27823                                                                              C.sub.6 H.sub.13OCHMeCOO                                                                      C.sub.2 H.sub.5                                                                     1 K75 A61 I                                            27824                                                                              H.sub.2 C/CH.sub.2  CHC.sub.11 H.sub.22O                                                      C.sub.5 H.sub.11                                                                      K111                                                                               C113 A156 N157 I                                 __________________________________________________________________________      ##STR56##                                                                     No     L      R        Cr    LC                                                __________________________________________________________________________     28262  C.sub.6 H.sub.13                                                                      OC.sub.4 H.sub.9                                                                        K79.5 C155.1 N230.7 I                                   28263  C.sub.10 H.sub.21                                                                     OC.sub.10 H.sub.21                                                                      K80.3 C198.2 I                                          28265  C.sub.6 H.sub.13                                                                      OOCC.sub.6 H.sub.13                                                                     K82.3 C199.4 N225.2 I                                   __________________________________________________________________________

                  TABLE 24                                                         ______________________________________                                          ##STR57##                                                                     No     L           R           Cr    LC                                        ______________________________________                                         32163  H           OC.sub.9 H.sub.19                                                                          K105  S126 I                                    32165  C.sub.6 H.sub.13                                                                           OC.sub.4 H.sub.9                                                                           K68   S115 N165 I                               32166  C.sub.6 H.sub.13                                                                           OC.sub.9 H.sub.19                                                                          K83   S167 N177 I                               32167  C.sub.4 H.sub.9O                                                                           OC.sub.4 H.sub.9                                                                           K103  S117 N210 I                               32168  C.sub.4 H.sub.9O                                                                           OC.sub.9 H.sub.19                                                                          K105  S141 N195 I                               32170  C.sub.6 H.sub.13O                                                                          OC.sub.5 H.sub.11                                                                          K95   S145 N199 I                               ______________________________________                                          ##STR58##                                                                     No       L          R        Cr     LC                                         ______________________________________                                         32162    C.sub.5 H.sub.13                                                                          C.sub.4 H.sub.9                                                                         K56    C89 A123 I                                 ______________________________________                                          ##STR59##                                                                     No       L           R         Cr    LC                                        ______________________________________                                         27671    C.sub.6 H.sub.13                                                                           H         K82   S128 I                                    27672    C.sub.6 H.sub.13O                                                                          H         K95   S152 I                                    27673    C.sub.4 H.sub.9                                                                            C.sub.5 H.sub.11                                                                         K47   S143 I                                    ______________________________________                                    

                                      TABLE 25                                     __________________________________________________________________________      ##STR60##                                                                     No    L         R          Cr   LC                                             __________________________________________________________________________     8296  C.sub.6 H.sub.13                                                                         C.sub.8 H.sub.17                                                                          K50.9                                                                               A126.6 I                                       8297  C.sub.10 H.sub.21                                                                        C.sub.8 H.sub.17                                                                          K37.1                                                                               A128.7 I                                       8299  C.sub.8 H.sub.13CHF                                                                      C.sub.8 H.sub.17                                                                    1     K63.4                                                                               A132.9 I                                       __________________________________________________________________________      ##STR61##                                                                     No  L    R         Cr  LC                                                      __________________________________________________________________________     37286                                                                              C.sub.3 H.sub.7                                                                     C.sub.7 H.sub.15                                                                         K95.5                                                                              S88 G99.5 C118 A154 N174.5 I                            37287                                                                              C.sub.3 H.sub.7                                                                     C.sub.10 H.sub.21                                                                        K76.5                                                                              S94.5 S95.5 C120.9 A159.7 N164.4 I                      37288                                                                              C.sub.4 H.sub.9                                                                     C.sub.9 H.sub.19                                                                         K81 S87 S98 C102 A103 N164 I                                37289                                                                              C.sub.5 H.sub.11                                                                    C.sub.7 H.sub.15                                                                         K50 G101 C105 A173 N176 I                                   37290                                                                              C.sub.5 H.sub.11                                                                    C.sub.10 H.sub.21                                                                        K69.2                                                                              S98.4 S107.3 S119.9 S170.6 I                            37291                                                                              C.sub.6 H.sub.13                                                                    C.sub.7 H.sub.15                                                                         K52 G83 C126 A159 N166 I                                    37292                                                                              C.sub.7 H.sub.15                                                                    C.sub.7 H.sub.15                                                                         K50 G101 B133 A173 I                                        37293                                                                              C.sub.8 H.sub.17                                                                    C.sub.7 H.sub.15                                                                         K62 G94 B134 A172 I                                         37294                                                                              C.sub.5 H.sub.11                                                                    CHMeC.sub.2 H.sub.5                                                                    2 K55.1                                                                              S103.8 A114.7 N120.6 I                                  __________________________________________________________________________

                  TABLE 26                                                         ______________________________________                                          ##STR62##                                                                     No     L          R         Cr   LC                                            ______________________________________                                         36949  C.sub.3 H.sub.7O                                                                          C.sub.7 H.sub.15                                                                         K94  C136 A144 N153 I                              36950  C.sub.4 H.sub.9O                                                                          C.sub.7 H.sub.15                                                                         K68  C144 A147 N154 I                              36951  C.sub.4 H.sub.5O                                                                          C.sub.11 H.sub.23                                                                        K90  C145 A155 I                                   36952  C.sub.6 H.sub.13O                                                                         C.sub.7 H.sub.15                                                                         K68  C103 A171 I                                   ______________________________________                                          ##STR63##                                                                     No      L        R         Cr    LC                                            ______________________________________                                         37296   C.sub.2 H.sub.5                                                                         C.sub.9 H.sub.19                                                                         K76   G94 C117 A124 I                               37297   C.sub.3 H.sub.7                                                                         C.sub.9 H.sub.19                                                                         K83   G105 C112 A130 I                              37298   C.sub.4 H.sub.9                                                                         C.sub.9 H.sub.19                                                                         K72   G110 C119 A142 I                              ______________________________________                                          ##STR64##                                                                     No    L          R          Cr   LC                                            ______________________________________                                         26651 C.sub.8 H.sub.17O                                                                         OC.sub.8 H.sub.17                                                                         K?   G259 C339.5 N344 I                            26652 C.sub.12 H.sub.25O                                                                        OC.sub.12 H.sub.25                                                                        K?   H235 C308 I                                   26653 C.sub.16 H.sub.33O                                                                        OC.sub.16 H.sub.33                                                                        K?   H229 F272 C290 I                              ______________________________________                                    

                  TABLE 27                                                         ______________________________________                                          ##STR65##                                                                     No    L          R          Cr    LC                                           ______________________________________                                         26625 Cl         Cl         K298  C258 N313 I                                  26628 C.sub.4 H.sub.9                                                                           C.sub.4 H.sub.9                                                                           K145  C166 N244 I                                  26629 C.sub.6 H.sub.13                                                                          C.sub.6 H.sub.13                                                                          K142  E135 C194 N225 I                             26633 C.sub.4 H.sub.9O                                                                          OC.sub.4 H.sub.9                                                                          K197.7                                                                               C210.6 N294.2 I                              26634 C.sub.5 H.sub.11O                                                                         OC.sub.5 H.sub.11                                                                         K179.8                                                                               1224.1 C270.7 I                              26635 C.sub.6 H.sub.13O                                                                         OC.sub.6 H.sub.13                                                                         K167.4                                                                               1232.6 C262.7 I                              26636 C.sub.7 H.sub.15O                                                                         OC.sub.7 H.sub.15                                                                         K160.7                                                                               1236.1 C250.3 I                              26637 C.sub.8 H.sub.17O                                                                         OC.sub.8 H.sub.17                                                                         K153.1                                                                               1237.1 C244 I                                26638 C.sub.9 H.sub.19O                                                                         OC.sub.9 H.sub.19                                                                         K147.6                                                                               1233.7 I                                     26639 C.sub.10 H.sub.21O                                                                        OC.sub.10 H.sub.21                                                                        K140.6                                                                               1226.8 I                                     26640 C.sub.12 H.sub.25O                                                                        OC.sub.12 H.sub.25                                                                        K129  1221.1 I                                     ______________________________________                                          ##STR66##                                                                     No       L         R         Cr    LC                                          ______________________________________                                         43323    C.sub.4 H.sub.9                                                                          C.sub.4 H.sub.9                                                                          K319  S340 A? Z                                   ______________________________________                                    

                  TABLE 28                                                         ______________________________________                                          ##STR67##                                                                     No   L          R          Cr    LC                                            ______________________________________                                         3978 C.sub.6 H.sub.13O                                                                         SC.sub.5 H.sub.11                                                                         K24   A71.5 I                                       3979 C.sub.6 H.sub.13O                                                                         SC.sub.6 H.sub.13                                                                         K30   A74.5 I                                       3980 C.sub.6 H.sub.13O                                                                         SC.sub.7 H.sub.15                                                                         K39.5 A72.5 I                                       3981 C.sub.6 H.sub.13O                                                                         SC.sub.8 H.sub.17                                                                         K27   A73 I                                         3982 C.sub.6 H.sub.13O                                                                         SC.sub.9 H.sub.19                                                                         K42.5 A72 I                                         3983 C.sub.6 H.sub.13O                                                                         SC.sub.10 H.sub.21                                                                        K31.5 A71.5 I                                       3984 C.sub.7 H.sub.15O                                                                         SCH.sub.3  K62.5 A73 I                                         3985 C.sub.7 H.sub.15O                                                                         SC.sub.6 H.sub.13                                                                         K40   A74.5 I                                       3986 C.sub.7 H.sub.15O                                                                         SC.sub.7 H.sub.15                                                                         K41   C42 A73 I                                     3987 C.sub.7 H.sub.15O                                                                         SC.sub.10 H.sub.21                                                                        K53   A71 I                                         3988 C.sub.7 H.sub.15O                                                                         SC.sub.11 H.sub.23                                                                        K61   A69.5 I                                       3989 C.sub.8 H.sub.17O                                                                         SC.sub.6 H.sub.13                                                                         K47   A76 I                                         3990 C.sub.8 H.sub.17O                                                                         SC.sub.7 H.sub.15                                                                         K39   G34 C51 A75 I                                 3991 C.sub.8 H.sub.17O                                                                         SC.sub.8 H.sub.17                                                                         K51   G40 C55 A75 I                                 3992 C.sub.8 H.sub.17O                                                                         SC.sub.9 H.sub.19                                                                         K47.6 G40.5 C54.5 A74.1 I                           3993 C.sub.8 H.sub.17O                                                                         SC.sub.10 H.sub.21                                                                        K54.8 G42.2 C59.7 A74 I                             3994 C.sub.8 H.sub.17O                                                                         SC.sub.11 H.sub.23                                                                        K61.4 C53.4 A74.5 I                                 3995 C.sub.9 H.sub.19O                                                                         SCH.sub.3  K73   A77.5 I                                       3996 C.sub.9 H.sub.19O                                                                         SC.sub.6 H.sub.13                                                                         K48   A76 I                                         3997 C.sub.9 H.sub.19O                                                                         SC.sub.8 H.sub.17                                                                         K52   G38.1 C58 A75.8 I                             3998 C.sub.9 H.sub.19O                                                                         SC.sub.9 H.sub.19                                                                         K48.5 G38.5 C57 A74.8 I                             3999 C.sub.9 H.sub.19O                                                                         SC.sub.10 H.sub.21                                                                        K54.7 G42.2 C59.7 A73.9 I                           4000 C.sub.9 H.sub.19O                                                                         SC.sub.11 H.sub.23                                                                        K60   C54.7 A73.4 I                                 4001 C.sub.10 H.sub.21O                                                                        SC.sub.6 H.sub.13                                                                         K56   A76.5 I                                       4002 C.sub.10 H.sub.21O                                                                        SC.sub.9 H.sub.19                                                                         K58.8 G54 C69.3 A75.7 I                             4003 C.sub.10 H.sub.21O                                                                        SC.sub.10 H.sub.21                                                                        K62.1 G57.8 C71 A75 I                               4004 C.sub.10 H.sub.21O                                                                        OC.sub.11 H.sub.23                                                                        K62   558.6 C70.9 A74.8 I                           4005 C.sub.11 H.sub.23O                                                                        SC.sub.10 H.sub.21                                                                        K64.5 G61.8 C73.9 A75 I                             4006 C.sub.11 H.sub.23O                                                                        OC.sub.11 H.sub.23                                                                        K65   S63 C74.2 A74.7 I                             4016 C.sub.6 H.sub.13S                                                                         C.sub.6 H.sub.13                                                                          K50   A57.5 I                                       ______________________________________                                    

                                      TABLE 29                                     __________________________________________________________________________      ##STR68##                                                                     No L                R                     Cr  LC                               __________________________________________________________________________     4017                                                                              C.sub.4 H.sub.9S SC.sub.6 H.sub.13     K42.5                                                                              A42 I                            4018                                                                              C.sub.6 H.sub.13S                                                                               SC.sub.6 H.sub.13     K40 A48.5 I                          4019                                                                              CH.sub.3CMe.sub.2C.sub.5 H.sub.10O                                                              C.sub.8 H.sub.17      K73 C64 A71 W                        4020                                                                              CH.sub.3CMe.sub.2C.sub.5 H.sub.10O                                                              OC.sub.9 H.sub.19     K86 C80 A82 W                        4021                                                                              CH.sub.3CMe.sub.2C.sub.5 H.sub.10O                                                              SC.sub.10 H.sub.21    K60 C53 A55 W                        4023                                                                              C.sub.6 H.sub.13OC.sub.2 H.sub.4OC.sub.2 H.sub.4O                                               OC.sub.9 H.sub.19     K48 A44 I                            4028                                                                              C.sub.5 H.sub.11COO                                                                             C.sub.6 H.sub.13      K79 B85.5 A95 I                      4030                                                                              C.sub.10 H.sub.21O                                                                              OCH.sub.2CHMeC.sub.2 H.sub.5                                                                       S K63 A69 I                            4031                                                                              C.sub.8 H.sub.17 OC.sub.3 H.sub.6CHMeC.sub.2 H.sub.5                                                                1 K51.8                                                                              A55 I                            4032                                                                              C.sub.10 H.sub.21O                                                                              OC.sub.3 H.sub.6CHMeC.sub.2 H.sub.5                                                                1 K63 C*57.5 A82 I                     4033                                                                              C.sub.10 H.sub.21O                                                                              OC.sub.2 H.sub.4CHMeC.sub.3 H.sub.6CHMeCH.sub.3                                                    1 K45 C*37 A58 I                       4034                                                                              C.sub.8 H.sub.17 OC.sub.5 H.sub.10CHMeC.sub.2 H.sub.5                                                               1 K46 C*35 A60 I                       4035                                                                              C.sub.8 H.sub.17O                                                                               C.sub.5 H.sub.10CHMeC.sub.2 H.sub.5                                                                S K36 S46 C*55 A71 I                   4036                                                                              C.sub.10 H.sub.21O                                                                              OC.sub.5 H.sub.10CHMeC.sub.2 H.sub.5                                                               1 K77 C*76 A86 I                       4037                                                                              C.sub.8 H.sub.17O                                                                               SC.sub.5 H.sub.10CHMeC.sub.2 H.sub.5                                                               S K55.8                                                                              S24 C*55.6 A64.3 I               4041                                                                              C.sub.5 H.sub.11 SCF.sub.2H            K50.8                                                                              N-17 E                           4042                                                                              C.sub.10 H.sub.21O                                                                              OC.sub.9 H.sub.18CH/CH.sub.2  CH.sub.2                                                               K88 S70.6 C84 A87.6 I                4049                                                                              CH.sub.3CHMeCHFCOO                                                                              OC.sub.9 H.sub.18CH/CH.sub.2  CH.sub.2                                                             S K78 A64 I                            4051                                                                              C.sub.2 H.sub.5CHMeCH.sub.2O                                                                    C.sub.8 H.sub.17    1 K51 A66 I                            4053                                                                              C.sub.2 H.sub.5CMeCH.sub.2O                                                                     OC.sub.10 H.sub.21  1 K82 A63 I                            4055                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                             C.sub.12 H.sub.25   1 K46 A62 I                            4056                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                             SC.sub.8 H.sub.17   2 K24 C36 A49.8 I                      4058                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                            C.sub.8 H.sub.17    S K40.2                                                                              G*43.4 C*57.8 A72.3 I            4059                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                            C.sub.12 H.sub.25   1 K57.1                                                                              C*58 A68 I                       4060                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                            OC.sub.8 H.sub.17   1 K73 C*78 A86 I                       4061                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                            OC.sub.9 H.sub.19   S K77.7                                                                              C*79.2 A84.7 I                   4062                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                            SC.sub.6 H.sub.13   S K46 C*51.5 A63 I                     4063                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                            SC.sub.7 H.sub.15   S K44.6                                                                              C*52.5 A59.8 I                   4064                                                                              C.sub.2 H.sub.5CMMeC.sub.5 H.sub.10O                                                            SC.sub.8 H.sub.17   1 K43 C*55 A60 I                       4065                                                                              C.sub.2 H.sub.5CMMeC.sub.5 H.sub.10O                                                            SC.sub.9 H.sub.19   S K28.1                                                                              C*53.5 A60.5                     __________________________________________________________________________                                                   I                           

                                      TABLE 30                                     __________________________________________________________________________      ##STR69##                                                                     No  L             R       Cr   LC                                              __________________________________________________________________________     4178                                                                               Me.sub.3 SiC.sub.5 H.sub.10O                                                                 OC.sub.8 H.sub.17                                                                      K69  C88 A93 E                                       4179                                                                               Me.sub.3 SiC.sub.6 H.sub.12O                                                                 C.sub.8 H.sub.17                                                                       K25  C47 A56.6 I                                     4180                                                                               Me.sub.3 SiC.sub.10 H.sub.20O                                                                OC.sub.8 H.sub.17                                                                      K41  C84 A92 E                                       4181                                                                               Me.sub.3 SiC.sub.11 H.sub.22O                                                                C.sub.8 H.sub.17                                                                       K56.7                                                                               C63.8 I                                         4182                                                                               Me.sub.3 SiC.sub.11 H.sub.22O                                                                OC.sub.8 H.sub.17                                                                      K70  C92 E                                           4183                                                                               C.sub.4 H.sub.9 SiMe.sub.2C.sub.3 H.sub.6O                                                   OC.sub.8 H.sub.17                                                                      K45  C65 A68 E                                       4184                                                                               C.sub.4 H.sub.9 SiMe.sub.2C.sub.4 H.sub.8O                                                   C.sub.8 H.sub.17                                                                       K16.7                                                                               C22.3 A25.9 I                                   4185                                                                               C.sub.4 H.sub.9 SiMe.sub.2C.sub.4 H.sub.8O                                                   OC.sub.8 H.sub.17                                                                      K16.5                                                                               C63.1 A64 I                                     4186                                                                               C.sub.4 H.sub.9 SiMe.sub.2C.sub.5 H.sub.10O                                                  OC.sub.8 H.sub.17                                                                      K38  C74 A82 E                                       4187                                                                               C.sub.4 H.sub.9 SiMe.sub.2C.sub.6 H.sub.12O                                                  OC.sub.8 H.sub.17                                                                      K22  C72 A78.5 E                                     4188                                                                               EtMe.sub.2 SiC.sub.4 H.sub.8O                                                                C.sub.8 H.sub.17                                                                       K35.2                                                                               C30.6 A32.3 I                                   4189                                                                               EtMe.sub.2 SiC.sub.4 H.sub.8O                                                                OC.sub.8 H.sub.17                                                                      K49.4                                                                               C71 A71.3 I                                     4190                                                                               EtMe.sub.2 SiC.sub.6 H.sub.12O                                                               C.sub.8 H.sub.17                                                                       K22.6                                                                               C41.6 A50.4 I                                   4191                                                                               EtMe.sub.2 SiC.sub.6 H.sub.12O                                                               OC.sub.8 H.sub.17                                                                      K38.6                                                                               C78 A84 I                                       4192                                                                               EtMe.sub.2 SiC.sub.11 H.sub.22O                                                              C.sub.8 H.sub.17                                                                       K45.7                                                                               C58.6 A58.9 I                                   4211                                                                               C.sub.5 H.sub.11                                                                             CN      K94  A93.5 N109 I                                    4212                                                                               C.sub.6 H.sub.13                                                                             CN      K86.5                                                                               A101.5 N103 I                                   4213                                                                               C.sub.7 H.sub.15                                                                             CN      K96.5                                                                               A109 I                                          4214                                                                               C.sub.9 H.sub.19                                                                             CN      K90  A107 I                                          4219                                                                               C.sub.5 H.sub.11O                                                                            CN      K97  A102.5 N133 I                                   4220                                                                               C.sub.6 H.sub.13O                                                                            CN      K93.5                                                                               A121 N134 I                                     4221                                                                               C.sub.7 H.sub.15O                                                                            CN      K102.5                                                                              A127 N129.5 I                                   4222                                                                               C.sub.8 H.sub.17O                                                                            CN      K102 A133 I                                          4223                                                                               C.sub.9 H.sub.19O                                                                            CN      K?   X? I                                            __________________________________________________________________________

                                      TABLE 31                                     __________________________________________________________________________      ##STR70##                                                                     No  L        R           Cr  LC                                                __________________________________________________________________________     4229                                                                               C.sub.6 H.sub.13OCOO                                                                    CN          K83 A96 N121 I                                        4230                                                                               C.sub.8 H.sub.17O                                                                       OC.sub.6 H.sub.12SiMe.sub.3                                                                K38.7                                                                              C64.5 I                                           4231                                                                               C.sub.8 H.sub.17O                                                                       OC.sub.11 H.sub.22SiMe.sub.3                                                               K69.4                                                                              C92 I                                             4232                                                                               C.sub.12 H.sub.25O                                                                      OC.sub.11 H.sub.22SiMe.sub.3                                                               K81.6                                                                              C89.9 I                                           4233                                                                               C.sub.8 H.sub.17O                                                                       OC.sub.4 H.sub.8SiMe.sub.2 C.sub.4 H.sub.9                                                 K36.4                                                                              A30.6 N30.7 I                                     4234                                                                               C.sub.8 H.sub.17O                                                                       OC.sub.6 H.sub.12SiMe.sub.2 Et                                                             K28.7                                                                              C56 I                                             4235                                                                               C.sub.12 H.sub.25O                                                                      OC.sub.11 H.sub.22SiMe.sub.2 Et                                                            K75.4                                                                              C84.9 I                                           4236                                                                               C.sub.5 H.sub.11                                                                        C.sub.6 H.sub.13                                                                           K10 A26.5 I                                           4237                                                                               C.sub.5 H.sub.11                                                                        C.sub.7 H.sub.15                                                                           K30.6                                                                              S47.7 I                                           4239                                                                               C.sub.6 H.sub.13                                                                        C.sub.7 H.sub.15                                                                           K21.1                                                                              A47.3 I                                           4240                                                                               C.sub.6 H.sub.13                                                                        C.sub.8 H.sub.17                                                                           K20.5                                                                              A48.4 I                                           4241                                                                               C.sub.7 H.sub.15                                                                        C.sub.6 H.sub.13                                                                           K15 A29 I                                             4242                                                                               C.sub.7 H.sub.15                                                                        C.sub.8 H.sub.17                                                                           K23.4                                                                              A50.3 I                                           4243                                                                               C.sub.7 H.sub.15                                                                        C.sub.9 H.sub.19                                                                           K41.1                                                                              F24 A59.7 I                                       4244                                                                               C.sub.7 H.sub.15                                                                        C.sub.10 H.sub.21                                                                          K29.8                                                                              F33.8 C43.3 A60.6 I                               4245                                                                               C.sub.7 H.sub.15                                                                        C.sub.11 H.sub.23                                                                          K39.2                                                                              F48.4 C53.5 A64.7 I                               4246                                                                               C.sub.7 H.sub.15                                                                        C.sub.12 H.sub.25                                                                          K41.4                                                                              F53.8 C58 A65.2 I                                 4247                                                                               C.sub.7 H.sub.15                                                                        C.sub.14 H.sub.29                                                                          K38.5                                                                              F62.7 A67.2 I                                     4248                                                                               C.sub.8 H.sub.17                                                                        C.sub.6 H.sub.13                                                                           K18 A29.5 I                                           4249                                                                               C.sub.8 H.sub.17                                                                        C.sub.7 H.sub.15                                                                           K18.5                                                                              A48.1 I                                           4250                                                                               C.sub.8 H.sub.17                                                                        C.sub.8 H.sub.17                                                                           K31.5                                                                              A50.2 I                                           4251                                                                               C.sub.8 H.sub.17                                                                        C.sub.9 H.sub.19                                                                           K29 F24.6 A59.8 I                                     4252                                                                               C.sub.8 H.sub.17                                                                        C.sub.10 H.sub.21                                                                          K33.6                                                                              F36.7 C46.2 A59.8 I                               4253                                                                               C.sub.8 H.sub.17                                                                        C.sub.11 H.sub.23                                                                          K41 F50.8 C55.4 A64.2 I                               4254                                                                               C.sub.8 H.sub.17                                                                        C.sub.12 H.sub.25                                                                          K47.5                                                                              F55.6 C62.2 A64.2 I                               4255                                                                               C.sub.8 H.sub.17                                                                        C.sub.14 H.sub.29                                                                          K57.7                                                                              F64.5 C66.3 I                                     __________________________________________________________________________

                  TABLE 32                                                         ______________________________________                                          ##STR71##                                                                     No    L        R          Cr     LC                                            ______________________________________                                         4256  C.sub.8 H.sub.17                                                                        C.sub.16 H.sub.33                                                                         K56    F67 I                                         4257  C.sub.9 H.sub.19                                                                        C.sub.6 H.sub.13                                                                          K23.5  A30.5 N33 I                                   4258  C.sub.9 H.sub.19                                                                        C.sub.8 H.sub.17                                                                          K27.3  A51.2 I                                       4259  C.sub.9 H.sub.19                                                                        C.sub.10 H.sub.21                                                                         K32.5  F36.5 C44 A60.7 I                             4260  C.sub.9 H.sub.19                                                                        C.sub.12 H.sub.25                                                                         K41    F56.8 C63.2 A65.6 I                           4261  C.sub.10 H.sub.21                                                                       C.sub.6 H.sub.13                                                                          K31    A29.3 N31 I                                   4262  C.sub.10 H.sub.21                                                                       C.sub.8 H.sub.17                                                                          K35.5  A49.7 I                                       4263  C.sub.10 H.sub.21                                                                       C.sub.10 H.sub.21                                                                         K46.3  C45 A59.8 I                                   4264  C.sub.10 H.sub.21                                                                       C.sub.11 H.sub.23                                                                         K41.2  F52.6 C54.8 A64.6 I                           4265  C.sub.10 H.sub.21                                                                       C.sub.12 H.sub.25                                                                         K48.8  F58 C64 A65 I                                 4266  C.sub.12 H.sub.25                                                                       C.sub.8 H.sub.17                                                                          K46.8  A48.3 I                                       4267  C.sub.12 H.sub.25                                                                       C.sub.11 H.sub.23                                                                         K52.9  F52.2 A63.6 I                                 4268  C.sub.12 H.sub.25                                                                       C.sub.12 H.sub.25                                                                         K59.9  F59.7 C64 A64.7 I                             4269  C.sub.4 H.sub.9                                                                         OC.sub.6 H.sub.13                                                                         K42    A72 I                                         4271  C.sub.6 H.sub.13                                                                        OC.sub.4 H.sub.9                                                                          K40    A56.5 N60.5 I                                 4272  C.sub.6 H.sub.13                                                                        OC.sub.5 H.sub.11                                                                         K48    A62 I                                         4273  C.sub.6 H.sub.13                                                                        OC.sub.6 H.sub.13                                                                         K49    A77 I                                         4274  C.sub.6 H.sub.13                                                                        OC.sub.7 H.sub.15                                                                         K32.5  C50.6 A76.6 I                                 4275  C.sub.6 H.sub.13                                                                        OC.sub.8 H.sub.17                                                                         K29    C68 A85 I                                     4276  C.sub.6 H.sub.13                                                                        OC.sub.9 H.sub.19                                                                         K47.7  C77.2 A83.6 I                                 4277  C.sub.6 H.sub.13                                                                        OC.sub.10 H.sub.21                                                                        K38    S35 C82 A87 I                                 4278  C.sub.6 H.sub.13                                                                        OC.sub.11 H.sub.23                                                                        K38.8  S42.3 C84.3 A86.4 I                           4279  C.sub.6 H.sub.13                                                                        OC.sub.12 H.sub.25                                                                        K35    S47.4 C85.6 A87.1 I                           4280  C.sub.6 H.sub.13                                                                        OC.sub.14 H.sub.29                                                                        K34.4  S54.9 C85.2 A86.6 I                           4281  C.sub.6 H.sub.13                                                                        OC.sub.15 H.sub.31                                                                        K49.9  S56.7 C83.3 A85.2 I                           4283  C.sub.7 H.sub.15                                                                        OC.sub.5 H.sub.11                                                                         K46    A64 N66 I                                     4284  C.sub.7 H.sub.15                                                                        OC.sub.6 H.sub.13                                                                         K51    A78 I                                         4285  C.sub.7 H.sub.15                                                                        OC.sub.7 H.sub.15                                                                         K32.2  C45 A77.5 I                                   ______________________________________                                    

                                      TABLE 33                                     __________________________________________________________________________      ##STR72##                                                                     No   L         R       Cr    LC                                                __________________________________________________________________________     4286 C.sub.7 H.sub.15                                                                         OC.sub.8 H.sub.17                                                                      K32   C64 A87 I                                         4287 C.sub.7 H.sub.15                                                                         OC.sub.9 H.sub.19                                                                      K34.2 C76.3 A85.1 I                                     4288 C.sub.7 H.sub.15                                                                         OC.sub.10 H.sub.21                                                                     K32   S33 C83 A88 I                                     4289 C.sub.7 H.sub.15                                                                         OC.sub.11 H.sub.23                                                                     K38.7 S45.2 C86.8 A88.6 I                               4290 C.sub.7 H.sub.15                                                                         OC.sub.12 H.sub.25                                                                     K46   S54 C88 A89 I                                     4292 C.sub.8 H.sub.17                                                                         OC.sub.5 H.sub.11                                                                      K47   A61 I                                             4293 C.sub.8 H.sub.17                                                                         OC.sub.6 H.sub.13                                                                      K46   A76 I                                             4294 C.sub.8 H.sub.17                                                                         OC.sub.7 H.sub.15                                                                      K46.5 C39 A77.5 I                                       4295 C.sub.8 H.sub.17                                                                         OC.sub.8 H.sub.17                                                                      K39   C58 A84 I                                         4296 C.sub.8 H.sub.17                                                                         OC.sub.9 H.sub.19                                                                      K40.5 C76 A84.6 I                                       4297 C.sub.8 H.sub.17                                                                         OC.sub.10 H.sub.21                                                                     K42   C84 A88 I                                         4298 C.sub.8 H.sub.17                                                                         OC.sub.11 H.sub.23                                                                     K54.3 C87.2 I                                           4299 C.sub.8 H.sub.17                                                                         OC.sub.12 H.sub.25                                                                     K57   S58 C89 I                                         4300 C.sub.8 H.sub.17                                                                         OC.sub.14 H.sub.29                                                                     K59.8 S67.2 C88.3 I                                     4301 C.sub.8 H.sub.17                                                                         OC.sub.15 H.sub.31                                                                     K57.9 S69.6 C87.5 I                                     4303 C.sub.9 H.sub.19                                                                         OC.sub.5 H.sub.11                                                                      K49   A62 N63 I                                         4304 C.sub.9 H.sub.19                                                                         OC.sub.6 H.sub.13                                                                      K48   A77 I                                             4305 C.sub.9 H.sub.19                                                                         OC.sub.7 H.sub.15                                                                      K40   A78 I                                             4306 C.sub.9 H.sub.19                                                                         OC.sub.8 H.sub.17                                                                      K36   C53 A85 I                                         4307 C.sub.9 H.sub.19                                                                         OC.sub.9 H.sub.19                                                                      K39   C73.9 A84.9 I                                     4308 C.sub.9 H.sub.19                                                                         OC.sub.10 H.sub.21                                                                     K37   532 C83 A87 I                                     4309 C.sub.9 H.sub.19                                                                         OC.sub.11 H.sub.23                                                                     K45   S46 C87 I                                         4310 C.sub.9 H.sub.19                                                                         OC.sub.12 H.sub.25                                                                     K47   S59 C89 I                                         4311 C.sub.10 H.sub.21                                                                        OC.sub.9 H.sub.19                                                                      K46.6 C71.4 A83.8 I                                     4312 C.sub.10 H.sub.21                                                                        OC.sub.11 H.sub.23                                                                     K51.4 S47 C86.5 I                                       4326 C.sub.8 H.sub.17                                                                         OOCC.sub.7 H.sub.15                                                                    K79.4 A74.4 I                                           4334 C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                         OC.sub.8 H.sub.17                                                                      K8    C47 A69 I                                         4335 C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                         OOCC.sub.7 H.sub.15                                                                    K70                                                     __________________________________________________________________________

                                      TABLE 34                                     __________________________________________________________________________      ##STR73##                                                                     No  L             R        Cr  LC                                              __________________________________________________________________________     4336                                                                               C.sub.6 H.sub.13OC.sub. HMe                                                                  OC.sub.10 H.sub.21                                                                    1 K<-40                                                                              C*-40 A-23 I                                    4337                                                                               C.sub.2 H.sub.5OC.sub. HMeC.sub.5 H.sub.10                                                   OC.sub.6 H.sub.13                                                                     1 K-22                                                                               C*-21 A48 I                                     4338                                                                               C.sub.2 H.sub.5OC.sub. HMeC.sub.5 H.sub.10                                                   OC.sub.8 H.sub.17                                                                     1 K?  S8 C*49 A55 I                                   4339                                                                               C.sub.2 H.sub.5OC.sub. HMeC.sub.5 H.sub.10                                                   OC.sub.10 H.sub.21                                                                    1 K?  S10 C*55 I                                      4340                                                                               C.sub.2 H.sub.5OC.sub. HMeC.sub.5 H.sub.10                                                   OC.sub.11 H.sub.23                                                                    1 K27 C*56 I                                          4341                                                                               C.sub.2 H.sub.5C.sub. HMeC.sub.5 H.sub.10                                                    OC.sub.12 H.sub.25                                                                    1 K13 C*56 I                                          4342                                                                               C.sub.3 H.sub.7OC.sub. HMeC.sub.5 H.sub.10                                                   OC.sub.8 H.sub.17                                                                     1 K?  S-6 C*46 A52 I                                  4343                                                                               C.sub.5 H.sub.11OC.sub. HMeC.sub.5 H.sub.10                                                  OC.sub.8 H.sub.17                                                                     1 K?  S-4 C*37 A44 I                                  4346                                                                               C.sub. H.sub.3O                                                                              C.sub.9 H.sub.19                                                                        K40 S31 N41 I                                       4349                                                                               C.sub.2 H.sub.5O                                                                             C.sub.8 H.sub.17                                                                        K42.5                                                                              A43.5 N58.5 I                                   4353                                                                               C.sub.3 H.sub.7O                                                                             C.sub.7 H.sub.15                                                                        K42 A43.5 N52 I                                     4354                                                                               C.sub.3 H.sub.7O                                                                             C.sub.8 H.sub.17                                                                        K45 A49.5 I                                         4358                                                                               C.sub.4 H.sub.9O                                                                             C.sub.7 H.sub.15                                                                        K40.5                                                                              A42 N64 I                                       4359                                                                               C.sub.4 H.sub.9O                                                                             C.sub.8 H.sub.17                                                                        K35 A53.5 N60 I                                     4363                                                                               C.sub.5 H.sub.11O                                                                            C.sub.7 H.sub.15                                                                        K49 C48.5 A52 N66 I                                 4364                                                                               C.sub.5 H.sub.11O                                                                            C.sub.8 H.sub.17                                                                        K38 A54 N58 I                                       4365                                                                               C.sub.5 H.sub.11O                                                                            C.sub.9 H.sub.19                                                                        K41 A65.5 I                                         4366                                                                               C.sub.5 H.sub.11O                                                                            C.sub.10 H.sub.21                                                                       K47.5                                                                              A67 I                                           __________________________________________________________________________

                  TABLE 35                                                         ______________________________________                                          ##STR74##                                                                     No    L          R         Cr    LC                                            ______________________________________                                         4370  C.sub.6 H.sub.13O                                                                         C.sub.7 H.sub.15                                                                         K45.5 A33 N69.5 I                                   4371  C.sub.6 H.sub.13O                                                                         C.sub.8 H.sub.17                                                                         K27.5 C44.5 A57.5 N65 I                             4372  C.sub.6 H.sub.13O                                                                         C.sub.9 H.sub.19                                                                         K33.5 C49.5 A71 N71.5 I                             4373  C.sub.6 H.sub.13O                                                                         C.sub.10 H.sub.21                                                                        K32.5 C62 A74.5 I                                   4377  C.sub.7 H.sub.15O                                                                         C.sub.7 H.sub.15                                                                         K44   C44 A49 N68 I                                 4378  C.sub.7 H.sub.15O                                                                         C.sub.8 H.sub.17                                                                         K46   C49 A61 N66 I                                 4379  C.sub.7 H.sub.15O                                                                         C.sub.9 H.sub.19                                                                         K35   C51.5 A71.5 I                                 4380  C.sub.7 H.sub.15O                                                                         C.sub.10 H.sub.21                                                                        K46   C62.5 A72 I                                   4384  C.sub.8 H.sub.17O                                                                         C.sub.7 H.sub.15                                                                         K49   A44 N69.5 I                                   4385  C.sub.8 H.sub.17O                                                                         C.sub.8 H.sub.17                                                                         K35   C57 A64 N70 I                                 4386  C.sub.8 H.sub.17O                                                                         C.sub.9 H.sub.19                                                                         K33   C60 A74.5 I                                   4387  C.sub.8 H.sub.17O                                                                         C.sub.10 H.sub.21                                                                        K37   C68.5 A73.5 I                                 4391  C.sub.9 H.sub.19O                                                                         C.sub.7 H.sub.15                                                                         K48   C51 A57 N70 I                                 4392  C.sub.9 H.sub.19O                                                                         C.sub.8 H.sub.17                                                                         K33   C56 A65 N68.5 I                               4393  C.sub.9 H.sub.19O                                                                         C.sub.9 H.sub.19                                                                         K34   C61 A75 I                                     4394  C.sub.9 H.sub.19O                                                                         C.sub.11 H.sub.23                                                                        K45   C78 A80 I                                     4397  C.sub.10 H.sub.21O                                                                        C.sub.7 H.sub.15                                                                         K53   A54.5 N71.5 I                                 ______________________________________                                    

                                      TABLE 36                                     __________________________________________________________________________      ##STR75##                                                                     No L      R                Cr  LC                                              __________________________________________________________________________     4398                                                                              C.sub.10 H.sub.21O                                                                    C.sub.8 H.sub.17 K32 C59.5 A65.5 N69.5 I                             4399                                                                              C.sub.10 H.sub.21O                                                                    C.sub.10 H.sub.21                                                                               K41 C74 A77 I                                       4401                                                                              C.sub.11 H.sub.23O                                                                    C.sub.7 H.sub.15 K55 C54.5 A62.5 N70 I                               4402                                                                              C.sub.11 H.sub.23O                                                                    C.sub.8 H.sub.17 K44.5                                                                              C60 A67 N69 I                                   4405                                                                              C.sub.12 H.sub.25O                                                                    C.sub.7 H.sub.15 K59.5                                                                              C57.5 A63 N71 I                                 4406                                                                              C.sub.12 H.sub.25O                                                                    C.sub.8 H.sub.17 K42 C61.5 A68.5 N70 I                               4408                                                                              C.sub.10 H.sub.21O                                                                    C.sub.5 H.sub.10CHMeOC.sub.2 H.sub.5                                                          1 K43 C*13 N*27 I                                     4409                                                                              C.sub.3 H.sub.7O                                                                      OC.sub.7 H.sub.15                                                                               K68.6                                                                              C65 A78.7 N83.6 I                               4410                                                                              C.sub.3 H.sub.7O                                                                      OC.sub.8 H.sub.17                                                                               K49.8                                                                              C70.5 A88.2 N88.7 I                             4411                                                                              C.sub.3 H.sub.7O                                                                      OC.sub.9 H.sub.19                                                                               K43.7                                                                              C72 A89.4 I                                     4412                                                                              C.sub.3 H.sub.7O                                                                      OC.sub.10 H.sub.21                                                                              K45.6                                                                              C71 A92.6 I                                     4413                                                                              C.sub.3 H.sub.7O                                                                      OC.sub.11 H.sub.23                                                                              K41.9                                                                              C68 A93 I                                       4414                                                                              C.sub.3 H.sub.7O                                                                      OC.sub.12 H.sub.25                                                                              K43.4                                                                              C61.6 A94.1 I                                   4415                                                                              C.sub.4 H.sub.9O                                                                      OC.sub.7 H.sub.15                                                                               K53.4                                                                              C75.1 A82.4 N92.1 I                             4416                                                                              C.sub.4 H.sub.9O                                                                      OC.sub.8 H.sub.17                                                                               K54.4                                                                              C84 A94.7 N96.6 I                               4417                                                                              C.sub.4 H.sub.9O                                                                      OC.sub.9 H.sub.19                                                                               K44.4                                                                              C87.7 A96.6 I                                   4418                                                                              C.sub.4 H.sub.9O                                                                      OC.sub.10 H.sub.21                                                                              K41.8                                                                              C90 A99.4 I                                     4419                                                                              C.sub.4 H.sub.9O                                                                      OC.sub.11 H.sub.23                                                                              K42.3                                                                              C89 A99.8 I                                     4420                                                                              C.sub.4 H.sub.9O                                                                      OC.sub.12 H.sub.25                                                                              K41.8                                                                              C88.4 A101 I                                    4422                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.6 H.sub.13                                                                               K62 C65.9 A76.6 N92.7 I                             4423                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.7 H.sub.15                                                                               K54.4                                                                              C77.4 A84.2 N91.3 I                             4424                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.8 H.sub.17                                                                               K50.2                                                                              C85.9 A93.9 N94.8 I                             4425                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.9 H.sub.19                                                                               K66.7                                                                              C90 A95 I                                       4426                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.10 H.sub.21                                                                              K41.4                                                                              C93.9 A97.2 I                                   4427                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.11 H.sub.23                                                                              K51.4                                                                              C95.9 A98.2 I                                   4428                                                                              C.sub.5 H.sub.11O                                                                     OC.sub.12 H.sub.25                                                                              K41.7                                                                              C96.2 A98.6 I                                   __________________________________________________________________________

                  TABLE 37                                                         ______________________________________                                          ##STR76##                                                                     No   L          R          Cr    LC                                            ______________________________________                                         4429 C.sub.6 H.sub.13O                                                                         OC.sub.6 H.sub.13                                                                         K62   A68 N69 I                                     4430 C.sub.6 H.sub.13O                                                                         OC.sub.7 H.sub.15                                                                         K45.8 C80.6 A84.7 N94.9 I                           4431 C.sub.6 H.sub.13O                                                                         OC.sub.8 H.sub.17                                                                         K42.6 C89.8 A96.6 N98.7 I                           4432 C.sub.6 H.sub.13O                                                                         OC.sub.9 H.sub.19                                                                         K49.9 C94.4 A97.9 I                                 4433 C.sub.6 H.sub.13O                                                                         OC.sub.10 H.sub.21                                                                        K43.8 C98.7 A100.3 I                                4434 C.sub.6 H.sub.13O                                                                         OC.sub.11 H.sub.23                                                                        K55.4 C100.4 A101 I                                 4435 C.sub.6 H.sub.13O                                                                         OC.sub.12 H.sub.25                                                                        K52.2 C102.2 I                                      4436 C.sub.7 H.sub.15O                                                                         OC.sub.6 H.sub.13                                                                         K60.8 C68.2 A79.4 N94.6 I                           4437 C.sub.7 H.sub.15O                                                                         OC.sub.7 H.sub.15                                                                         K59.2 C79.9 A87.6 N93.6 I                           4438 C.sub.7 H.sub.15O                                                                         OC.sub.8 H.sub.17                                                                         K51.6 C87.2 A96.4 N97.1 I                           4439 C.sub.7 H.sub.15O                                                                         OC.sub.9 H.sub.19                                                                         K56   C94.9 A97.8 I                                 4440 C.sub.7 H.sub.15O                                                                         OC.sub.10 H.sub.21                                                                        K55.6 C99.6 A100.3 I                                4441 C.sub.7 H.sub.15O                                                                         OC.sub.11 H.sub.23                                                                        K67.4 C100.1 I                                      4442 C.sub.7 H.sub.15O                                                                         OC.sub.12 H.sub.25                                                                        K54.8 C100.3 I                                      4444 C.sub.8 H.sub.17O                                                                         OC.sub.6 H.sub.13                                                                         K59.3 C73 A80 N96.2 I                               4445 C.sub.8 H.sub.17O                                                                         OC.sub.7 H.sub.15                                                                         K53.4 C81.5 A88.3 N95.4 I                           4446 C.sub.8 H.sub.17O                                                                         OC.sub.8 H.sub.17                                                                         K51   C92.3 A99.5 N100.3 I                          4447 C.sub.8 H.sub.17O                                                                         OC.sub.9 H.sub.19                                                                         K48.2 C96.4 A99 I                                   4448 C.sub.8 H.sub.17O                                                                         OC.sub.10 H.sub.21                                                                        K51.7 C101.7 A102.1 I                               4449 C.sub.8 H.sub.17O                                                                         OC.sub.11 H.sub.23                                                                        K59.9 C101.7 I                                      4450 C.sub.8 H.sub.17O                                                                         OC.sub.12 H.sub.25                                                                        K57.1 C102.9 I                                      4451 C.sub.9 H.sub.19O                                                                         OC.sub.6 H.sub.13                                                                         K61.6 C68.9 A83.2 N93.7 I                           4452 C.sub.9 H.sub.19O                                                                         OC.sub.7 H.sub.15                                                                         K55.2 C78.7 A89.6 N93.6 I                           4453 C.sub.9 H.sub.19O                                                                         OC.sub.8 H.sub.17                                                                         K55.1 C87.5 A96.2 I                                 4454 C.sub.9 H.sub.19O                                                                         OC.sub.9 H.sub.19                                                                         K65   C97 A101 I                                    4455 C.sub.9 H.sub.19O                                                                         OC.sub.10 H.sub.21                                                                        K52.5 C101.1 I                                      4456 C.sub.9 H.sub.19O                                                                         OC.sub.11 H.sub.23                                                                        K62   C101 I                                        4457 C.sub.9 H.sub.19O                                                                         OC.sub.12 H.sub.25                                                                        K60.3 C100.3 I                                      4458 C.sub.10 H.sub.21O                                                                        OC.sub.6 H.sub.13                                                                         K62.3 C71.6 A83.8 N93.6 I                           ______________________________________                                    

                                      TABLE 38                                     __________________________________________________________________________      ##STR77##                                                                     No  L      R             Cr  LC                                                __________________________________________________________________________     4459                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.7 H.sub.15                                                                            K50.4                                                                              C79.7 A90.1 N93.6 I                               4460                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.8 H.sub.17                                                                            K50 C89 A99.6 I                                       4461                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.9 H.sub.19                                                                            K52.3                                                                              C96.2 A99 I                                       4462                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.10 H.sub.21                                                                           K52.7                                                                              C101.4 I                                          4463                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.11 H.sub.23                                                                           K62.9                                                                              C101.2 I                                          4464                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.12 H.sub.25                                                                           K65.4                                                                              C102.8 I                                          4465                                                                               C.sub.10 H.sub.21O                                                                    OC.sub.14 H.sub.29                                                                           K67 C103 I                                            4466                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.6 H.sub.13                                                                            K69.3                                                                              C69 A86.2 N91.8 I                                 4467                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.7 H.sub.15                                                                            K58.2                                                                              C77 A90.1 N91.9 I                                 4468                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.8 H.sub.17                                                                            K56 C84.9 A97.1 I                                     4469                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.9 H.sub.18                                                                            K56.2                                                                              C92.7 A96.1 I                                     4470                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.10 H.sub.21                                                                           K53.1                                                                              C100.6 I                                          4471                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.11 H.sub.23                                                                           K69.8                                                                              C99.8 I                                           4472                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.12 H.sub.25                                                                           K65.6                                                                              C101 I                                            4473                                                                               C.sub.11 H.sub.23O                                                                    OC.sub.16 H.sub.33                                                                           K71.3                                                                              S75.6 C100.9 I                                    4474                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.6 H.sub.13                                                                            K70.3                                                                              C70.7 A86.2 N91.4 I                               4475                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.7 H.sub.15                                                                            K57.1                                                                              C77.2 A89.4 N90.9 I                               4476                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.8 H.sub.17                                                                            K50 C86 A98 I                                         4477                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.9 H.sub.19                                                                            K53.8                                                                              C93.5 A96.9 I                                     4478                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.10 H.sub.21                                                                           K54.6                                                                              C100.3 I                                          4479                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.11 H.sub.23                                                                           K59.5                                                                              C100.7 I                                          4480                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.12 H.sub.25                                                                           K63.7                                                                              C104.3 I                                          4481                                                                               C.sub.12 H.sub.25O                                                                    OC.sub.16 H.sub.33                                                                           K71.2                                                                              S73.7 C99 I                                       4484                                                                               C.sub.8 H.sub.17O                                                                     OC.sub.4 H.sub.8CMe.sub.2C.sub.4 H.sub.9                                                     K54 C34 N37 I                                         4485                                                                               C.sub.8 H.sub.17O                                                                     OC.sub.6 H.sub.12CMe.sub.2C.sub.4 H.sub.9                                                    K43 C55 I                                             4498                                                                               C.sub.7 H.sub.15O                                                                     OOC.sub.C.sub.6 H.sub.13                                                                     K64.9                                                                              C66.2 N85.8 I                                     4499                                                                               C.sub.7 H.sub.15O                                                                     OOC.sub.C.sub.9 H.sub.19                                                                     K74.8                                                                              C96.5 I                                           4500                                                                               C.sub.7 H.sub.15O                                                                     OOC.sub.C.sub.13 H.sub.27                                                                    K81 S73 C101 I                                        4501                                                                               C.sub.8 H.sub.17O                                                                     OOC.sub.C.sub.6 H.sub.13                                                                     K63.4                                                                              C69.7 N89.7 I                                     4502                                                                               C.sub.8 H.sub.17O                                                                     OOC.sub.C.sub.7 H.sub.15                                                                     K75 C74.4 N91.3 I                                     __________________________________________________________________________

                                      TABLE 39                                     __________________________________________________________________________      ##STR78##                                                                     No L              R                Cr  LC                                      __________________________________________________________________________     4614                                                                              C.sub.7 H.sub.15COO                                                                           C.sub.7 H.sub.15 K54 A40 N57 I                               4615                                                                              C.sub.7 H.sub.15COO                                                                           C.sub.8 H.sub.17 K51 C52 A54 N56 I                           4616                                                                              C.sub.7 H.sub.15COO                                                                           C.sub.9 H.sub.19 K53 C64 A65 I                               4619                                                                              C.sub.8 H.sub.17COO                                                                           C.sub.8 H.sub.17 K49 C53.5 A54.8 N56.5 I                     4620                                                                              C.sub.8 H.sub.17COO                                                                           C.sub.10 H.sub.21                                                                               K53 S50 C70 I                               4623                                                                              C.sub.9 H.sub.19COO                                                                           C.sub.8 H.sub.17 K42 C55.5 N59.8 I                           4626                                                                              C.sub.10 H.sub.21COO                                                                          C.sub.8 H.sub.17 K57 C56.5 A56.7 N59 I                       4629                                                                              C.sub.11 H.sub.23COO                                                                          C.sub.8 H.sub.17 K56 C57.5 N60.8 I                           4630                                                                              C.sub.7 H.sub.15COO                                                                           OC.sub.8 H.sub.17                                                                               K73 C89 A92 N93 I                           4636                                                                              C.sub.4 H.sub.9CMe.sub.2CH.sub.2COO                                                           OC.sub.8 H.sub.17                                                                               K53 C49 N50 I                               4637                                                                              C.sub.6 H.sub.13CMe.sub.2CH.sub.2COO                                                          OC.sub.8 H.sub.17                                                                               K45 C42 N46 I                               4643                                                                              C.sub.5 H.sub.11OCOO                                                                          C.sub.12 H.sub.25                                                                               K48 A52                                     4645                                                                              C.sub.9 H.sub.19OCOO                                                                          C.sub.12 H.sub.25                                                                               K46 C59 I                                   4647                                                                              C.sub.12 H.sub.25OCOO                                                                         C.sub.12 H.sub.25                                                                               K57 C60 I                                   4661                                                                              C.sub.8 H.sub.17O                                                                             C.sub.3 H.sub.6C.sub. HMeC.sub.2 H.sub.5                                                      1 K33.5                                                                              N*19U                                   4662                                                                              C.sub.9 H.sub.19O                                                                             C.sub.3 H.sub.6C.sub. HMeC.sub.2 H.sub.5                                                      1 K35 N*20U                                   4663                                                                              C.sub.10 H.sub.21O                                                                            C.sub.3 H.sub.6C.sub. HMeC.sub.2 H.sub.5                                                      1 K38 N*21.5U                                 4664                                                                              C.sub.12 H.sub.25O                                                                            C.sub.3 H.sub.6C.sub. HMeC.sub.2 H.sub.5                                                      1 K43.5                                                                              N*40.5U                                 4665                                                                              C.sub.8 H.sub.17                                                                              OC.sub.5 H.sub.10C.sub. HMeC.sub.2 H.sub.5                                                    1 K-13                                                                               S10 S18 C*51 A51.4 I                    4666                                                                              C.sub.8 H.sub.17                                                                              OC.sub.5 H.sub.10C.sub. HMeC.sub.2 H.sub.5                                                    2 K16 C57.5 A59 I                             __________________________________________________________________________

                                      TABLE 40                                     __________________________________________________________________________      ##STR79##                                                                     No L        R                 Cr  LC                                           __________________________________________________________________________     4697                                                                              C.sub.8 H.sub.17O                                                                       OCH.sub.2CHFC.sub.8 H.sub.17                                                                   1 K62.5                                                                              C*92 A97 I                                   4698                                                                              C.sub.9 H.sub.19O                                                                       OCH.sub.2CHFC.sub.6 H.sub.13                                                                   1 K61 C*90.3 A96.2 I                               4699                                                                              C.sub.10 H.sub.21O                                                                      OCH.sub.2CHFC.sub.6 H.sub.13                                                                   1 K47 C*90 A97 I                                   4700                                                                              C.sub.12 H.sub.25O                                                                      OCH.sub.2CHFC.sub.6 H.sub.13                                                                   1 K66 C*89 A96 I                                   4701                                                                              C.sub.8 H.sub.17                                                                        C.sub.2 H.sub.4CHFC.sub.6 H.sub.13                                                             1 K31 C*25 A62 I                                   4702                                                                              C.sub.8 H.sub.17O                                                                       C.sub.2 H.sub.4CHFC.sub.6 H.sub.13                                                             S K74 A82 I                                        4703                                                                              C.sub.10 H.sub.21O                                                                      C.sub.2 H.sub.4CHFC.sub.6 H.sub.13                                                             1 K71 C*69 A82 I                                   4704                                                                              C.sub.10 H.sub.21O                                                                      C.sub.2 H.sub.4CHFC.sub.8 H.sub.17                                                             S K85 C*84 A86 I                                   4705                                                                              C.sub.12 H.sub.25O                                                                      C.sub.2 H.sub.4CHFC.sub.6 H.sub.13                                                             S K74 A82 I                                        4706                                                                              C.sub.10 H.sub.21O                                                                      OC.sub.2 H.sub.4CHFC.sub.6 H.sub.13                                                            1 K50 C*96 N*97 I                                  4707                                                                              C.sub.10 H.sub.21O                                                                      OC.sub.3 H.sub.6CHFC.sub.6 H.sub.13                                                            1 K61 C*102 A103 I                                 4715                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OOCCH.sub.CHC.sub.7 H.sub.15                                                                     K63 C61 N69 I                                    4716                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OOCCH.sub.CHC.sub.8 H.sub.17                                                                     K53 C62 A64 N68 I                                4717                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OOCCH.sub.CHC.sub.9 H.sub.19                                                                     K63 C73 I                                        4718                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CH.sub.CHC.sub.2 H.sub.5                                                                K57 A63 I                                        4719                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.3 H.sub.7                                                                     K67 A76 I                                        4720                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.4 H.sub.9                                                                     K62 C65 A71 I                                    4721                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.5 H.sub.11                                                                    K61 C76 A80 I                                    4722                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.6 H.sub.13                                                                    K74 C78 I                                        4723                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.7 H.sub.15                                                                    K65 C82 I                                        4724                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.8 H.sub.17                                                                    K73 C82 I                                        4725                                                                              C.sub.6 H.sub.13                                                                        OCH.sub.2CHCHC.sub.9 H.sub.19                                                                    K56 S72 C84 I                                    4726                                                                              C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.2 H.sub.5                                                                     K53 A66 I                                        4727                                                                              C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.3 H.sub.7                                                                     K69 A78 I                                        4728                                                                              C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.4 H.sub.9                                                                     K60 C61 A73 I                                    4729                                                                              C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.5 H.sub.11                                                                    K59 C75 A82 I                                    4730                                                                              C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.6 H.sub.13                                                                    K67 C80 I                                        __________________________________________________________________________

                                      TABLE 41                                     __________________________________________________________________________      ##STR80##                                                                     No  L        R               Cr  LC                                            __________________________________________________________________________     4731                                                                               C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.7 H.sub.15                                                                  K64 C86 I                                         4732                                                                               C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.8 H.sub.17                                                                  K72 C85 I                                         4733                                                                               C.sub.7 H.sub.15                                                                        OCH.sub.2CHCHC.sub.9 H.sub.19                                                                  K67 S74 C87 I                                     4734                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.2 H.sub.5                                                                   K53 A65 I                                         4735                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.3 H.sub.7                                                                   K68 A77 I                                         4736                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.4 H.sub.9                                                                   K57 A73 I                                         4737                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.5 H.sub.11                                                                  K56 C69.5 A81 I                                   4738                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.6 H.sub.13                                                                  K67 C79 I                                         4739                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.7 H.sub.15                                                                  K39 S62 C84 I                                     4740                                                                               C.sub.8 H.sub.17                                                                        CCH.sub.2CHCHC.sub.8 H.sub.17                                                                  K51 S67 C85 I                                     4741                                                                               C.sub.8 H.sub.17                                                                        OCH.sub.2CHCHC.sub.9 H.sub.19                                                                  K66 S74 C86 I                                     4742                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.2 H.sub.5                                                                   K57 A66 I                                         4743                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.3 H.sub.7                                                                   K70 A77 I                                         4744                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.4 H.sub.9                                                                   K57 C48 A73 I                                     4745                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.5 H.sub.11                                                                  K56 C65 A82 I                                     4746                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.6 H.sub.13                                                                  K62 C78 A80 I                                     4747                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.7 H.sub.15                                                                  K60 S58 C84 I                                     4748                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.8 H.sub.17                                                                  K50 S63 C86 I                                     4749                                                                               C.sub.9 H.sub.19                                                                        OCH.sub.2CHCHC.sub.9 H.sub.19                                                                  K61 S74 C87 I                                     4750                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.3 H.sub.7                                                                   K47 A56 I                                         4751                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.4 H.sub.9                                                                   K20 A41 I                                         4752                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.5 H.sub.11                                                                  K36 C58 A63 I                                     4753                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.6 H.sub.13                                                                  K51 C60 I                                         4754                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.7 H.sub.15                                                                  K44 C65 I                                         4755                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.8 H.sub.17                                                                  K50 S49 C68 I                                     4756                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                        OCH.sub.2CHCHC.sub.9 H.sub.19                                                                  K53 S59 C71 I                                     4760                                                                               C.sub.6 H.sub.13                                                                        OC.sub.3 H.sub.6CHCH.sub.2                                                                     K39 A69 I                                         4761                                                                               C.sub.6 H.sub.13                                                                        OC.sub.3 H.sub.6CHCHC.sub.3 H.sub.7                                                            K57 C68 A80 I                                     4762                                                                               C.sub.7 H.sub.15                                                                        OC.sub.3 H.sub.6CHCH.sub.2                                                                     K48 A72 I                                         __________________________________________________________________________

                                      TABLE 42                                     __________________________________________________________________________      ##STR81##                                                                     No  L         R              Cr LC                                             __________________________________________________________________________     4763                                                                               C.sub.7 H.sub.15                                                                         OC.sub.3 H.sub.6CHCHC.sub.3 H.sub.7                                                           K57                                                                               C66 A82 I                                      4764                                                                               C.sub.8 H.sub.17                                                                         OC.sub.3 H.sub.6CHCH.sub.2                                                                    K43                                                                               A69 I                                          4765                                                                               C.sub.8 H.sub.17                                                                         OC.sub.3 H.sub.6CHCHC.sub.3 H.sub.7                                                           K53                                                                               C55 A82 I                                      4766                                                                               C.sub.9 H.sub.19                                                                         OC.sub.3 H.sub.6CHCH.sub.2                                                                    K50                                                                               A70 I                                          4767                                                                               C.sub.9 H.sub.19                                                                         OC.sub.3 H.sub.6CHCHC.sub.3 H.sub.7                                                           K47                                                                               C52 A82 I                                      4769                                                                               C.sub.6 H.sub.13                                                                         OC.sub.4 H.sub.8CHCH.sub.2                                                                    K35                                                                               A64 I                                          4770                                                                               C.sub.7 H.sub.15                                                                         OC.sub.4 H.sub.8CHCH.sub.2                                                                    K37                                                                               A67 I                                          4771                                                                               C.sub.8 H.sub.17                                                                         OC.sub.4 H.sub.8CHCH.sub.2                                                                    K33                                                                               A64 I                                          4772                                                                               C.sub.9 H.sub.19                                                                         OC.sub.4 H.sub.8CHCH.sub.2                                                                    K33                                                                               A65 I                                          4774                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                         OC.sub.4 H.sub.8CHCH.sub.2                                                                    K18                                                                               A55 I                                          4776                                                                               C.sub.6 H.sub.13                                                                         OC.sub.5 H.sub.10CHCH.sub.2                                                                   K34                                                                               A79 I                                          4777                                                                               C.sub.6 H.sub.13                                                                         OC.sub.5 H.sub.10CHCHCH.sub.3                                                                 K45                                                                               C50 A85 I                                      4778                                                                               C.sub.7 H.sub.15                                                                         OC.sub.5 H.sub.10CHCH.sub.2                                                                   K35                                                                               A81 I                                          4779                                                                               C.sub.7 H.sub.15                                                                         OC.sub.5 H.sub.10CHCHCH.sub.3                                                                 K48                                                                               A87 I                                          4780                                                                               C.sub.8 H.sub.17                                                                         OC.sub.5 H.sub.10CHCH.sub.2                                                                   K37                                                                               A80 I                                          4781                                                                               C.sub.8 H.sub.17                                                                         OC.sub.5 H.sub.10CHCHCH.sub.3                                                                 K44                                                                               A85 I                                          4782                                                                               C.sub.9 H.sub.19                                                                         OC.sub.5 H.sub.10CHCH.sub.2                                                                   K38                                                                               A81 I                                          4783                                                                               C.sub.9 H.sub.19                                                                         OC.sub.5 H.sub.10CHCHCH.sub.3                                                                 K51                                                                               A86 I                                          4785                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                         OC.sub.5 H.sub.10CHCH.sub.2                                                                   K10                                                                               A59 I                                          4786                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                         OC.sub.5 H.sub.10CHCHCH.sub.3                                                                 K21                                                                               A70 I                                          4788                                                                               C.sub.6 H.sub.13                                                                         OC.sub.6 H.sub.12CHCH.sub.2                                                                   K26                                                                               C54 A75 I                                      4789                                                                               C.sub.7 H.sub.15                                                                         OC.sub.6 H.sub.12CHCH.sub.2                                                                   K24                                                                               C50 A78 I                                      4790                                                                               C.sub.8 H.sub.17                                                                         OC.sub.6 H.sub.12CHCH.sub.2                                                                   K42                                                                               C43 A76 I                                      4791                                                                               C.sub.9 H.sub.19                                                                         OC.sub.6 H.sub.12CHCH.sub.2                                                                   K34                                                                               C38 A77 I                                      4792                                                                               C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                         OC.sub.6 H.sub.12CHCH.sub.2                                                                   K15                                                                               C35 A60 I                                      4793                                                                               C.sub.6 H.sub.13                                                                         OC.sub.7 H.sub.14CHCH.sub.2                                                                   K20                                                                               C65 A81 I                                      4794                                                                               C.sub.7 H.sub.15                                                                         OC.sub.2 H.sub.14CHCH.sub.2                                                                   K16                                                                               S23 C62 A84 I                                  4795                                                                               C.sub.8 H.sub.17                                                                         OC.sub.7 H.sub.14CHCH.sub.2                                                                   K20                                                                               C60 A83 I                                      4796                                                                               C.sub.9 H.sub.19                                                                         OC.sub.7 H.sub.14CHCH.sub.2                                                                   K30                                                                               C53 A84 I                                      4797                                                                               C.sub.3 H.sub.7OC.sub.9 H.sub.10                                                         OC.sub.7 H.sub.14CHCH.sub.2                                                                   K-30                                                                              C30 A61 I                                      __________________________________________________________________________

                                      TABLE 43                                     __________________________________________________________________________      ##STR82##                                                                     No L          R                  Cr  LC                                        __________________________________________________________________________     4798                                                                              C.sub.6 H.sub.13                                                                          OC.sub.8 H.sub.16CHCH.sub.2                                                                       K33 S35 C73 A80 I                             4799                                                                              C.sub.7 H.sub.15                                                                          OC.sub.8 H.sub.16CHCH.sub.2                                                                       K32 S33 C72 A82 I                             4800                                                                              C.sub.8 H.sub.17                                                                          OC.sub.8 H.sub.16CHCH.sub.2                                                                       K36 C72 A81 I                                 4801                                                                              C.sub.9 H.sub.19                                                                          OC.sub.8 H.sub.16CHCH.sub.2                                                                       K35 C71 A82 I                                 4802                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                          OC.sub.8 H.sub.16CHCH.sub.2                                                                       K-3 C57 A64 I                                 4803                                                                              C.sub.6 H.sub.13                                                                          OC.sub.9 H.sub.18CHCH.sub.2                                                                       K29 S28 C76 A82 I                             4804                                                                              C.sub.6 H.sub.13                                                                          OC.sub.10 H.sub.20CHCH.sub.2                                                                      K33 S35 C76 A81 I                             4805                                                                              C.sub.7 H.sub.15                                                                          OC.sub.9 H.sub.18CHCH.sub.2                                                                       K28 S29 C77 A85 I                             4806                                                                              C.sub.7 H.sub.15                                                                          OC.sub.10 H.sub.20CHCH.sub.2                                                                      K38 S40 C79 A84 I                             4807                                                                              C.sub.8 H.sub.17                                                                          OC.sub.9 H.sub.18CHCH.sub.2                                                                       K38 C78 A84 I                                 4808                                                                              C.sub.8 H.sub.17                                                                          OC.sub.10 H.sub.20CHCH.sub.2                                                                      K43 C80 A82 I                                 4809                                                                              C.sub.9 H.sub.19                                                                          OC.sub.9 H.sub.18CHCH.sub.2                                                                       K38 C78 A85 I                                 4810                                                                              C.sub.9 H.sub.19                                                                          OC.sub.10 H.sub.20CHCH.sub.2                                                                      K43 C82 A83 I                                 4811                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                          OC.sub.9 H.sub.18CHCH.sub.2                                                                       K0  C55 A65 I                                 4812                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                          OC.sub.10 H.sub.20CHCH.sub.2                                                                      K19 S36 S59 C70 I                             4817                                                                              C.sub.8 H.sub.17                                                                          OC.sub.2 H.sub.4CH%CHC.sub.4 H.sub.9                                                              K52 A43 I                                     4818                                                                              C.sub.9 H.sub.19                                                                          OC.sub.2 H.sub.4CH%CHC.sub.4 H.sub.9                                                              K52 A44 I                                     4822                                                                              C.sub.6 H.sub.13                                                                          OC.sub.4 H.sub.8CH%CHC.sub.2 H.sub.5                                                              K45 C52 A55 I                                 4823                                                                              C.sub.7 H.sub.15                                                                          OC.sub.4 H.sub.8CH%CHC.sub.2 H.sub.5                                                              K42 C52 A55 I                                 4824                                                                              C.sub.8 H.sub.17                                                                          OC.sub.4 H.sub.8CH%CHC.sub.2 H.sub.5                                                              K38 C46 A57 I                                 4825                                                                              C.sub.9 H.sub.19                                                                          OC.sub.4 H.sub.8CH%CHC.sub.2 H.sub.5                                                              K38 C44 A58 I                                 4826                                                                              C.sub.3 H.sub.7OC.sub.5 H.sub.10                                                          OC.sub.4 H.sub.8CH%CHC.sub.2 H.sub.5                                                              K10 C33 A37 I                                 4828                                                                              C.sub.9 H.sub.19O                                                                         OC.sub.4 H.sub.8 OCH.sub.2CH/CH.sub.2  CH.sub.2                                                   K72.4                                                                              C58.4 N72 I                               4829                                                                              C.sub.6 H.sub.13O                                                                         OC.sub.4 H.sub.8CH/CH.sub.2  CH.sub.2                                                             K64 C48 N88 U                                 4830                                                                              C.sub.4 H.sub.9OC.sub.4 H.sub.8O                                                          OC.sub.4 H.sub.8CH/CH.sub.2  CH.sub.2                                                             K42 C45 A47 N64 I                             4831                                                                              C.sub.6 H.sub.13O                                                                         OC.sub.5 H.sub.10CH/CH.sub.2  CH.sub.2                                                            K53 C73 A75 N86 I                             4832                                                                              C.sub.4 H.sub.9OC.sub.4 H.sub.8O                                                          OC.sub.5 H.sub.10CH/CH.sub.2  CH.sub.2                                                            K39 C63 A65 N67 I                             4833                                                                              C.sub.8 H.sub.17O                                                                         OC.sub.6 H.sub.12CH/CH.sub.2  CH.sub.3                                                            K56 C78 A84 N89 I                             4834                                                                              C.sub.8 H.sub.19O                                                                         OC.sub.6 H.sub.12CH/CH.sub.2  CH.sub.2                                                            K56.5                                                                              C79 A85 N89.5 I                           __________________________________________________________________________

                                      TABLE 44                                     __________________________________________________________________________      ##STR83##                                                                     No L             R                 Cr  LC                                      __________________________________________________________________________     4835                                                                              C.sub.11 H.sub.23O                                                                           OC.sub.6 H.sub.12CH/CH.sub.2  CH.sub.2                                                           K57.5                                                                              C76.5 A86.7 N87 I                       4836                                                                              C.sub.12 H.sub.25O                                                                           OC.sub.6 H.sub.12CH/CH.sub.2  CH.sub.2                                                           K61 C>70 A87 I                              4837                                                                              C.sub.4 H.sub.9OC.sub.4 H.sub.8O                                                             OC.sub.6 H.sub.12CH/CH.sub.2  CH.sub.2                                                           K46 C66 A67 N69 I                           4838                                                                              C.sub.6 H.sub.13O                                                                            OC.sub.7 H.sub.14CH/CH.sub.2  CH.sub.2                                                           K51.8                                                                              C86.5 A89.6 N89.8 I                     4839                                                                              C.sub.9 H.sub.19O                                                                            OC.sub.7 H.sub.14CH/CH.sub.2  CH.sub.2                                                           K60 C87.9 A90.4 I                           4840                                                                              C.sub.10 H.sub.21O                                                                           OC.sub.7 H.sub.14CH/CH.sub.2  CH.sub.2                                                           K55.7                                                                              C90 A92.5 I                             4841                                                                              C.sub.11 H.sub.23O                                                                           OC.sub.7 H.sub.14CH/CH.sub.2  CH.sub.2                                                           K53.4                                                                              C87.6 A90.5 I                           4842                                                                              C.sub.12 H.sub.25O                                                                           OC.sub.7 H.sub.14CH/CH.sub.2  CH.sub.2                                                           K67.4                                                                              C86.1 A90.5 I                           4843                                                                              C.sub.4 H.sub.9OC.sub.4 H.sub.8O                                                             OC.sub.7 H.sub.14CH/CH.sub.2  CH.sub.2                                                           K43 C73 I                                   4844                                                                              C.sub.4 H.sub.9O                                                                             OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K55.4                                                                              C81 A87.8 I                             4845                                                                              C.sub.6 H.sub.13O                                                                            OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K54.1                                                                              C88.2 A90.8 I                           4846                                                                              C.sub.8 H.sub.17O                                                                            OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K56.4                                                                              C91.7 A92.9 I                           4847                                                                              C.sub.9 H.sub.19O                                                                            OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K56.2                                                                              C91.8 A93 I                             4848                                                                              C.sub.10 H.sub.21O                                                                           OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K58.5                                                                              C91.6 A92 I                             4849                                                                              C.sub.11 H.sub.23O                                                                           OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K53.6                                                                              C92.3 A93.1 I                           4850                                                                              C.sub.l2 H.sub.25 O                                                                          OC.sub.8 H.sub.16CH/CH.sub.2  CH.sub.2                                                           K54.9                                                                              C92.3 A93 I                             4851                                                                              C.sub.7 H.sub.15O                                                                            OC.sub.9 H.sub.18CH/CH.sub.2  CH.sub.2                                                           K64.7                                                                              C91 I                                   4852                                                                              C.sub.6 H.sub.17O                                                                            OC.sub.9 H.sub.18CH/CH.sub.2  CH.sub.2                                                           K63.7                                                                              C93.2 I                                 4853                                                                              C.sub.12 H.sub.25O                                                                           OC.sub.11 H.sub.22CH/CH.sub.2  CH.sub.2                                                          K64.6                                                                              C73.8 I                                 4854                                                                              C.sub.8 H.sub.17                                                                             OCH.sub.2CH/O CH(t)C.sub.3 H.sub.7                                                             1 K55 B90 A102 I                              4855                                                                              C.sub.8 H.sub.17                                                                             OCH.sub.2CH/O CH(t)C.sub.5 H.sub.11                                                            1 K70 F*101 A104 I                            4857                                                                              C.sub.2 H.sub.5CMe.sub.2C.sub.4 H.sub.8O                                                     OCH.sub.2CH/O CH(t)C.sub.4 H.sub.9                                                             1 K83 S87 A92 I                               4858                                                                              C.sub.2 H.sub.5CMe.sub.2C.sub.6 H.sub.12O                                                    OCH.sub.2CH/O CH(t)C.sub.4 H.sub.9                                                             1 K90 C*96 A106 I                             4859                                                                              C.sub.2 H.sub.5CHMeOCH.sub.2                                                                 C.sub.10 H.sub.21                                                                              1 K15.6                                                                              S15.2 I                                 4861                                                                              C.sub.6 H.sub.13CHMeOCH.sub.2                                                                C.sub.10 H.sub.21                                                                              2 K16.9                                                                              A-8.5 I                                 4869                                                                              C.sub.2 H.sub.5CHMeCOO                                                                       C.sub.11 H.sub.23                                                                              S K52.2                                                                              S40.7 I                                 4871                                                                              C.sub.2 H.sub.5CHMeCOO                                                                       OC.sub.8 H.sub.17                                                                              S K66 C*62.2 I                                4872                                                                              C.sub.2 H.sub.5CHMeCOO                                                                       OC.sub.11 H.sub.23                                                                             S K43 C*64.1 S67.2 I                          4873                                                                              CH.sub.3CHMeCHClCOO                                                                          C.sub.7 H.sub.15                                                                               S K64 X-10 I                                  4875                                                                              C.sub.2 H.sub.5CHMeCHClCOO                                                                   C.sub.7 H.sub.15                                                                               3 K59 X-20 I                                  __________________________________________________________________________

                                      TABLE 45                                     __________________________________________________________________________      ##STR84##                                                                     No L                    R        Cr  LC                                        __________________________________________________________________________     4919                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                                 C.sub.8 H.sub.17                                                                      S K31.2                                                                              B16.8 C*46.8 A50.8 I                      4920                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                                 C.sub.9 H.sub.19                                                                      S K23 S28 C*30 A51.5 N*52 I                     4921                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                                 C.sub.10 H.sub.21                                                                     S K33 S38.5 C*58 I                              4922                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                                 C.sub.11 H.sub.23                                                                     S K35.9                                                                              C*60 I                                    4923                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                                 C.sub.12 H.sub.25                                                                     S K41 S23.8 C*62.2 I                            4924                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                                 C.sub.14 H.sub.29                                                                     S K32 B45 C*59.8 I                              4925                                                                              C.sub.3 H.sub.7CHMeC.sub.3 H.sub.6O                                                                 C.sub.9 H.sub.19                                                                      2 K15.5                                                                              C44.5 A54.5 I                             4926                                                                              C.sub.5 H.sub.11CHMeC.sub.3 H.sub.6O                                                                C.sub.8 H.sub.17                                                                      2 K15 C9 A42.5 I                                4927                                                                              C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6CHMeCH.sub.2O                                                     C.sub.8 H.sub.17                                                                      7 K37 A34 I                                     4928                                                                              CH.sub.3CHMeC.sub.3 H.sub.5CHMeC.sub.2 H.sub.4O                                                     C.sub.9 H.sub.19                                                                      S K27 A40 I                                     4931                                                                              CH.sub.3CHMeC.sub.3 H.sub.5CHMeCH.sub.2COO                                                          C.sub.9 H.sub.19                                                                      S K44 C*<7 I                                    4932                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.6 H.sub.13                                                                      S K-5 A27 N*42 I                                4933                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.7 H.sub.15                                                                      S K-6 A46.3 N*49 I                              4934                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.8 H.sub.17                                                                      S K12 C*34.7 A49.5 I                            4935                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.9 H.sub.19                                                                      S K10 C*46 A59 I                                4936                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.10 H.sub.21                                                                     S K17 C*53.8 A63 I                              4937                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.11 H.sub.23                                                                     S K20 C*59 I                                    4938                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                                 C.sub.12 H.sub.25                                                                     S K23 S16 C*61.5 I                              4939                                                                              C.sub.3 H.sub.7CHMeC.sub.4 H.sub.8O                                                                 C.sub.8 H.sub.17                                                                      2 K3.5                                                                               S31.5 A47.5 I                             4940                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8CO                                                                C.sub.8 H.sub.17                                                                      S K67 C*69 A79.3 I                              4941                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8COO                                                               C.sub.8 H.sub.17                                                                      S K38.5                                                                              S24 C*44.8 I                              4942                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8COO                                                               C.sub.11 H.sub.23                                                                     S K62.3                                                                              S46.5 C*60 I                              4943                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8COO                                                               C.sub.14 H.sub.29                                                                     S K46 S50 C*62.8 I                              4944                                                                              C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8COO                                                               OC.sub.8 H.sub.17                                                                     S K76 C*79.5 I                                  4945                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                                C.sub.6 H.sub.13                                                                      S K12 C*23.8 N*45.6 I                           4946                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                                C.sub.7 H.sub.15                                                                      S K10 S16 C*39 A54 N*61 I                       4947                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                                C.sub.8 H.sub.17                                                                      S K3  B14.2 C*48.6 A56.3 I                      4948                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                                C.sub.9 H.sub.19                                                                      S K16 C*49.1 A61 I                              4949                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                                C.sub.10 H.sub.21                                                                     S K41 S<? C*61 I                                4950                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                                C.sub.11 H.sub.23                                                                     S K?  B36.7 C*68 I                              __________________________________________________________________________

                                      TABLE 46                                     __________________________________________________________________________      ##STR85##                                                                     No L            R         Cr  LC                                               __________________________________________________________________________     4951                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                        C.sub.12 H.sub.25                                                                      S K40.5                                                                              C*70 I                                           4952                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                        C.sub.14 H.sub.29                                                                      S K43 B45 C*66 I                                       4953                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                        C.sub.8 H.sub.17                                                                       2 K3  C47.5 A58 I                                      4954                                                                              C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                        OC.sub.8 H.sub.17                                                                      S K40.7                                                                              C*82.8 A89.1 I                                   4955                                                                              C.sub.2 H.sub.0CHMeC.sub.5 H.sub.10O                                                        COOC.sub.8 H.sub.17                                                                    S K76.5                                                                              C*79.7 I                                         4956                                                                              CH.sub.3CHMeC.sub.6 H.sub.12                                                                C.sub.9 H.sub.19                                                                         K29.5                                                                              F31 A58.2 I                                      4957                                                                              CH.sub.3CHMeC.sub.5 H.sub.12                                                                C.sub.10 H.sub.21                                                                        K38.6                                                                              F41.3 C51.4 A58.4 I                              4962                                                                              C.sub.2 H.sub.5CHFCOO                                                                       C.sub.9 H.sub.19                                                                       1 K70 S58 I                                            4964                                                                              C.sub.2 H.sub.5CHFCOO                                                                       C.sub.12 H.sub.25                                                                      1 K69 A59 I                                            4965                                                                              C.sub.4 H.sub.9CHFCOO                                                                       C.sub.10 H.sub.21                                                                      S K46 S30 A49 I                                        4966                                                                              C.sub.4 H.sub.9CHFCOO                                                                       C.sub.12 H.sub.25                                                                      S K59 C*45 A52 I                                       4968                                                                              C.sub.5 H.sub.11CHFCOO                                                                      C.sub.12 H.sub.25                                                                      S K14 S? A50 I                                         4969                                                                              C.sub.6 H.sub.13CHFCOO                                                                      C.sub.8 H.sub.17                                                                       1 K56 A38 I                                            4970                                                                              C.sub.6 H.sub.13CHFCOO                                                                      C.sub.9 H.sub.19                                                                       1 K53 A46 I                                            4971                                                                              C.sub.6 H.sub.13CHFCOO                                                                      C.sub.10 H.sub.21                                                                      1 K57 S32 C*45 I                                       4972                                                                              C.sub.6 H.sub.13CHFCOO                                                                      C.sub.12 H.sub.25                                                                      1 K62 C*52 I                                           4973                                                                              C.sub.7 H.sub.15CHFCOO                                                                      C.sub.10 H.sub.21                                                                      S K59 A46 I                                            4974                                                                              C.sub.7 H.sub.15CHFCOO                                                                      C.sub.12 H.sub.25                                                                      S K22 S? A61 I                                         4976                                                                              C.sub.8 H.sub.17CHFCOO                                                                      C.sub.9 H.sub.19                                                                       1 K64 A46 I                                            4977                                                                              C.sub.8 H.sub.17CHFCOO                                                                      C.sub.10 H.sub.21                                                                      1 K59 C*43 A46 N*48 I                                  4978                                                                              C.sub.8 H.sub.17CHFCOO                                                                      C.sub.12 H.sub.25                                                                      S K23 S87 I                                            4979                                                                              C.sub.4 H.sub.9CHFCH.sub.2O                                                                 C.sub.10 H.sub.21                                                                      S K48 C*43 A66 I                                       4980                                                                              C.sub.4 H.sub.9CHFCH.sub.2O                                                                 C.sub.12 H.sub.25                                                                      S K59 S37 S39 C*43 A71 I                               4981                                                                              C.sub.5 H.sub.11CHFCH.sub.2O                                                                C.sub.8 H.sub.17                                                                       S K24 A35 I                                            4982                                                                              C.sub.5 H.sub.11CHFCH.sub.2O                                                                C.sub.10 H.sub.21                                                                      S K49 C*60 A66 I                                       4983                                                                              C.sub.5 H.sub.11CHFCH.sub.2O                                                                C.sub.12 H.sub.25                                                                      S K60 S49 C*61 A72 I                                   4984                                                                              C.sub.6 H.sub.13CHFCH.sub.2O                                                                C.sub.8 H.sub.17                                                                       S K62 A59 I                                            4985                                                                              C.sub.6 H.sub.13CHFCH.sub.2O                                                                C.sub.9 H.sub.19                                                                       S K63 A67 I                                            4986                                                                              C.sub.6 H.sub.13CHFCH.sub.2O                                                                C.sub.10 H.sub.21                                                                      S K61 S49 C*62 A71 I                                   4987                                                                              C.sub.6 H.sub.13CHFCH.sub.2O                                                                C.sub.12 H.sub.25                                                                      S K56 C*70 A74 I                                       __________________________________________________________________________

                                      TABLE 47                                     __________________________________________________________________________      ##STR86##                                                                     No  L              R     Cr     LC                                             __________________________________________________________________________     5039                                                                               CF.sub.3O      C.sub.3 H.sub.7                                                                        K43.1                                                                               S48.2 N-17 E                                   5040                                                                               CF.sub.3O      C.sub.5 H.sub.11                                                                       K32  A45.2 N- 6                                     5041                                                                               CF.sub.3O      C.sub.7 H.sub.15                                                                       K25  A34 N-20 E                                     5042                                                                               C.sub.9 F.sub.19O                                                                             C.sub.8 H.sub.17                                                                       K65.1                                                                               A115.1 I                                       5043                                                                               C.sub.3 F.sub.7CH.sub.2O                                                                      C.sub.10 H.sub.21                                                                      K36  C52 A64 I                                      5044                                                                               C.sub.5 F.sub.11CH.sub.2O                                                                     C.sub.10 H.sub.21                                                                      K47  C73 A84 I                                      5045                                                                               C.sub.6 F.sub.13CH.sub.2O                                                                     C.sub.7 H.sub.15                                                                       K?   C? A? I                                        5046                                                                               C.sub.7 F.sub.15CH.sub.2O                                                                     C.sub.6 H.sub.13                                                                       K50  C56 A133 I                                     5047                                                                               C.sub.7 F.sub.15CH.sub.2O                                                                     C.sub.7 H.sub.15                                                                       K54  C67 A125 I                                     5048                                                                               C.sub.7 F.sub.15CH.sub.2O                                                                     C.sub.8 H.sub.17                                                                       K71  C80 A117 I                                     5049                                                                               C.sub.7 F.sub.15CH.sub.2O                                                                     C.sub.9 H.sub.19                                                                       K71  C85 A112 I                                     5050                                                                               C.sub.7 F.sub.15CH.sub.2O                                                                     C.sub.10 H.sub.21                                                                      K75  C87 A104 I                                     5051                                                                               C.sub.8 F.sub.17CH.sub.2O                                                                     C.sub.7 H.sub.15                                                                       K?   C? A? I                                        5052                                                                               C.sub.9 F.sub.19CH.sub.2O                                                                     C.sub.7 H.sub.15                                                                       K?   C? A? I                                        5053                                                                               C.sub.10 F.sub.21CH.sub.2O                                                                    C.sub.3 H.sub.7                                                                        K?   C? A? I                                        5054                                                                               C.sub.10 F.sub.21CH.sub.2O                                                                    C.sub.5 H.sub.11                                                                       K?   C? A? I                                        5055                                                                               C.sub.6 F.sub.13C.sub.3 H.sub.6O                                                              C.sub.8 H.sub.17                                                                       K63  C95 A132 I                                     5056                                                                               C.sub.4 F.sub.9C.sub.4 H.sub.8O                                                               C.sub.8 H.sub.17                                                                       K66  A114 I                                         5057                                                                               C.sub.4 F.sub.9C.sub.4 H.sub.8O                                                               C.sub.10 H.sub.21                                                                      K58  C80 A106 I                                     5061                                                                               HCF.sub.2O     C.sub.3 H.sub.7                                                                        K41  NO E                                           5062                                                                               HCF.sub.2O     C.sub.5 H.sub.11                                                                       K21  A26 NO E                                       5063                                                                               HCF.sub.2O     C.sub.7 H.sub.15                                                                       K26  A32 NO E                                       5064                                                                               HCF.sub.2O     C.sub.8 H.sub.17                                                                       K26.3                                                                               S31.6 N-3 E                                    5065                                                                               HC.sub.2 F.sub.4O                                                                             C.sub.7 H.sub.15                                                                       K46  X43 I                                          5066                                                                               HCF.sub.2S     C.sub.3 H.sub.7                                                                        K53.2                                                                               N-16 E                                         5067                                                                               HCF.sub.2S     C.sub.5 H.sub.11                                                                       K43.1                                                                               N-6 E                                          5068                                                                               C.sub.6 H.sub.13CHCF.sub.3OCH.sub.2                                                           C.sub.10 H.sub.21                                                                    1 K56.8                                                                               S18.4 I                                        5070                                                                               C.sub.4 H.sub.9CHCF.sub.3CH.sub.2COO                                                          C.sub.10 H.sub.21                                                                    1 K28  S1 S7 I                                        5072                                                                               H.sub.2 CCHCOOC.sub.6 H.sub.12O                                                               C.sub.8 H.sub.17                                                                       K50  S52.5 N53 I                                    __________________________________________________________________________

                                      TABLE 48                                     __________________________________________________________________________      ##STR87##                                                                     No  L              R    Cr  LC                                                 __________________________________________________________________________     5106                                                                               CH.sub.3 CHCHCH.sub.2 O                                                                       C.sub.9 H.sub.19                                                                    K59 A65 N75                                                                               I                                           5107                                                                               C.sub.2 H.sub.5 CHCHCH.sub.2 O                                                                C.sub.7 H.sub.15                                                                    K31 C30 N62                                                                               I                                           5108                                                                               C.sub.2 H.sub.5 CHCHCH.sub.2 O                                                                C.sub.8 H.sub.17                                                                    K53 C49 A55 N61                                                                           I                                           5109                                                                               C.sub.2 H.sub.5 CHCHCH.sub.2 O                                                                C.sub.9 H.sub.19                                                                    K56 C42 A68                                                                               I                                           5111                                                                               C.sub.3 H.sub.7 CHCHCH.sub.2 O                                                                C.sub.9 H.sub.17                                                                    K43 C51 N66                                                                               I                                           5112                                                                               C.sub.3 H.sub.7 CHCHCH.sub.2 O                                                                C.sub.8 H.sub.19                                                                    K49 C63 A70 N72                                                                           I                                           5113                                                                               C.sub.3 H.sub.7 CHCHCH.sub.2 O                                                                C.sub.10 H.sub.21                                                                   K30 C53 A65.5                                                                             I                                           5114                                                                               C.sub.4 H.sub.9 CHCHCH.sub.2 O                                                                C.sub.7 H.sub.15                                                                    K22 C33 N63                                                                               I                                           5115                                                                               C.sub.4 H.sub.9 CHCHCH.sub.2 O                                                                C.sub.8 H.sub.17                                                                    K30 C55 N64                                                                               I                                           5116                                                                               C.sub.4 H.sub.9 CHCHCH.sub.2 O                                                                C.sub.9 H.sub.19                                                                    K46 C66 A70                                                                               I                                           5117                                                                               C.sub.5 H.sub.11 CHCHCH.sub.2 O                                                               C.sub.7 H.sub.15                                                                    K38 C35 N68                                                                               I                                           5118                                                                               C.sub.5 H.sub.11 CHCHCH.sub.2 O                                                               C.sub.8 H.sub.17                                                                    K24 C56 N68                                                                               I                                           5119                                                                               C.sub.5 H.sub.11 CHCHCH.sub.2 O                                                               C.sub.9 H.sub.19                                                                    K42 C70 A72 N73                                                                           I                                           5120                                                                               C.sub.6 H.sub.13 CHCHCH.sub.2 O                                                               C.sub.7 H.sub.15                                                                    K40 C41 N66                                                                               I                                           5121                                                                               C.sub.6 H.sub.13 CHCHCH.sub.2 O                                                               C.sub.8 H.sub.17                                                                    K29 C58 N66                                                                               I                                           5122                                                                               C.sub.6 H.sub.13 CHCHCH.sub.2 O                                                               C.sub.9 H.sub.19                                                                    K20 C70 A71 N72                                                                           I                                           5123                                                                               C.sub.7 H.sub.15 CHCHCH.sub.2 O                                                               C.sub.7 H.sub.15                                                                    K49 C42 N68                                                                               I                                           5124                                                                               C.sub.7 H.sub.15 CHCHCH.sub.2 O                                                               C.sub.8 H.sub.17                                                                    K31 C59 N68                                                                               I                                           5125                                                                               C.sub.7 H.sub.15 CHCHCH.sub.2 O                                                               C.sub.9 H.sub.19                                                                    K37 C72 A73 N74                                                                           I                                           5126                                                                               C.sub.8 H.sub.17 CHCHCH.sub.2 O                                                               C.sub.7 H.sub.15                                                                    K43 C47 N66                                                                               I                                           5127                                                                               C.sub.8 H.sub.17 CHCHCH.sub.2 O                                                               C.sub.8 H.sub.17                                                                    K40 C60 N66                                                                               I                                           5128                                                                               C.sub.8 H.sub.17 CHCHCH.sub.2 O                                                               C.sub.9 H.sub.19                                                                    K36 C72 A73                                                                               I                                           5129                                                                               C.sub.9 H.sub.19 CHCHCH.sub.2 O                                                               C.sub.7 H.sub.15                                                                    K55 C49 N68                                                                               I                                           5130                                                                               C.sub.9 H.sub.19 CHCHCH.sub.2 O                                                               C.sub.8 H.sub.17                                                                    K44 C62 N68                                                                               I                                           5131                                                                               C.sub.9 H.sub.19 CHCHCH.sub.2 O                                                               C.sub.9 H.sub.19                                                                    K42 C74    I                                           5132                                                                               H.sub.2 CCHC.sub.2 H.sub.4 O                                                                  C.sub.4 H.sub.9                                                                     K37.3                                                                              N12.5  U                                           5133                                                                               H.sub.2 CCHC.sub.2 H.sub.4 O                                                                  C.sub.7 H.sub.15                                                                    K38 A41 N49                                                                               I                                           5134                                                                               H.sub.2 CCHC.sub.2 H.sub.4 O                                                                  C.sub.8 H.sub.17                                                                    K34 A46    I                                           5135                                                                               H.sub.2 CCHC.sub.2 H.sub.4 O                                                                  C.sub.9 H.sub.19                                                                    K55 A56    I                                           __________________________________________________________________________

                                      TABLE 49                                     __________________________________________________________________________      ##STR88##                                                                     No  L               R             Cr  LC                                       __________________________________________________________________________     5139                                                                               C.sub.3 H.sub.7 CHCHC.sub.2 H.sub.4 COO                                                        C.sub.8 H.sub.17                                                                             K54 A45 N50                                                                               I                                 5140                                                                               C.sub.3 H.sub.7 CHCHC.sub.2 H.sub.4 COO                                                        C.sub.9 H.sub.19                                                                             K67 A61    I                                 5142                                                                               H.sub.2 CCHC.sub.3 H.sub.6 O                                                                   C.sub.7 H.sub.15                                                                             K46 A45 N63                                                                               I                                 5143                                                                               H.sub.2 CCHC.sub.3 H.sub.6 O                                                                   C.sub.8 H.sub.17                                                                             K38 A54 N58                                                                               I                                 5144                                                                               H.sub.2 CCHC.sub.3 H.sub.6 O                                                                   C.sub.9 H.sub.19                                                                             K40 A65    I                                 5145                                                                               CH.sub.3 CHCHC.sub.3 H.sub.6 O                                                                 C.sub.9 H.sub.19                                                                             K48 C35 A70 N72                                                                           I                                 5146                                                                               C.sub.3 H.sub.7 CHCHC.sub.3 H.sub.6 O                                                          C.sub.7 H.sub.15                                                                             K39 C45 N65                                                                               I                                 5147                                                                               C.sub.3 H.sub.7 CHCHC.sub.3 H.sub.6 O                                                          C.sub.8 H.sub.17                                                                             K32 C56 A59 N63                                                                           I                                 5148                                                                               C.sub.3 H.sub.7 CHCHC.sub.3 H.sub.6 O                                                          C.sub.9 H.sub.19                                                                             K42 C64 A73                                                                               I                                 5151                                                                               H.sub.2 CCHC.sub.4 H.sub.8 O                                                                   C.sub.7 H.sub.15                                                                             K27 A43 N57                                                                               I                                 5152                                                                               H.sub.2 CCHC.sub.4 H.sub.8 O                                                                   C.sub.8 H.sub.17                                                                             K44 A51 N55                                                                               I                                 5153                                                                               H.sub.2 CCHC.sub.4 H.sub.8 O                                                                   C.sub.9 H.sub.19                                                                             K48 A62    I                                 5154                                                                               H.sub.2 CCHC.sub.4 H.sub.8 O                                                                   C.sub.10 H.sub.21                                                                            K55.5                                                                              C33 A62                                                                               I                                 5155                                                                               CH.sub.3 CHCHC.sub.4 H.sub.8 COO                                                               C.sub.7 H.sub.15                                                                             K51 A34 N55                                                                               I                                 5156                                                                               CH.sub.3 CHCHC.sub.4 H.sub.8 COO                                                               C.sub.8 H.sub.17                                                                             K48 C39 A46 N52                                                                           I                                 5157                                                                               CH.sub.3 CHCHC.sub.4 H.sub.8 COO                                                               C.sub.9 H.sub.19                                                                             K56 C48 A60                                                                               I                                 5160                                                                               H.sub.2 CCHC.sub.5 H.sub.10 O                                                                  C.sub.7 H.sub.15                                                                             K56 C34 A47 N67                                                                           I                                 5161                                                                               H.sub.2 CCHC.sub.5 H.sub.10 O                                                                  C.sub.8 H.sub.17                                                                             K37 C30 A58 N64                                                                           I                                 5162                                                                               H.sub.2 CCHC.sub.5 H.sub.10 O                                                                  C.sub.9 H.sub.19                                                                             K31 A69    I                                 5163                                                                               CH.sub.3 CHCHC.sub.5 H.sub.10 O                                                                C.sub.7 H.sub.15                                                                             K39 C45 A65                                                                               I                                 5164                                                                               CH.sub.3 CHCHC.sub.5 H.sub.10 O                                                                C.sub.8 H.sub.17                                                                             K40 C52 A57 N67                                                                           I                                 5165                                                                               CH.sub.3 CHCHC.sub.5 H.sub.10 O                                                                C.sub.9 H.sub.19                                                                             K39 C53 A71 N72                                                                           I                                 5166                                                                               H.sub.2 CCHC.sub.5 H.sub.10 COO                                                                C.sub.7 H.sub.15                                                                             K43 A36 N46                                                                               I                                 5167                                                                               H.sub.2 CCHC.sub.5 H.sub.10 COO                                                                C.sub.8 H.sub.17                                                                             K37 C34 A43 N44                                                                           I                                 5168                                                                               H.sub.2 CCHC.sub.5 H.sub.10 COO                                                                C.sub.9 H.sub.19                                                                             K48 C42 A56                                                                               I                                 5169                                                                               H.sub.2 CCHC.sub.5 H.sub.10 O                                                                  C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K35 C*29 N*46                                                                             I                                 5170                                                                               H.sub.2 CCHC.sub.5 H.sub.10 O                                                                  C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K7  C*19 N*39                                                                             I                                 __________________________________________________________________________

                                      TABLE 50                                     __________________________________________________________________________      ##STR89##                                                                     No  L            R             Cr  LC                                          __________________________________________________________________________     5171                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               C.sub.7 H.sub.15                                                                             K36 C33 A48 N62                                                                             I                                  5172                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               C.sub.8 H.sub.17                                                                             K19.2                                                                              C33.3 A56.1 N60.2                                                                       I                                  5173                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               C.sub.9 H.sub.19                                                                             K37 A67      I                                  5174                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               C.sub.10 H.sub.21                                                                            K38.2                                                                              C49.6 A67.9                                                                             I                                  5175                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               OC.sub.8 H.sub.17                                                                            K48.5                                                                              C76.3 A92 N92.6                                                                         I                                  5176                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K29 C*28 N*40                                                                               I                                  5177                                                                               H.sub.2 CCHC.sub.6 H.sub.12 O                                                               C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K4  C*15 N*32                                                                               I                                  5178                                                                               H.sub.2 CCHC.sub.7 H.sub.14 O                                                               C.sub.7 H.sub.15                                                                             K52 C43 A54 N67                                                                             I                                  5179                                                                               H.sub.2 CCHC.sub.7 H.sub.14 O                                                               C.sub.8 H.sub.17                                                                             K27 C45 A62 N66                                                                             I                                  5180                                                                               H.sub.2 CCHC.sub.7 H.sub.14 O                                                               C.sub.9 H.sub.19                                                                             K19 C39 A71  I                                  5181                                                                               H.sub.2 CCHC.sub.7 H.sub.14 O                                                               C.sub.10 H.sub.21                                                                            K32.5                                                                              C55 A72  I                                  5182                                                                               H.sub.2 CCHC.sub.7 H.sub.14 O                                                               C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K16 C*35 N*48                                                                               I                                  5183                                                                               H.sub.2 CCHC.sub.7 H.sub.14 O                                                               C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K-1 C*28 N*42                                                                               I                                  5184                                                                               H.sub.2 CCHC.sub.8 H.sub.16 O                                                               C.sub.7 H.sub.15                                                                             K43 C42 A55 N64                                                                             I                                  5185                                                                               H.sub.2 CCHC.sub.8 H.sub.16 O                                                               C.sub.8 H.sub.17                                                                             K24 C46 A60 N63                                                                             I                                  5186                                                                               H.sub.2 CCHC.sub.8 H.sub.16 O                                                               C.sub.9 H.sub.19                                                                             K35 C45 A70  I                                  5187                                                                               H.sub.2 CCHC.sub.8 H.sub.16 O                                                               C.sub.10 H.sub.21                                                                            K33 C57 A70  I                                  5188                                                                               H.sub.2 CCHC.sub.8 H.sub.16 O                                                               C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K17 C*34 N*44                                                                               I                                  5189                                                                               H.sub.2 CCHC.sub.8 H.sub.16 O                                                               C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K12 C*27 N*38                                                                               I                                  5191                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               C.sub.7 H.sub.15                                                                             K49 C46 A59 N67                                                                             I                                  5192                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               C.sub.8 H.sub.17                                                                             K33.9                                                                              C53 A64.4 N66.2                                                                         I                                  5193                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               C.sub.9 H.sub.19                                                                             K31.3                                                                              C52.8 A71.7                                                                             I                                  5194                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               C.sub.10 H.sub.21                                                                            K39.9                                                                              C65.2 A72.5                                                                             I                                  5195                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               C.sub.12 H.sub.25                                                                            K45.9                                                                              C75.5 A76.5                                                                             I                                  5196                                                                               H.sub.2 CCHC.sub.10 H.sub.20 O                                                              C.sub.7 H.sub.15                                                                             K50 C45 A60 N65                                                                             I                                  5197                                                                               H.sub.2 CCHC.sub.10 H.sub.20 O                                                              C.sub.8 H.sub.17                                                                             K36 C50 A63 N64                                                                             I                                  5198                                                                               H.sub.2 CCHC.sub.10 H.sub.20 O                                                              C.sub.9 H.sub.19                                                                             K46 C50 A70  I                                  5199                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               OC.sub.8 H.sub.17                                                                            K44.1                                                                              C78.5 A94.5                                                                             I                                  5200                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                               C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K20 C*40 N*49                                                                               I                                  5201                                                                               H.sub.2 CCHC.sub.10 H.sub.20 O                                                              C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K35 C*40 N*47                                                                               I                                  __________________________________________________________________________

                                      TABLE 51                                     __________________________________________________________________________      ##STR90##                                                                     No  L               R             Cr LC                                        __________________________________________________________________________     5202                                                                               H.sub.2 CCHC.sub.9 H.sub.18 O                                                                  C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K17                                                                               C*36 N*45                                                                            I                                   5203                                                                               H.sub.2 CCHC.sub.10 H.sub.20 O                                                                 C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K33                                                                               C*37 N*43                                                                            I                                   5204                                                                               C.sub.3 H.sub.7 CH%CHCH.sub.2 O                                                                C.sub.9 H.sub.19                                                                             K32                                                                               A17   I                                   5208                                                                               CH.sub.3 CH%CHC.sub.2 H.sub.4 O                                                                C.sub.7 H.sub.15                                                                             K45                                                                               A41 N47                                                                              I                                   5209                                                                               CH.sub.3 CH%CHC.sub.2 H.sub.4 O                                                                C.sub.8 H.sub.17                                                                             K34                                                                               A45   I                                   5210                                                                               CH.sub.3 CH%CHC.sub.2 H.sub.4 O                                                                C.sub.9 H.sub.19                                                                             K48                                                                               C25 A55                                                                              I                                   5211                                                                               C.sub.2 H.sub.5 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.7 H.sub.15                                                                             K43                                                                               A45 N48                                                                              I                                   5212                                                                               C.sub.2 H.sub.5 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.8 H.sub.17                                                                             K42                                                                               C32 A47                                                                              I                                   5213                                                                               C.sub.2 H.sub.5 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.9 H.sub.19                                                                             K58                                                                               C41 A56                                                                              I                                   5214                                                                               C.sub.3 H.sub.7 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.7 H.sub.15                                                                             K20                                                                               A44   I                                   5215                                                                               C.sub.3 H.sub.7 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.8 H.sub.17                                                                             K33                                                                               C35 A46                                                                              I                                   5216                                                                               C.sub.3 H.sub.7 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.9 H.sub.19                                                                             K34                                                                               C45 A54                                                                              I                                   5217                                                                               C.sub.4 H.sub.9 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.7 H.sub.15                                                                             K28                                                                               A43 N44                                                                              I                                   5218                                                                               C.sub.4 H.sub.9 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.8 H.sub.17                                                                             K25                                                                               C34 A46                                                                              I                                   5219                                                                               C.sub.4 H.sub.9 CH%CHC.sub.2 H.sub.4 O                                                         C.sub.9 H.sub.19                                                                             K24                                                                               C43 A54                                                                              I                                   5220                                                                               C.sub.5 H.sub.11 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.7 H.sub.15                                                                             K25                                                                               A40   I                                   5221                                                                               C.sub.5 H.sub.11 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.8 H.sub.17                                                                             K12                                                                               C30 A42                                                                              I                                   5222                                                                               C.sub.5 H.sub.11 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.9 H.sub.19                                                                             K6 C38 A51                                                                              I                                   5223                                                                               C.sub.6 H.sub.13 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.7 H.sub.15                                                                             K33                                                                               A39   I                                   5224                                                                               C.sub.6 H.sub.13 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.8 H.sub.17                                                                             K22                                                                               C25 A41                                                                              I                                   5225                                                                               C.sub.6 H.sub.13 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.9 H.sub.19                                                                             K19                                                                               C34 A49                                                                              I                                   5226                                                                               C.sub.7 H.sub.15 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.7 H.sub.15                                                                             K40                                                                               A37   I                                   5227                                                                               C.sub.7 H.sub.15 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.8 H.sub.17                                                                             K30                                                                               C20 A39                                                                              I                                   5228                                                                               C.sub.7 H.sub.15 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.9 H.sub.19                                                                             K26                                                                               C24 A47                                                                              I                                   5229                                                                               C.sub.8 H.sub.17 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.7 H.sub.15                                                                             K31                                                                               A35   I                                   5230                                                                               C.sub.8 H.sub.17 CH%CHC.sub.7 H.sub.4 O                                                        C.sub.8 H.sub.17                                                                             K32                                                                               C14 A41                                                                              I                                   5231                                                                               C.sub.8 H.sub.17 CH%CHC.sub.2 H.sub.4 O                                                        C.sub.9 H.sub.19                                                                             K29                                                                               C14 A50                                                                              I                                   5232                                                                               CH.sub.3 CH%CHC.sub.3 H.sub.6 O                                                                C.sub.9 H.sub.19                                                                             K22                                                                               A46   I                                   5233                                                                               C.sub.2 H.sub.5 CH%CHC.sub.3 H.sub.6 COO                                                       C.sub.7 H.sub.15                                                                             K26                                                                               A31   I                                   __________________________________________________________________________

                                      TABLE 52                                     __________________________________________________________________________      ##STR91##                                                                     No  L            R             Cr  LC                                          __________________________________________________________________________     27740                                                                              ClCF.sub.2 O C.sub.4 H.sub.9                                                                              K30 S130.6 N135.2                                                                         I                                    27749                                                                              NC           C.sub.7 H.sub.15                                                                             K82 A158 N223                                                                             I                                    27750                                                                              NC           OC.sub.2 H.sub.5                                                                             K144.5                                                                             N232   B                                    27751                                                                              NC           OC.sub.3 H.sub.7                                                                             K114.5                                                                             N223.5 B                                    27752                                                                              NC           OC.sub.5 H.sub.11                                                                            K93 N205   B                                    27753                                                                              NC           CH.sub.2 CHMeC.sub.2 H.sub.5                                                               1 K76 S125 N*178                                                                            I                                    27754                                                                              NC           C.sub.2 H.sub.4 CHMeC.sub.2 H.sub.5                                                        1 K101                                                                               S159 N*189.5                                                                          I                                    27755                                                                              C.sub.2 H.sub.5                                                                             C.sub.7 H.sub.15                                                                             K68 S179 N182                                                                             I                                    27756                                                                              C.sub.3 H.sub.7                                                                             C.sub.2 H.sub.5                                                                              K125.5                                                                             S128.5 N167                                                                           I                                    27757                                                                              C.sub.3 H.sub.7                                                                             C.sub.3 H.sub.7                                                                              K116.5                                                                             S175 N194.5                                                                           I                                    27758                                                                              C.sub.3 H.sub.7                                                                             C.sub.5 H.sub.11                                                                             K51 S190   I                                    27759                                                                              C.sub.4 H.sub.9                                                                             C.sub.2 H.sub.5                                                                              K108.5                                                                             S140 N163.5                                                                           I                                    27760                                                                              C.sub.4 H.sub.9                                                                             C.sub.5 H.sub.11                                                                             K37.5                                                                              S187   I                                    27761                                                                              C.sub.5 H.sub.11                                                                            C.sub.2 H.sub.5                                                                              K101                                                                               S139 N167                                                                             I                                    27762                                                                              C.sub.5 H.sub.11                                                                            C.sub.3 H.sub.7                                                                              K93.5                                                                              S179 N190                                                                             I                                    27763                                                                              C.sub.5 H.sub.11                                                                            C.sub.5 H.sub.11                                                                             K39.5                                                                              S189.2 I                                    27764                                                                              C.sub.5 H.sub.11                                                                            C.sub.7 H.sub.15                                                                             K122.5                                                                             S186.5 I                                    27765                                                                              C.sub.7 H.sub.15                                                                            C.sub.2 H.sub.5                                                                              K80 S136.5 N157                                                                           I                                    27768                                                                              C.sub.6 H.sub.13 CHMeOCH.sub.2                                                              C.sub.7 H.sub.15                                                                           1 K36.5                                                                              A98.4  I                                    27769                                                                              C.sub.2 H.sub.5 CHMeCH.sub.2 O                                                              OC.sub.8 H.sub.17                                                                          S K64.6                                                                              B104.9 A160.5                                                                         I                                    27770                                                                              C.sub.2 H.sub.5 CHMeCH.sub.2 O                                                              OC.sub.5 H.sub.19                                                                          S K61.7                                                                              B108.2 A156                                                                           I                                    27771                                                                              C.sub.2 H.sub.5 CHMeC.sub.3 H.sub.6 O                                                       OC.sub.8 H.sub.17                                                                          S K68 B101 A160.9                                                                           I                                    27772                                                                              C.sub.2 H.sub.5 CHMeC.sub.3 H.sub.6 O                                                       OC.sub.9 H.sub.19                                                                          S K63.5                                                                              B103 A157.4                                                                           I                                    __________________________________________________________________________

                                      TABLE 53                                     __________________________________________________________________________      ##STR92##                                                                     No  L          R                Cr LC                                          __________________________________________________________________________     28508                                                                              C.sub.5 H.sub.11                                                                          OOCC.sub.10 H.sub.21                                                                            K118                                                                              C133 N172  I                                28509                                                                              C.sub.5 H.sub.11                                                                          OOCC.sub.11 H.sub.23                                                                            K120                                                                              C138 N169  I                                28510                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    C.sub.6 H.sub.13                                                                              S K34                                                                               B98 A137   I                                28511                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    C.sub.7 H.sub.15                                                                              S K53                                                                               B101 A143  I                                28512                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    C.sub.8 H.sub.17                                                                              S K41                                                                               B109 A143  I                                28513                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    C.sub.9 H.sub.19                                                                              S K49                                                                               B113 A145  I                                28514                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    C.sub.10 H.sub.21                                                                             S K48                                                                               B116 A145  I                                28515                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    OC.sub.6 H.sub.13                                                                             R K58                                                                               C*81 A161 N*165                                                                           I                                28516                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    OC.sub.7 H.sub.15                                                                             R K44                                                                               B78 C*95 A162 N*163                                                                       I                                28517                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    OC.sub.8 H.sub.17                                                                             R K53                                                                               B88 C*102 A162                                                                            I                                28518                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    OC.sub.9 H.sub.19                                                                             R K60                                                                               B92 C*106 A163                                                                            I                                28519                                                                              C.sub.4 H.sub.9 CHFCOO                                                                    OC.sub.10 H.sub.21                                                                            R K35                                                                               S70 B98 C*108 A165                                                                        I                                28522                                                                              C.sub.5 H.sub.11                                                                          OCH.sub.2 CHCHC.sub.5 H.sub.11                                                                  K97                                                                               C115 N176  I                                28523                                                                              C.sub.5 H.sub.11                                                                          OCH.sub.2 CHCHC.sub.6 H.sub.13                                                                  K94                                                                               C125 N170  I                                28524                                                                              C.sub.5 H.sub.11                                                                          OCH.sub.2 CHCHC.sub.7 H.sub.15                                                                  K86                                                                               C135 N167  I                                28525                                                                              C.sub.5 H.sub.11                                                                          OCH.sub.2 CHCHC.sub.8 H.sub.17                                                                  K93                                                                               C140 N163  I                                28526                                                                              C.sub.5 H.sub.11                                                                          OC.sub.3 H.sub.6 CHCHC.sub.3 H.sub.7                                                            K87                                                                               C93 N184   I                                28528                                                                              C.sub.5 H.sub.11                                                                          OC.sub.5 H.sub.10 CHCH.sub.2                                                                    K55                                                                               C65 A112 N185                                                                             I                                28529                                                                              C.sub.5 H.sub.11                                                                          OC.sub.5 H.sub.10 CHCHCH.sub.3                                                                  K81                                                                               C111 A130 N185                                                                            I                                28530                                                                              C.sub.5 H.sub.11                                                                          OC.sub.6 H.sub.12 CHCH.sub.2                                                                    K67                                                                               C96 A121 N176                                                                             I                                28531                                                                              C.sub.5 H.sub.11                                                                          OC.sub.7 H.sub.14 CHCH.sub.2                                                                    K59                                                                               C91 A142 N176                                                                             I                                28532                                                                              C.sub.5 H.sub.11                                                                          OC.sub.8 H.sub.16 CHCH.sub.2                                                                    K55                                                                               C103 A145 N169                                                                            I                                28533                                                                              C.sub.5 H.sub.11                                                                          OC.sub.9 H.sub.18 CHCH.sub.2                                                                    K57                                                                               C97 A151 N168                                                                             I                                28535                                                                              C.sub.5 H.sub.11                                                                          OC.sub.4 H.sub.8 CH%CHC.sub.2 H.sub.5                                                           K86                                                                               C85 N168   I                                28536                                                                              C.sub.5 H.sub.11                                                                          OC.sub.4 H.sub.8 CH/CH.sub.2 \CH.sub.2                                                K81                                                                               S75 N180   I                                28537                                                                              C.sub.3 H.sub.7                                                                           OC.sub.6 H.sub.12 CH/CH.sub.2 \CH.sub.2                                               K80                                                                               S70 C84 N174                                                                              I                                __________________________________________________________________________

                  TABLE 54                                                         ______________________________________                                          ##STR93##                                                                     No       L         R         Cr    LC                                          ______________________________________                                         28896    C.sub.5 H.sub.11                                                                         C.sub.5 H.sub.11                                                                         K33.4 S121.2 I                                    ______________________________________                                          ##STR94##                                                                     No     L          R        Cr    LC                                            ______________________________________                                         28548  C.sub.8 H.sub.17O                                                                         C.sub.6 H.sub.17                                                                        K51   C63 A113 N121                                                                            I                                   ______________________________________                                          ##STR95##                                                                     No     L         R         Cr     LC                                           ______________________________________                                         33521  C.sub.5 H.sub.11                                                                         C.sub.6 H.sub.13                                                                         K72    S65 N104                                                                               I                                    33522  C.sub.5 H.sub.11                                                                         C.sub.7 H.sub.15                                                                         K76    S86 N109                                                                               I                                    33523  C.sub.5 H.sub.11                                                                         C.sub.9 H.sub.19                                                                         K52    S107 N113                                                                              I                                    33524  C.sub.6 H.sub.13                                                                         C.sub.6 H.sub.13                                                                         K61    S76 N100.8                                                                             I                                    33525  C.sub.6 H.sub.13                                                                         C.sub.7 H.sub.15                                                                         K48    S92 N107                                                                               I                                    33526  C.sub.6 H.sub.13                                                                         C.sub.9 H.sub.19                                                                         K66    S109 N110                                                                              I                                    33527  C.sub.8 H.sub.17                                                                         C.sub.8 H.sub.17                                                                         K73    F66 C103.5                                                                             I                                    ______________________________________                                    

                                      TABLE 55                                     __________________________________________________________________________      ##STR96##                                                                     No  L              R             Cr LC                                         __________________________________________________________________________     33600                                                                              C.sub.4 H.sub.9 OCHMeCOO                                                                      C.sub.8 H.sub.17                                                                           S K44                                                                               C*60 N*96                                                                             I                                   33601                                                                              C.sub.4 H.sub.9 OCHMeCOO                                                                      OC.sub.8 H.sub.17                                                                          S K68                                                                               C*103 N*138                                                                           I                                   33603                                                                              C.sub.6 H.sub.13 O                                                                            C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K56                                                                               C*54 N*152                                                                            I                                   33604                                                                              C.sub.7 H.sub.15 O                                                                            C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K64                                                                               C*65 N*148                                                                            I                                   33605                                                                              C.sub.8 H.sub.17 O                                                                            C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K71                                                                               C*70 N*142                                                                            I                                   33606                                                                              C.sub.9 H.sub.19 O                                                                            C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K78                                                                               C*77 N*142                                                                            I                                   33607                                                                              C.sub.10 H.sub.21 O                                                                           C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K74                                                                               C*82 N*141                                                                            I                                   33608                                                                              C.sub.11 H.sub.23 O                                                                           C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K78                                                                               C*85 N*136                                                                            I                                   33609                                                                              C.sub.12 H.sub.25 O                                                                           C.sub.4 H.sub.8 CHMeC.sub.2 H.sub.5                                                        S K83                                                                               C*88 N*133                                                                            I                                   33610                                                                              C.sub.6 H.sub.13 O                                                                            C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K72                                                                               C*50 N*148                                                                            I                                   33611                                                                              C.sub.7 H.sub.15 O                                                                            C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K56                                                                               C*64 N*144                                                                            I                                   33612                                                                              C.sub.8 H.sub.17 O                                                                            C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K56                                                                               C*72 N*142                                                                            I                                   33613                                                                              C.sub.9 H.sub.19 O                                                                            C.sub.8 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K68                                                                               C*80 N*138                                                                            I                                   33614                                                                              C.sub.10 H.sub.21 O                                                                           C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K86                                                                               C*84 N*137                                                                            I                                   33615                                                                              C.sub.11 H.sub.23 O                                                                           C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K83                                                                               C*90 N*132                                                                            I                                   33616                                                                              C.sub.12 H.sub.25 O                                                                           C.sub.5 H.sub.10 CHMeC.sub.2 H.sub.5                                                       S K69                                                                               C*94 N*132                                                                            I                                   33618                                                                              C.sub.6 H.sub.13 CHMeO                                                                        OC.sub.8 H.sub.17                                                                          1 K72                                                                               C*48 N*115                                                                            I                                   33620                                                                              CH.sub.3 CHMeCHClCOO                                                                          C.sub.7 H.sub.15                                                                           S K70                                                                               C*96 N*202                                                                            I                                   33621                                                                              CH.sub.3 CHMeCHClCOO                                                                          C.sub.9 H.sub.19                                                                           S K62                                                                               C*69 N*157                                                                            I                                   33622                                                                              C.sub.2 H.sub.5 CHMeCHClCOO                                                                   C.sub.8 H.sub.17                                                                           3 K? C*77 N*124                                                                            I                                   __________________________________________________________________________

                                      TABLE 56                                     __________________________________________________________________________      ##STR97##                                                                     No       L     R            Cr LC                                              __________________________________________________________________________     36376    C.sub.4 H.sub.9                                                                      OC.sub.9 H.sub.19                                                                       2   K66                                                                               S190 I                                          __________________________________________________________________________      ##STR98##                                                                     No  L           R      Cr  LC                                                  __________________________________________________________________________     37030                                                                              C.sub.2 H.sub.5                                                                            CN     K137                                                                               S136 N243   I                                       37031                                                                              C.sub.5 H.sub.11                                                                           CN     K117                                                                               S192 N248   I                                       37033                                                                              CH.sub.3    C.sub.10 H.sub.21                                                                     K76 C77 N124    I                                       37035                                                                              C.sub.2 H.sub.5                                                                            C.sub.10 H.sub.21                                                                     K82 C82 N142    I                                       37038                                                                              C.sub.3 H.sub.7                                                                            C.sub.10 H.sub.21                                                                     K76 C89 N161    I                                       37039                                                                              C.sub.3 H.sub.7                                                                            C.sub.12 H.sub.25                                                                     K64.9                                                                              S76.3 C108.1 N152.8                                                                        I                                       37041                                                                              C.sub.4 H.sub.9                                                                            C.sub.10 H.sub.21                                                                     K40 B82 C99 N160                                                                               I                                       37042                                                                              C.sub.4 H.sub.9                                                                            C.sub.12 H.sub.25                                                                     K80 S82 S83.8 C115.3 N152.7                                                                    I                                       37046                                                                              C.sub.5 H.sub.11                                                                           C.sub.10 H.sub.21                                                                     K64 B85 C104 N161                                                                              I                                       37047                                                                              C.sub.5 H.sub.11                                                                           C.sub.11 H.sub.23                                                                     K70 S80 S82.7 C114.5 N160.5                                                                    I                                       37048                                                                              C.sub.5 H.sub.11                                                                           C.sub.12 H.sub.25                                                                     K67 S83 S87.2 C121.5 N156                                                                      I                                       37051                                                                              C.sub.7 H.sub.15                                                                           C.sub.10 H.sub.21                                                                     K78 B89 C116 N158                                                                              I                                       37052                                                                              C.sub.9 H.sub.19                                                                           C.sub.10 H.sub.21                                                                     K77 S85 C123 N153                                                                              I                                       37053                                                                              C.sub.10 H.sub.21                                                                          C.sub.10 H.sub.21                                                                     K77 S87 C125 N150                                                                              I                                       37054                                                                              C.sub.5 H.sub.11                                                                           OC.sub.8 H.sub.17                                                                     K72.1                                                                              S68 S74 C100 N193                                                                          I                                       37055                                                                              C.sub.5 H.sub.11                                                                           OC.sub.9 H.sub.19                                                                     K74.3                                                                              G69 C117.7 N189                                                                            I                                       37056                                                                              C.sub.5 H.sub.11                                                                           OC.sub.10 H.sub.21                                                                    K74.7                                                                              G72.5 C129.8 N186.5                                                                        I                                       37058                                                                              H.sub.2 CCHC.sub.2 H.sub.4                                                                 C.sub.10 H.sub.21                                                                     K71 C92 N162    I                                       37059                                                                              CH.sub.3 CHCHC.sub.2 H.sub.4                                                               C.sub.10 H.sub.21                                                                     K52 S56 S64 S69 C92 N170                                                                       I                                       __________________________________________________________________________

                                      TABLE 57                                     __________________________________________________________________________      ##STR99##                                                                     No  L          R         Cr LC                                                 __________________________________________________________________________     37078                                                                              (Me).sub.2 CCHC.sub.2 H.sub.4                                                             C.sub.10 H.sub.21                                                                     2  K40                                                                               C83 N106                                                                              I                                           37079                                                                              (Me).sub.2 CCHC.sub.2 H.sub.4                                                             OC.sub.10 H.sub.21                                                                    2  K82                                                                               C112 N138                                                                             I                                           37080                                                                              CH.sub.3   C.sub.10 H.sub.21                                                                     2  K50                                                                               S54 C68 N107                                                                          I                                           __________________________________________________________________________      ##STR100##                                                                    No  L       R         Cr  LC                                                   __________________________________________________________________________     37109                                                                              H       C.sub.6 H.sub.13                                                                         K44 N53      W                                           37110                                                                              H       C.sub.8 H.sub.17                                                                         K41.3                                                                              C51 A57.6 N60.2                                                                         W                                           37111                                                                              H       C.sub.9 H.sub.19                                                                         K52.8                                                                              C56.8 A67.2                                                                             W                                           37112                                                                              H       C.sub.10 H.sub.21                                                                        K44 C64.9 A67.7                                                                             W                                           37113                                                                              H       C.sub.11 H.sub.23                                                                        K48 C70.2 A71.6                                                                             W                                           37114                                                                              H       C.sub.12 H.sub.25                                                                        K52 C72.3    W                                           37115                                                                              H       OC.sub.7 H.sub.15                                                                        K56.4                                                                              C71.3 A83.4 N85.1                                                                       W                                           37116                                                                              H       OC.sub.8 H.sub.17                                                                        K69.2                                                                              C75.8 A90.2                                                                             W                                           37117                                                                              H       OC.sub.11 H.sub.23                                                                       K68 C95      W                                           37118                                                                              C.sub.2 H.sub.5 OOC                                                                    C.sub.8 H.sub.17                                                                      1  K38 C*36     I                                           __________________________________________________________________________

                                      TABLE 58                                     __________________________________________________________________________      ##STR101##                                                                    No  L             R            Cr  LC                                          __________________________________________________________________________     9165                                                                               C.sub.2 H.sub.5 CHMeCH.sub.2 OOC                                                             OC.sub.11 H.sub.22 OH                                                                     S K80 C*58.9 A72.8                                                                          I                                    9179                                                                               C.sub.5 H.sub.11                                                                             Cl           K69 N37    E                                    9182                                                                               C.sub.10 H.sub.21 O                                                                          Cl           K85.5                                                                              C86.5  I                                    9200                                                                               CH.sub.3      CN           K160                                                                               N65    E                                    9201                                                                               C.sub.2 H.sub.5                                                                              CN           K110                                                                               N62    E                                    9209                                                                               C.sub.10 H.sub.21                                                                            CN           K64.4                                                                              A47.9 N62.1                                                                           B                                    9210                                                                               C.sub.11 H.sub.23                                                                            CN           K64 A61.4 N66.7                                                                           I                                    9211                                                                               C.sub.12 H.sub.25                                                                            CN           K72 A64.7 N66                                                                             I                                    9221                                                                               C.sub.14 H.sub.29 O                                                                          CN           K96 A91    I                                    9226                                                                               C.sub.7 H.sub.15                                                                             OC.sub.3 H.sub.6 CN                                                                         K85.5                                                                              A70 N77                                                                               I                                    __________________________________________________________________________      ##STR102##                                                                    No   L           R           Cr   LC                                           __________________________________________________________________________     9227 C.sub.7 H.sub.15 O                                                                         OC.sub.3 H.sub.6 CN                                                                        K105.5                                                                              N102.5 U                                     9228 C.sub.5 H.sub.11                                                                           OC.sub.5 H.sub.10 CN                                                                       K63.4                                                                               A53 N70                                                                               I                                     9230 C.sub.2 H.sub.5 CHMeC.sub.2 H.sub.4                                                        CN       S  K81  N*23.5 B                                     9237 H.sub.2 CCHCH.sub.2 O                                                                      CN          K115.2                                                                              N104.1 I                                     9243 CH.sub.3 NMe                                                                               NO.sub.2    K217 X220   Z                                     9256 C.sub.4 H.sub.9                                                                            C.sub.7 H.sub.15                                                                           K6.2 S-2.5 N17.5                                                                           I                                     9257 C.sub.4 H.sub.9                                                                            C.sub.8 H.sub.17                                                                           K14.2                                                                               S10.3 N16.5                                                                           I                                     9258 C.sub.4 H.sub.9                                                                            C.sub.9 H.sub.19                                                                           K30  S20.5 N27                                                                             I                                     9259 C.sub.5 H.sub.11                                                                           C.sub.6 H.sub.13                                                                           K31.2                                                                               S21    I                                     9260 C.sub.5 H.sub.11                                                                           C.sub.7 H.sub.15                                                                           K27.3                                                                               S17.5 N39.1                                                                           I                                     9261 C.sub.5 H.sub.11                                                                           C.sub.8 H.sub.17                                                                           K8.6 S30.5 N33.7                                                                           I                                     9262 C.sub.5 H.sub.11                                                                           C.sub.9 H.sub.19                                                                           K28  S37 N44.9                                                                             I                                     9263 C.sub.6 H.sub.13                                                                           C.sub.7 H.sub.15                                                                           K19.3                                                                               S20 N30                                                                               I                                     9264 C.sub.6 H.sub.13                                                                           C.sub.8 H.sub.17                                                                           K22.2                                                                               S27.8  I                                     9265 C.sub.6 H.sub.13                                                                           C.sub.9 H.sub.19                                                                           K23.7                                                                               S31.7  I                                     9266 C.sub.7 H.sub.15                                                                           C.sub.7 H.sub.15                                                                           K41.6                                                                               S35.2 N40.8                                                                           I                                     9267 C.sub.7 H.sub.15                                                                           C.sub.9 H.sub.19                                                                           K20  S43.8  I                                     9271 CH.sub.3    OCH.sub.3   K124.8                                                                              N32.1  E                                     __________________________________________________________________________

                                      TABLE 59                                     __________________________________________________________________________      ##STR103##                                                                    No  L              R               Cr LC                                       __________________________________________________________________________     5352                                                                               C.sub.12 H.sub.25                                                                             CN              K87                                                                               A81  I                                   5353                                                                               C.sub.13 H.sub.27                                                                             CN              K87                                                                               S80  B                                   5355                                                                               C.sub.8 H.sub.17 O                                                                            CN              K84                                                                               A112 I                                   5356                                                                               C.sub.10 H.sub.21 O                                                                           CN              K70                                                                               A111 I                                   5357                                                                               C.sub.12 H.sub.25 O                                                                           CN              K85                                                                               A111 I                                   5358                                                                               C.sub.12 H.sub.25                                                                             OC.sub.4 H.sub.9                                                                               K48                                                                               S43  I                                   5360                                                                               CH.sub.3 O     C.sub.8 H.sub.17                                                                               K68                                                                               A63  I                                   5361                                                                               CH.sub.3 O     C.sub.12 H.sub.25                                                                              K90                                                                               A83  I                                   5362                                                                               C.sub.8 H.sub.17 O                                                                            C.sub.8 H.sub.17                                                                               K65                                                                               C64 A79                                                                             I                                   5367                                                                               C.sub.12 H.sub.25 O                                                                           OCH.sub.2 CHMeC.sub.2 H.sub.5                                                                S K63                                                                               A45  I                                   5369                                                                               C.sub.8 H.sub.17 O                                                                            COOCH.sub.2 CHMeC.sub.2 H.sub.5                                                              S K41                                                                               S52 A60                                                                             I                                   5370                                                                               C.sub.12 H.sub.25 O                                                                           COOCH.sub.2 CHMeC.sub.2 H.sub.5                                                              S K42                                                                               A60  I                                   5371                                                                               C.sub.8 H.sub.17 O                                                                            OC.sub.3 H.sub.6 CHMeC.sub.2 H.sub.5                                                         S K42                                                                               C*61 A66                                                                            I                                   5372                                                                               C.sub.12 H.sub.25 O                                                                           OC.sub.3 H.sub.6 CHMeC.sub.2 H.sub.5                                                         S K50                                                                               C*63 A72                                                                            I                                   5374                                                                               C.sub.2 H.sub.5 CHMeCH.sub.2 O                                                                OC.sub.12 H.sub.25                                                                           S K56                                                                               A46  I                                   5376                                                                               C.sub.2 H.sub.5 CHMeCH.sub.2 OOC                                                              OC.sub.12 H.sub.25                                                                           S K58                                                                               C*45 A49                                                                            I                                   5377                                                                               C.sub.2 H.sub.5 CHMeC.sub.3 H.sub.6 OOC                                                       OC.sub.12 H.sub.25                                                                           1 K? A<?  I                                   5378                                                                               C.sub.3 H.sub.7 CHMeC.sub.4 H.sub.8 O                                                         C.sub.8 H.sub.17                                                                             2 K48                                                                               C56.5                                                                               I                                   5379                                                                               C.sub.2 H.sub.5 CHMeC.sub.5 H.sub.10 O                                                        C.sub.8 H.sub.17                                                                             2 K49                                                                               C62  I                                   __________________________________________________________________________      ##STR104##                                                                    No       L                R      Cr LC                                         __________________________________________________________________________     5381     C.sub.5 H.sub.11 CHCHCH.sub.2 O                                                                 C.sub.8 H.sub.17                                                                      K48                                                                               C77  I                                     __________________________________________________________________________

                                      TABLE 60                                     __________________________________________________________________________      ##STR105##                                                                    No  L              R               Cr LC                                       __________________________________________________________________________     5352                                                                               C.sub.12 H.sub.25                                                                             CN              K87                                                                               A81  I                                   5353                                                                               C.sub.13 H.sub.27                                                                             CN              K87                                                                               S80  B                                   5355                                                                               C.sub.8 H.sub.17 O                                                                            CN              K84                                                                               A112 I                                   5356                                                                               C.sub.10 H.sub.21 O                                                                           CN              K70                                                                               A111 I                                   5357                                                                               C.sub.12 H.sub.25 O                                                                           CN              K85                                                                               A111 I                                   5358                                                                               C.sub.12 H.sub.25                                                                             OC.sub.4 H.sub.9                                                                               K48                                                                               S43  I                                   5360                                                                               CH.sub.3 O     C.sub.8 H.sub.17                                                                               K68                                                                               A63  I                                   5361                                                                               CH.sub.3 O     C.sub.12 H.sub.25                                                                              K90                                                                               A83  I                                   5362                                                                               C.sub.8 H.sub.17 O                                                                            C.sub.8 H.sub.17                                                                               K65                                                                               C64 A79                                                                             I                                   5367                                                                               C.sub.12 H.sub.25 O                                                                           OCH.sub.2 CHMeC.sub.2 H.sub.5                                                                S K63                                                                               A45  I                                   5369                                                                               C.sub.8 H.sub.17 O                                                                            COOCH.sub.2 CHMeC.sub.2 H.sub.5                                                              S K41                                                                               S52 A60                                                                             I                                   5370                                                                               C.sub.12 H.sub.25 O                                                                           COOCH.sub.2 CHMeC.sub.2 H.sub.5                                                              S K42                                                                               A60  I                                   5371                                                                               C.sub.8 H.sub.17 O                                                                            OC.sub.3 H.sub.6 CHMeC.sub.2 H.sub.5                                                         S K42                                                                               C*61 A66                                                                            I                                   5372                                                                               C.sub.12 H.sub.25 O                                                                           OC.sub.3 H.sub.6 CHMeC.sub.2 H.sub.5                                                         S K50                                                                               C*63 A72                                                                            I                                   5374                                                                               C.sub.2 H.sub.5 CHMeCH.sub.2 O                                                                OC.sub.12 H.sub.25                                                                           S K56                                                                               A46  I                                   5376                                                                               C.sub.2 H.sub.5 CHMeCH.sub.2 OOC                                                              OC.sub.12 H.sub.25                                                                           S K58                                                                               C*45 A49                                                                            I                                   5377                                                                               C.sub.2 H.sub.5 CHMeC.sub.3 H.sub.6 OOC                                                       OC.sub.12 H.sub.25                                                                           1 K? A<?  I                                   5378                                                                               C.sub.3 H.sub.7 CHMeC.sub.4 H.sub.8 O                                                         C.sub.8 H.sub.17                                                                             2 K48                                                                               C56.5                                                                               I                                   5379                                                                               C.sub.2 H.sub.5 CHMeC.sub.5 H.sub.10 O                                                        C.sub.5 H.sub.17                                                                             2 K49                                                                               C62  I                                   __________________________________________________________________________

                                      TABLE 61                                     __________________________________________________________________________      ##STR106##                                                                    No   L      R     Cr   LC                                                      __________________________________________________________________________     25427                                                                               CH.sub.3                                                                              CN    K196 A221 N296  I                                            25428                                                                               C.sub.2 H.sub.5                                                                       CN    K190 A197 N278  I                                            25429                                                                               C.sub.3 H.sub.7                                                                       CN    K169 A179 N277  I                                            25430                                                                               C.sub.4 H.sub.9                                                                       CN    K129 A139 N256  I                                            25431                                                                               C.sub.5 H.sub.11                                                                      CN    K131 A140 N263  I                                            25432                                                                               C.sub.6 H.sub.13                                                                      CN    K107 A125 N225  U                                            25433                                                                               C.sub.7 H.sub.15                                                                      CN    K110 A132 N242  I                                            25434                                                                               C.sub.8 H.sub.17                                                                      CN    K125 A133 N240  I                                            25435                                                                               C.sub.9 H.sub.19                                                                      CN    K105 A107 N232  I                                            25436                                                                               C.sub.12 H.sub.25                                                                     CN    K109 C119 A227  I                                            25437                                                                               C.sub.16 H.sub.33                                                                     CN    K106 C119 A221  I                                            25438                                                                               CH.sub.3 O                                                                            CN    K182 S169 N321  I                                            25439                                                                               C.sub.7 H.sub.15O                                                                     CN    K97  X267       I                                            25440                                                                               C.sub.8 H.sub.17 O                                                                    CN    K96  X270       I                                            25441                                                                               C.sub.9 H.sub.19 O                                                                    CN    K102 X263       I                                            25442                                                                               C.sub.10 H.sub.21 O                                                                   CN    K104 X252       I                                            25443                                                                               C.sub.11 H.sub.23 O                                                                   CN    K109 X263       I                                            25444                                                                               C.sub.12 H.sub.25 O                                                                   CN    K105 X252       I                                            25445                                                                               C.sub.13 H.sub.27 O                                                                   CN    K103 X246       I                                            25450                                                                               C.sub.4 H.sub.9                                                                       C.sub.4 H.sub.9                                                                      K161.3                                                                              C166.4 N181.9                                                                             I                                            25451                                                                               C.sub.5 H.sub.11                                                                      C.sub.5 H.sub.11                                                                     K134.3                                                                              C173.6 A182.2 N191.3                                                                      I                                            25452                                                                               C.sub.6 H.sub.13                                                                      C.sub.6 H.sub.13                                                                     K116.1                                                                              C172.3 A179.2                                                                             I                                            __________________________________________________________________________

                                      TABLE 62                                     __________________________________________________________________________      ##STR107##                                                                    No  L      R             Cr  LC                                                __________________________________________________________________________     25453                                                                              C.sub.7 H.sub.15                                                                      C.sub.7 H.sub.15                                                                             K109.6                                                                             C175 A187                                                                               I                                        25454                                                                              C.sub.8 H.sub.17                                                                      C.sub.8 H.sub.17                                                                             K104.6                                                                             C178 A187                                                                               I                                        25455                                                                              C.sub.9 H.sub.19                                                                      C.sub.9 H.sub.19                                                                             K108.8                                                                             C177     I                                        25456                                                                              C.sub.10 H.sub.21                                                                     C.sub.10 H.sub.21                                                                            K112                                                                               S106 C170.5                                                                             I                                        25458                                                                              C.sub.2 H.sub.5                                                                       OCH.sub.3     K162                                                                               A163 N229                                                                               I                                        25460                                                                              C.sub.4 H.sub.9                                                                       OCH.sub.3     K138                                                                               A139 N230                                                                               I                                        25462                                                                              C.sub.6 H.sub.13                                                                      OCH.sub.3     K137                                                                               A138 N206                                                                               U                                        25464                                                                              C.sub.8 H.sub.17                                                                      OCH.sub.3     K135                                                                               A136 N225                                                                               U                                        25466                                                                              C.sub.12 H.sub.25                                                                     OCH.sub.3     K131                                                                               A169 N180                                                                               I                                        25467                                                                              C.sub.16 H.sub.33                                                                     OCH.sub.3     K127                                                                               A175     I                                        25469                                                                              C.sub.5 H.sub.11                                                                      OOCC.sub.3 H.sub.7                                                                           K158                                                                               S200 N219                                                                               I                                        25473                                                                              C.sub.4 H.sub.9 O                                                                     OC.sub.4 H.sub.9                                                                             K170.3                                                                             C218 N246                                                                               I                                        25474                                                                              C.sub.5 H.sub.11 O                                                                    OC.sub.5 H.sub.11                                                                            K153.4                                                                             C211 N224                                                                               I                                        25475                                                                              C.sub.6 H.sub.13 O                                                                    OC.sub.6 H.sub.13                                                                            K135.7                                                                             B139.6 C212 N220                                                                        I                                        25476                                                                              C.sub.7 H.sub.15 O                                                                    OC.sub.7 H.sub.15                                                                            K126                                                                               B128.5 C211 N212                                                                        I                                        25477                                                                              C.sub.8 H.sub.17 O                                                                    OC.sub.8 H.sub.17                                                                            K118.8                                                                             B121.1 C209                                                                             I                                        25478                                                                              C.sub.9 H.sub.19 O                                                                    OC.sub.9 H.sub.19                                                                            K118.7                                                                             C204     I                                        25479                                                                              C.sub.10 H.sub.21 O                                                                   OC.sub.10 H.sub.21                                                                           K113                                                                               C201     I                                        25481                                                                              C.sub.8 H.sub.17 O                                                                    COOCHMeC.sub.2 H.sub.5                                                                     1 K11 C*161 A184                                                                              I                                        25482                                                                              C.sub.10 H.sub.21 O                                                                   COOCHMeC.sub.6 H.sub.13                                                                    1 K138                                                                               C*139 A162                                                                              I                                        __________________________________________________________________________

                                      TABLE 63                                     __________________________________________________________________________      ##STR108##                                                                    No  L      R                Cr LC                                              __________________________________________________________________________     25483                                                                              C.sub.12 H.sub.25                                                                     OCH.sub.2CHMeC.sub.2 H.sub.5                                                                  S K67                                                                               S100 C*155 A157 I                               25484                                                                              C.sub.10 H.sub.21                                                                     COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K85                                                                               C*120 A166 I                                    25485                                                                              C.sub.12 H.sub.25                                                                     COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K95                                                                               C*130 A162 I                                    25486                                                                              C.sub.16 H.sub.33                                                                     COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K95                                                                               C*100 A165 I                                    25487                                                                              C.sub.7 H.sub.15O                                                                     COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K126                                                                              C*175 A200 I                                    25488                                                                              C.sub.8 H.sub.17O                                                                     COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K109                                                                              C*131 A182 I                                    25489                                                                              C.sub.9 H.sub.19O                                                                     COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K113                                                                              C*171 A199 I                                    25490                                                                              C.sub.10 H.sub.21O                                                                    COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K98                                                                               C*168 A187 I                                    25491                                                                              C.sub.11 H.sub.23O                                                                    COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K90                                                                               C*160 A193 I                                    25492                                                                              C.sub.12 H.sub.25O                                                                    COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K110                                                                              C*166 A186 I                                    25493                                                                              C.sub.13 H.sub.27O                                                                    COOCH.sub.2CHMeC.sub.2 H.sub.5                                                                S K100                                                                              C*160 A185 I                                    25494                                                                              C.sub.10 H.sub.21O                                                                    COOC.sub.3 H.sub.6CHMeC.sub.2 H.sub.5                                                         S K68                                                                               C*168 A199 I                                    __________________________________________________________________________      ##STR109##                                                                    No    L    R        Cr   LC                                                    __________________________________________________________________________     26944 F    OC.sub.4 H.sub.9                                                                        K118.7                                                                              A202.3 I                                              26945 F    OC.sub.5 H.sub.11                                                                       K120 A204 I                                                26946 F    OC.sub.6 H.sub.13                                                                       K110.5                                                                              A195.5 I                                              26947 F    OC.sub.7 H.sub.15                                                                       K117.1                                                                              A191.1 I                                              26948 F    OC.sub.8 H.sub.17                                                                       K115.6                                                                              A188 I                                                26949 F    OC.sub.9 H.sub.19                                                                       K116.2                                                                              A179.4 I                                              26950 F    OC.sub.10 H.sub.21                                                                      K117.1                                                                              A178.6 I                                              26951 F    OC.sub.12 H.sub.25                                                                      K121.3                                                                              A170.5 I                                              26952 C.sub.3 H.sub.7                                                                     OC.sub.4 H.sub.9                                                                        K91.7                                                                               E149.2 B161 A198.7 N201.3 I                           26953 C.sub.3 H.sub.7                                                                     OC.sub.5 H.sub.11                                                                       K92.4                                                                               E143 B156 A191.2 N192.5 I                             26954 C.sub.3 H.sub.7                                                                     OC.sub.6 H.sub.13                                                                       K92.6                                                                               E135.9 B149.8 A191.4 N192.1 I                         26955 C.sub.3 H.sub.7                                                                     OC.sub.7 H.sub.15                                                                       K77.3                                                                               E132.7 B147.8 A187.9 I                                26956 C.sub.3 H.sub.7                                                                     OC.sub.8 H.sub.17                                                                       K86.8                                                                               E130.5 B149.9 A198.5 U                                26957 C.sub.3 H.sub.7                                                                     OC.sub.9 H.sub.19                                                                       K91.8                                                                               E120.7 B138.3 N180.5 I                                26958 C.sub.3 H.sub.7                                                                     OC.sub.10 H.sub.21                                                                      K93.2                                                                               E118 B135 N181 I                                      26959 C.sub.3 H.sub.7                                                                     OC.sub.12 H.sub.25                                                                      K105.4                                                                              E108 B128.4 N171.7 I                                  __________________________________________________________________________

                  TABLE 64                                                         ______________________________________                                          ##STR110##                                                                    No    L           R         Cr     LC                                          ______________________________________                                         5543  C.sub.4 H.sub.9                                                                            C.sub.6 H.sub.13                                                                         K57.5  A56.5 I                                     5544  C.sub.6 H.sub.13                                                                           C.sub.4 H.sub.9                                                                          K45    A61.5 I                                     5545  C.sub.6 H.sub.13                                                                           C.sub.5 H.sub.11                                                                         K31    A68 I                                       5546  C.sub.6 H.sub.13                                                                           C.sub.6 H.sub.13                                                                         K44    A68 I                                       5547  C.sub.6 H.sub.13                                                                           C.sub.7 H.sub.15                                                                         K43    A69.5 I                                     5548  C.sub.7 H.sub.15                                                                           C.sub.7 H.sub.15                                                                         K41    A72 I                                       5549  C.sub.8 H.sub.17                                                                           C.sub.4 H.sub.9                                                                          K36.5  A64.5 I                                     5550  C.sub.8 H.sub.17                                                                           C.sub.5 H.sub.11                                                                         K37    B46 A71 I                                   5551  C.sub.8 H.sub.17                                                                           C.sub.6 H.sub.13                                                                         K44    B49 A72 I                                   5552  C.sub.8 H.sub.17                                                                           C.sub.7 H.sub.15                                                                         K50    B51.5 A73.5 I                               5553  C.sub.9 H.sub.19                                                                           C.sub.4 H.sub.9                                                                          K37    A63.5 I                                     5554  C.sub.9 H.sub.19                                                                           C.sub.5 H.sub.11                                                                         K42    A78 I                                       5555  C.sub.9 H.sub.19                                                                           C.sub.6 H.sub.13                                                                         K34    A73 I                                       5556  C.sub.9 H.sub.19                                                                           C.sub.7 H.sub.15                                                                         K44    A73 I                                       5560  C.sub.5 H.sub.11O                                                                          C.sub.4 H.sub.9                                                                          K55    A101 I                                      5561  C.sub.5 H.sub.11O                                                                          C.sub.6 H.sub.13                                                                         K58    A103 I                                      5562  C.sub.6 H.sub.13O                                                                          CH.sub.3  K99    A101 I                                      5563  C.sub.6 H.sub.13O                                                                          C.sub.4 H.sub.9                                                                          K57    A100 I                                      5564  C.sub.6 H.sub.13O                                                                          C.sub.6 H.sub.13                                                                         K55    A103 I                                      ______________________________________                                    

                                      TABLE 65                                     __________________________________________________________________________      ##STR111##                                                                    No  L              R       Cr  LC                                              __________________________________________________________________________     5567                                                                               C.sub.2 H.sub.5CHMeCH.sub.2O                                                                  C.sub.8 H.sub.17                                                                     S K57.8                                                                              A53.9 I                                         5568                                                                               C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                           C.sub.4 H.sub.9                                                                      S K42.5                                                                              C*66.2 A77.3 I                                  5569                                                                               C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                           C.sub.5 H.sub.11                                                                     S K50.5                                                                              C*76.5 A82 I                                    5570                                                                               C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                           C.sub.6 H.sub.13                                                                     S K49 C*75.1 A80.1 I                                  5571                                                                               C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                           C.sub.7 H.sub.15                                                                     S K55 C*77.1 A82 I                                    5572                                                                               C.sub.2 H.sub.5CHMeC.sub.3 H.sub.6O                                                           C.sub.8 H.sub.17                                                                     S K48 C*72.1 A76.9 I                                  5573                                                                               C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                           C.sub.6 H.sub.13                                                                     S K34.5                                                                              C*70.7 A78.1 I                                  5574                                                                               C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8O                                                           C.sub.8 H.sub.17                                                                     S K52.5                                                                              C*70 A73 I                                      5575                                                                               C.sub.2 H.sub.5CHMeC.sub.4 H.sub.8COO                                                         C.sub.8 H.sub.17                                                                     S K68 C*79.6 A80.8 I                                  5576                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.2 H.sub.5                                                                      S K33 A85.4 I                                         5577                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.3 H.sub.7                                                                      S K34.5                                                                              A93.4 I                                         5578                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.4 H.sub.9                                                                      S K29.8                                                                              C*57.1 A85 I                                    5579                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.5 H.sub.11                                                                     S K44 C*76.5 A89.5 I                                  5580                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.6 H.sub.13                                                                     S K37 C*79.3 A85.7 I                                  5581                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.7 H.sub.15                                                                     S K50.5                                                                              C*86.9 A88.8 I                                  5582                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.8 H.sub.19                                                                     S K44.5                                                                              C*81.2 A84.6 I                                  5583                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.9 H.sub.19                                                                     S K59.5                                                                              C*86 I                                          5584                                                                               C.sub.2 H.sub.5CHMeC.sub.5 H.sub.10O                                                          C.sub.10 H.sub.21                                                                    S K51.5                                                                              C*81.2 I                                        __________________________________________________________________________

                                      TABLE 66                                     __________________________________________________________________________      ##STR112##                                                                    No    L         R       Cr    LC                                               __________________________________________________________________________     5654  C.sub.5 H.sub.11O                                                                        C.sub.6 H.sub.13                                                                       K65   C58.5 I                                          5655  C.sub.5 H.sub.11O                                                                        C.sub.7 H.sub.15                                                                       K49   C52.5 N63 I                                      5656  C.sub.6 H.sub.13O                                                                        C.sub.5 H.sub.11                                                                       K55   A68 I                                            5657  C.sub.6 H.sub.13O                                                                        C.sub.7 H.sub.15                                                                       K58   C67 A74 N76 I                                    5658  C.sub.4 H.sub.9O                                                                         OC.sub.4 H.sub.9                                                                       K75.5 S57.5 N74 I                                      5659  C.sub.4 H.sub.9O                                                                         OC.sub.6 H.sub.13                                                                      K70   S68.5 N80 I                                      5660  C.sub.5 H.sub.11O                                                                        OC.sub.4 H.sub.9                                                                       K53.5 S61 N71 I                                        5661  C.sub.5 H.sub.11O                                                                        OC.sub.6 H.sub.13                                                                      K55.5 S70 S72.5 N82 I                                  5676  C.sub.7 H.sub.15COO                                                                      C.sub.6 H.sub.13                                                                       K56   C50.5 A65 I                                      __________________________________________________________________________      ##STR113##                                                                    No  L       R               Cr   LC                                            __________________________________________________________________________     7081                                                                               O.sub.2 N                                                                              OOCC.sub.10 H.sub.20Si.sub.4 O.sub.4 Me.sub.7 -cy                                              K?   A50 I                                         7083                                                                               F       C.sub.2 H.sub.5 K<20 N-36.2 I                                      7084                                                                               F       C.sub.3 H.sub.7 K<20 N-14.6 I                                      7089                                                                               NC      C.sub.6 H.sub.13                                                                               K29.7                                                                               N14.5 I                                       7097                                                                               C.sub.4 H.sub.9                                                                        C.sub.6 H.sub.13                                                                               K20  B44 I                                         7098                                                                               C.sub.4 H.sub.9O                                                                       C.sub.6 H.sub.13                                                                               K40  B78 I                                         7099                                                                               CH.sub.3OOC                                                                            C.sub.5 H.sub.11                                                                               K86.5                                                                               A90.5 I                                       7100                                                                               C.sub.3 H.sub.7OOC                                                                     C.sub.5 H.sub.11                                                                               K37.8                                                                               A68 I                                         7101                                                                               C.sub.4 H.sub.9OOC                                                                     C.sub.5 H.sub.11                                                                               K42  A57.8 I                                       7102                                                                               C.sub.5 H.sub.11OOC                                                                    C.sub.5 H.sub.11                                                                               K45.5                                                                               A59 I                                         __________________________________________________________________________

                  TABLE 67                                                         ______________________________________                                          ##STR114##                                                                    No    L          R          Cr    LC                                           ______________________________________                                         7260  C.sub.5 H.sub.11                                                                          OC.sub.8 H.sub.17                                                                         K72   A114 I                                       7261  C.sub.4 H.sub.9O                                                                          C.sub.4 H.sub.9                                                                           K79   C96 N108 I                                   7262  C.sub.5 H.sub.11O                                                                         C.sub.4 H.sub.9                                                                           K86   C101 N106.5 I                                7264  C.sub.4 H.sub.9O                                                                          OC.sub.4 H.sub.9                                                                          K104  C112 N142 N150 I                             7265  C.sub.4 H.sub.9O                                                                          OC.sub.8 H.sub.17                                                                         K92   C95 A140 N142.5 I                            7266  C.sub.9 H.sub.19O                                                                         OCH.sub.3  K99   A116 N127 I                                  7267  C.sub.9 H.sub.19O                                                                         OC.sub.8 H.sub.17                                                                         K74.5 C135.5 A144 I                                7268  C.sub.4 H.sub.9S                                                                          OC.sub.8 H.sub.17                                                                         K71.8 A119 I                                       ______________________________________                                    

                  TABLE 68                                                         ______________________________________                                          ##STR115##                                                                    No    L          R          Cr    LC                                           ______________________________________                                         7276  C.sub.2 H.sub.5O                                                                          CN         K150  S144 N189 I                                  7277  C.sub.8 H.sub.17                                                                          C.sub.6 H.sub.13                                                                          K68   C106 N116 I                                  7281  C.sub.5 H.sub.11                                                                          OC.sub.4 H.sub.9                                                                          K77   S76 N118 I                                   7285  C.sub.5 H.sub.11O                                                                         C.sub.5 H.sub.11                                                                          K73   C77 N118 I                                   7286  C.sub.5 H.sub.11O                                                                         C.sub.6 H.sub.13                                                                          K73   C88 N114 I                                   7287  C.sub.5 H.sub.11O                                                                         C.sub.7 H.sub.15                                                                          K71   C96 A98 N118 I                               7288  C.sub.5 H.sub.11O                                                                         C.sub.8 H.sub.17                                                                          K73   C92 A105 N112 I                              7289  C.sub.6 H.sub.13O                                                                         C.sub.5 H.sub.11                                                                          K68   C93 N125 I                                   7290  C.sub.6 H.sub.13O                                                                         C.sub.6 H.sub.13                                                                          K66   C98 N117 I                                   7291  C.sub.6 H.sub.13O                                                                         C.sub.7 H.sub.15                                                                          K65   C104 A106 N121 I                             7292  C.sub.6 H.sub.13O                                                                         C.sub.8 H.sub.17                                                                          K69   C104 A113 N117 I                             7293  C.sub.7 H.sub.15O                                                                         C.sub.5 H.sub.11                                                                          K73   C98 N121 I                                   7294  C.sub.7 H.sub.15O                                                                         C.sub.6 H.sub.13                                                                          K70   C105 N116 I                                  7295  C.sub.7 H.sub.15O                                                                         C.sub.7 H.sub.15                                                                          K70   C109 A113 N120 I                             7296  C.sub.7 H.sub.15O                                                                         C.sub.8 H.sub.17                                                                          K71   C109 A115 N116 I                             7297  C.sub.8 H.sub.17O                                                                         C.sub.5 H.sub.11                                                                          K72   C104 N120 I                                  7298  C.sub.8 H.sub.17O                                                                         C.sub.6 H.sub.13                                                                          K68   C106 N116 I                                  7299  C.sub.8 H.sub.17O                                                                         C.sub.7 H.sub.15                                                                          K70   C109 A117 N120 I                             ______________________________________                                          ##STR116##                                                                    No    L          R          Cr    LC                                           ______________________________________                                         7260  C.sub.5 H.sub.11                                                                          OC.sub.8 H.sub.17                                                                         K72   A114 I                                       7261  C.sub.4 H.sub.9O                                                                          C.sub.4 H.sub.9                                                                           K79   C96 N108 I                                   7262  C.sub.5 H.sub.11O                                                                         C.sub.4 H.sub.9                                                                           K86   C101 N106.5 I                                7264  C.sub.4 H.sub.9O                                                                          OC.sub.4 H.sub.9                                                                          K104  C112 A142 N150 I                             7265  C.sub.4 H.sub.9O                                                                          OC.sub.8 H.sub.17                                                                         K92   C95 A140 N142.5 I                            7266  C.sub.9 H.sub.19O                                                                         OCH.sub.3  K99   A116 N127 I                                  7267  C.sub.9 H.sub.19O                                                                         OC.sub.8 H.sub.17                                                                         K74.5 C135.5 A144 I                                7268  C.sub.4 H.sub.9S                                                                          OC.sub.8 H.sub.17                                                                         K71.8 A119 I                                       ______________________________________                                    

                                      TABLE 69                                     __________________________________________________________________________      ##STR117##                                                                    No  L           R       Cr   LC                                                __________________________________________________________________________     7300                                                                               C.sub.8 H.sub.17O                                                                          C.sub.8 H.sub.17                                                                       K69  C113 A118 I                                       7301                                                                               C.sub.9 H.sub.19O                                                                          C.sub.5 H.sub.11                                                                       K76  C107 A109 N118 I                                  7302                                                                               C.sub.9 H.sub.19O                                                                          C.sub.6 H.sub.13                                                                       K76  C111 A113 N116 I                                  7303                                                                               C.sub.9 H.sub.19O                                                                          C.sub.7 H.sub.15                                                                       K76  C113 A119 I                                       7304                                                                               C.sub.9 H.sub.19O                                                                          C.sub.8 H.sub.17                                                                       K75  C114 A117 I                                       7305                                                                               C.sub.10 H.sub.21O                                                                         C.sub.5 H.sub.11                                                                       K77  C107 A113 N118 I                                  7306                                                                               C.sub.10 H.sub.21O                                                                         C.sub.6 H.sub.13                                                                       K75  C110 A114 N116 I                                  7307                                                                               C.sub.10 H.sub.21O                                                                         C.sub.7 H.sub.15                                                                       K74  C114 A119 I                                       7308                                                                               C.sub.10 H.sub.21()                                                                        C.sub.8 H.sub.17                                                                       K68  C114 A116 I                                       7309                                                                               C.sub.11 H.sub.23O                                                                         C.sub.5 H.sub.11                                                                       K83  C105 A114 N116 I                                  7310                                                                               C.sub.11 H.sub.23O                                                                         C.sub.6 H.sub.13                                                                       K82  C110 A115 I                                       7311                                                                               C.sub.11 H.sub.23O                                                                         C.sub.7 H.sub.15                                                                       K81  C113 A118 I                                       7312                                                                               C.sub.11 H.sub.23O                                                                         C.sub.8 H.sub.17                                                                       K80  C115 A117 I                                       7313                                                                               C.sub.12 H.sub.25O                                                                         C.sub.5 H.sub.11                                                                       K83  C104 A114 N116 I                                  7314                                                                               C.sub.12 H.sub.25O                                                                         C.sub.6 H.sub.13                                                                       K103 C108 A113 I                                       7315                                                                               C.sub.12 H.sub.25O                                                                         C.sub.7 H.sub.15                                                                       K79  C112 A118 I                                       7316                                                                               C.sub.12 H.sub.25O                                                                         C.sub.8 H.sub.17                                                                       K79  C113 A115 I                                       7317                                                                               C.sub.5 H.sub.11CFMeCOO                                                                    C.sub.8 H.sub.17                                                                     1 K65.3                                                                               S63.5 I                                           __________________________________________________________________________

                                      TABLE 70                                     __________________________________________________________________________      ##STR118##                                                                    No  L                 R    Cr  LC                                              __________________________________________________________________________     27333                                                                              CH.sub.3          H    K153                                                                               A151.5 N163.5 I                                 27334                                                                              C.sub.2 H.sub.5   H    K142                                                                               A164 I                                          27335                                                                              C.sub.3 H.sub.7   H    K125                                                                               A175.5 I                                        27336                                                                              C.sub.4 H.sub.9   H    K120.5                                                                             A170 I                                          27337                                                                              C.sub.5 H.sub.11  H    K113                                                                               A175 I                                          27338                                                                              C.sub.6 H.sub.13  H    K99.5                                                                              A176 I                                          27339                                                                              C.sub.7 H.sub.15  H    K86 E88 A170 I                                      27340                                                                              C.sub.8 H.sub.17  H    K60 E82 A176 I                                      27341                                                                              C.sub.9 H.sub.19  H    K61 S82 A173 I                                      27342                                                                              C.sub.10 H.sub.21 H    K53 E83 A171 I                                      27343                                                                              CH.sub.3O         H    K169                                                                               A163 N203 I                                     27344                                                                              C.sub.2 H.sub.5O  H    K175                                                                               A202 N216 I                                     27345                                                                              C.sub.3 H.sub.7O  H    K157                                                                               A204 I                                          27346                                                                              C.sub.5 H.sub.11O H    K145                                                                               E130 A206 I                                     27347                                                                              C.sub.8 H.sub.17O H    K96 E115 A195 I                                     27348                                                                              C.sub.10 H.sub.21O                                                                               H    K98 E120 A194 I                                     27349                                                                              C.sub.16 H.sub.33O                                                                               H    K109                                                                               E106 A182.5 I                                   27351                                                                              C.sub.5 H.sub.11 -Oxazolldinyl-N-oxy-C.sub.4 H.sub.8O                                            H  2 K118                                                                               C101 A108 I                                     27352                                                                              C.sub.8 H.sub.17 -Oxazolldinyl-N-oxy-C.sub.7 H.sub.14O                                           H  2 K79 E99 C119 A134 I                                 27353                                                                              CH.sub.3 -Oxazolldinyl-N-oxy-C.sub.8 H.sub.16O                                                   H  2 K113                                                                               C123 A158.5 I                                   __________________________________________________________________________      ##STR119##                                                                    No       L       R       Cr    LC                                              __________________________________________________________________________     8797     C.sub.6 H.sub.13                                                                       C.sub.6 H.sub.13                                                                       K170  S172 A236 I                                     __________________________________________________________________________

                  TABLE 71                                                         ______________________________________                                          ##STR120##                                                                    No      L          R         Cr     LC                                         ______________________________________                                         8797    C.sub.6 H.sub.13                                                                          C.sub.6 H.sub.13                                                                         K170   S172 A236 I                                ______________________________________                                          ##STR121##                                                                    No     L         R         Cr    LC                                            ______________________________________                                         28635  C.sub.5 H.sub.11                                                                         C.sub.6 H.sub.13                                                                         K67   S125 A204 N214 I                              ______________________________________                                          ##STR122##                                                                    No    L          R          Cr    LC                                           ______________________________________                                         7557  C.sub.8 H.sub.17O                                                                         F          K71.5 A128.5 I                                     7558  C.sub.8 H.sub.17O                                                                         Cl         K72   E94.5 A164 I                                 7559  C.sub.8 H.sub.17O                                                                         Br         K75.5 E107.5 A149.5 I                              7561  C.sub.6 H.sub.13                                                                          C.sub.6 H.sub.13                                                                          K54   A45 N56 I                                    7562  C.sub.8 H.sub.17                                                                          C.sub.6 H.sub.13                                                                          K62   A69 I                                        7563  C.sub.8 H.sub.17O                                                                         C.sub.6 H.sub.13                                                                          K55   C106 I                                       7570  C.sub.8 H.sub.17O                                                                         OC.sub.4 H.sub.9                                                                          K70.8 S99.8 N123.1 I                               7572  C.sub.12 H.sub.25O                                                                        OCH.sub.3  K90.7 S96.9 N113.4 I                               ______________________________________                                    

EXAMPLE A1

44.6 g (0.34 mol) of 4-cyanobenzaldehyde and 54.4 g (0.64 mol) of o-aminobenzenethiol were dissolved in 300 ml of dimethyl sulfoxide, and the temperature of the solution was raised to 140° C. The produced water and the dimethyl sulfoxide were distilled off. After heating for one hr, the residue was cooled, water was added thereto, and the resultant precipitate was collected by filtration and washed with ethanol. The crude crystal thus obtained was recrystallized from ethyl acetate to give 2-(4'-cyanophenyl)benzothiazole. 22.4 g (0.095 mol) of the compound was dissolved in 250 ml of acetic acid, and 18.6 g (0.116 mol) of bromine was dropwise added thereto. As soon as bromine was added, a yellow bromine adduct was produced. Subsequently, 150 ml of water was added, and the mixture was stirred at 80° C. for 2 hr. It was then cooled, and the resultant precipitate was collected by filtration and washed with ethanol. The crude product thus obtained was recrystallized from ethyl acetate.

A 60% by weight dispersion of 0.8 g (0.02 mol) of sodium hydride in an oil was suspended in 50 ml of ether, 3.22 g (0.022 mol) of 1-octanethiol was dropwise added thereto, and the mixture was refluxed for 30 min. Thereafter, the ether was distilled off, 50 ml of N,N-dimethylimidazolidinone was added to the residue, and the temperature of the system was raised to 60° C. 0.01 mol of 2-(4'-cyanophenyl)-6-bromobenzothiazole was added to the solution, and stirring was continued for one hr. The solution was cooled, water was added thereto, and the resultant precipitate was collected by filtration and washed with ethanol. The product thus obtained was recrystallized from a hexane/ethyl acetate mixed solution to give a compound represented by the following formula: ##STR123##

EXAMPLE A2

1.31 g (0.01 mol) of 4-cyanobenzaldehyde, 2.5 g (0.01 mol) of 2-amino-6-hexyloxybenzothiazole, and 30 ml of ethanol were heated at 70° C. for 2 hr. The reaction mixture was then cooled to room temperature, and the resultant solid matter was collected by filtration and recrystallized from ethanol to give a compound represented by the following formula: ##STR124##

EXAMPLE A3

2.21 g (0.01 mol) of 2,5-diamino-1,4-benzenedithiol/dihydrochloric acid adduct, 5.34 g (0.024 mol) of 4-hexyloxybenzoic acid, 3 g of phosphorus pentaoxide, and 50 ml of methanesulfonic acid were allowed to react at 90° C. for one hr and then heated at 80° C. for 5 hr. The resultant product was collected by filtration and recrystallized from N-methylpyrrolidone to give a compound represented by the following formula: ##STR125##

EXAMPLE A4

2.56 g (0.01 mol) of 2,6-dimercaptobenzo(1,2-d: 5,6-d')bisthiazole, 4.54 g (0.02 mol) of 4-hexyloxybenzyl chloride, 1.2 g of potassium carbonate, and 15 ml of N-methylpyrrolidone were heated at 80° C. for 3 hr. The reaction mixture was poured into water, and the resultant solid matter was collected by filtration and washed with water, methanol, and chloroform. It was then recrystallized from benzene to give a compound represented by the following formula: ##STR126## wherein R═CH₃ (CH₂)₅ O.

EXAMPLE A5

The procedure of Example A1 was repeated to prepare liquid crystalline compounds represented by the general formula (A) wherein R₁ and R₂ represent the following groups. The liquid crystalline compounds thus obtained had the same properties as the liquid crystalline compound prepared in Example A1.

    ______________________________________                                         Example     R.sub.1          R.sub.2                                           ______________________________________                                         A5-1        CH.sub.3 (CH.sub.2).sub.9 O                                                                     CN                                                A5-2        CH.sub.3 CH.sub.3 C*H(CH.sub.3)CH.sub.2 O                                                       CN                                                A5-3        CH.sub.3 (CH.sub.2).sub.5 O                                                                     O(CH.sub.2).sub.9 CH.sub.3                        A5-4        NO.sub.2         S(CH.sub.2).sub.7 CH.sub.3                        A5-5        NO.sub.2         O(CH.sub.2).sub.7 CH.sub.3                        A5-6        F                O(CH.sub.2).sub.9 CH.sub.3                        ______________________________________                                    

EXAMPLE A6

The procedure of Example A2 was repeated to prepare liquid crystalline compounds represented by the general formula (B) wherein R₁ and R₂ represent the following groups. The liquid crystalline compounds thus obtained had the same properties as the liquid crystalline compound prepared in Example A2.

    ______________________________________                                         Example R.sub.1         R.sub.2    Z                                           ______________________________________                                         A6-1    NO.sub.2        O(CH.sub.2).sub.9 CH.sub.3                                                                CH═N                                    A6-2    CH.sub.3 (CH.sub.2).sub.5 O                                                                    O(CH.sub.2).sub.5 CH.sub.3                                                                COO                                         A6-3    CH.sub.3 CH.sub.2 C*H(CH.sub.3)CH.sub.2 O                                                      O(CH.sub.2).sub.7 CH.sub.3                                                                CH═CH                                   A6-4    CN              O(CH.sub.2).sub.8 CH.sub.3                                                                CH═CH                                   A6-5    CH.sub.3 (CH.sub.2).sub.9 O                                                                    O(CH.sub.2).sub.3 CH.sub.3                                                                C.tbd.C                                     A6-6    CH.sub.3 (CH.sub.2).sub.5 O                                                                    O(CH.sub.2).sub.5 CH.sub.3                                                                N═N                                     ______________________________________                                    

EXAMPLE A7

The procedure of Example A3 was repeated to prepare liquid crystalline compounds represented by the general formula (C) wherein R₁ represents the following groups. The liquid crystalline compounds thus obtained had the same properties as the liquid crystalline compound prepared in Example A3.

    ______________________________________                                         Example          R.sub.1                                                       ______________________________________                                         A7-1             CH.sub.3 (CH.sub.2).sub.9 O                                   A7-2             CH.sub.3 (CH.sub.2).sub.9                                     A7-3             CH.sub.3 (CH.sub.2).sub.9 S                                   A7-4             CH.sub.3 (CH.sub.2).sub.5 S                                   A7-5             CH.sub.3 (CH.sub.2).sub.8 S                                   A7-6             CH.sub.3 CH.sub.2 C*H(CH.sub.3)CH.sub.2 O                     ______________________________________                                    

EXAMPLE A8

The procedure of Example A3 was repeated to prepare liquid crystalline compounds represented by the general formula (D) wherein R₁ represents the following group. The liquid crystalline compounds thus obtained had the same properties as the liquid crystalline compound prepared in Example A4.

    ______________________________________                                         Example     R.sub.1         Z                                                  ______________________________________                                         A8-1        CH.sub.3 (CH.sub.2).sub.5 O                                                                    COO                                                A8-2        CH.sub.3 (CH.sub.2).sub.5 O                                                                    CH═N                                           A8-3        CH.sub.3 CH.sub.2 C*H(CH.sub.3)CH.sub.2 O                                                      CH═CH                                          A8-4        CH.sub.3 (CH.sub.2).sub.5 S                                                                    CH═N                                           A8-5        CH.sub.3 (CH.sub.2).sub.3 O                                                                    N═N                                            A8-6        CH.sub.3 (CH.sub.2).sub.9 O                                                                    COO                                                ______________________________________                                    

According to the present invention, novel liquid crystalline compounds are provided which exhibit liquid crystallinity and, in addition, photoconductivity and fluorescence. The novel liquid crystalline compounds are useful as materials for liquid crystal displays, photosensitive materials for electrophotography and the like.

EXAMPLE B

Synthesis of 2-(4'-heptyloxyphenyl)benzothiazole!74.2 g (0.34 mol) of 4-heptyloxybenzaldehyde and 54.4 g (0.46 mol) of o-aminobenzenethiol were dissolved in 300 ml of dimethyl sulfoxide, and the temperature of the solution was raised to 140° C. The produced water and the dimethyl sulfoxide were distilled off. After heating for one hr, the residue was cooled, water was added thereto, and the resultant precipitate was collected by filtration and washed with ethanol. The crude crystal thus obtained was recrystallized from ethyl acetate. The yield was 90%.

The above compound exhibited the following peaks in NMR spectrum:

¹ H NMR (CDCl₃) δ=0.90 (3H, t, J=6.6 Hz), 1.25-1.47 (8H, m), 1.81 (2H, quint, J=6.6 Hz), 4.01 (2H, t, J=6.5 Hz), 6.97 (2H, d, J=8.5 Hz), 7.33 (1H, d, J=8.9 Hz), 7.45 (1H, t, J=8.5 Hz), 7.86 (1H, d, J=7.9 Hz), 8.01 (1H, d, J=8.9 Hz), 8.02 (2H, d, J=8.5 Hz)

Further, it exhibited the following peaks in IR (KBr disc) spectrum: 506, 568, 622, 648, 698, 730, 968, 1010, 1037, 1300, 1316, 1394, 1417, 1441, 1470, 1483, 1520, 1603, 2852, 2912 cm⁻¹

Synthesis of 2-(4'-heptyloxyphenyl)-6-bromobenzothiazole!

31.0 g (0.095 mol) of 2-(4'-heptyloxyphenyl)benzothiazole was dissolved in 250 ml of acetic acid, and 18.6 g (0.116 mol) of bromine was dropwise added thereto. As soon as bromine was added, a yellow bromine adduct was produced. Subsequently, 150 ml of water was added, and the mixture was stirred at 80° C. for 2 hr. It was then cooled, and the resultant precipitate was collected by filtration and washed with ethanol. The crude product thus obtained was recrystallized from ethyl acetate. The yield was 68%.

The above compound exhibited the following peaks in NMR spectrum:

¹ H NMR (CDCl₃) δ=0.90 (3H, t, J=6.6 Hz), 1.33-1.50 (8H, m), 1.81 (2H, quint, J=6.6 Hz), 4.03 (2H, t, J=6.6 Hz), 6.98 (2H, d, J=8.6 Hz), 7.55 (1H, d, J=2.0 and J2=8.6 Hz), 7.85 (1H, d, J=8.6 Hz), 7.98 (1H, d, J=2.0 Hz), 7.99 (2H, d, J=8.6 Hz)

Further, it exhibited the following peaks in IR (KBr disc) spectrum: 520, 563, 622, 666, 695, 723, 748, 859, 1015, 1040, 1090, 1115, 1224, 1393, 1438, 1474, 1488, 1520, 1541, 2855, 2922, 2937 cm⁻¹

General process for synthesizing 2-(4'-alkoxyphenyl)-6-alkylthiobenzothiazole derivatives!

A 60% by weight dispersion of 0.8 g (0.02 mol) of sodium hydride in an oil was suspended in 50 ml of ether, 0.022 mol of a corresponding alkanethiol was dropwise added thereto, and the mixture was refluxed for 30 min. Thereafter, the ether was distilled off, 50 ml of N,N'-dimethylimidazolidinone was added to the residue, and the temperature of the system was raised to 600° C. 0.01 mol of 2-(4'-heptyloxyphenyl)-6-bromobenzothiazole was added to the solution, and stirring was continued for one hr. The solution was cooled, water was added thereto, and the resultant precipitate was collected by filtration and washed with ethanol. The crude product thus obtained was recrystallized from hexane.

2-(4'-alkoxyphenyl)-6-alkylthiobenzothiazole, having the same R (heptyl group) and different R', had the following properties.

2-(4'-heptyloxyphenyl)-6-hexylthiobenzothiazole! (yield 65%):

¹ H NMR (CDCl₃) δ=0.89 (3H, t, J=6.6 Hz), 0.90 (3H, t, J=6.6 Hz), 1.27-1.47 (14H, m), 1.67 (2H, quint, J=7.2 Hz), 1.82 (2H, quint, J=6.6 Hz), 2.98 (2H, t, J=7.2 Hz), 4.02 (2H, t, J=6.6 Hz), 6.98 (2H, d, J=8.6 Hz), 7.43 (1H, dd, J1 1.7 and J2=Hz), 7.82 (1H, d, J=1.7 Hz), 7.91 (1H, d, J=8.3 Hz), 7.99 (2H, d, J=8.6 Hz)

IR (KBr disc) 520, 570, 621, 701, 727, 966, 1010, 1040, 1112, 1276, 1306, 1396, 1418, 1441, 1474, 1485, 1520, 1543, 1575, 1606, 2855, 2956 cm⁻¹

Heating: Cryst (80.5° C.)--SmA (103.7° C.)--iso (2° C./min)

Cooling: Iso (103.2° C.)--SmA (83.9° C.)--Cryst (5° C./min)

2-(4'-heptyloxyphenyl)-6-octylthiobenzothiazole! (yield 54%):

¹ H NMR (CDCl₃) δ=0.87 (3H, t, J=6.9 Hz), 0.90 (3H, t, J=6.6 Hz), 1.18-1.47 (18H, m), 1.67 (2H, quint, J=7.3 Hz), 1.81 (2H, quint, J=6.6 Hz), 2.97 (2H, t, J=7.3 Hz), 4.02 (2H, t, J=6.6 Hz), 6.98 (2H, d, J=8.9 Hz), 7.42 (1H, dd, J1=1.6 and J2=8.6 Hz), 7.81 (1H, d, J=1.6 Hz), 7.90 (1H, d, J=8.6 Hz), 7.98 (2H, d, J=8.9 Hz)

IR (KBr disc) 520, 570, 621, 702, 727, 774, 843, 967, 1017, 1041, 1112, 1176, 1276, 1306, 1396, 1441, 1474, 1486, 1520, 1543, 1575, 1607, 2855, 2956 cm⁻¹

Heating: Cryst (94.0° C.)--SmA (102.0° C.)--iso (2° C./min)

Cooling: Iso (100.3° C.)--SmA (89.8° C.)--Sm? (78.2° C.)--Cryst (5° C./min)

2-(4'-heptyloxyphenyl)-6-decylthiobenzothiazole! (yield 63%):

¹ H NMR (CDCl₃) δ=0.87 (3H, t, J=6.9 Hz), 0.90 (3H, t, J=6.6 Hz), 1.25-1.47 (22H, m), 1.66 (2H, quint, J=7.3 Hz), 1.81 (2H, quint, J=6.6 Hz), 2.96 (2H, t, J=7.3 Hz), 4.02 (2H, t, J=6.6 Hz), 6.97 (2H, d, J=8.9 Hz), 7.43 (1H, dd, J1=2.0 and J2=8.6 Hz), 7.81 (1H, d, J=2.2 Hz), 7.89 (1H, d, J=8.6 Hz), 7.98 (2H, d, J=8.9 Hz)

IR (KBr disc) 570, 812, 842, 967, 1018, 1041, 1112, 1177, 1306, 1393, 1441, 1474, 1485, 1519,1575, 1607, 2853, 2957 cm⁻¹

Heating: Cryst (95.5° C.)--SmA (100.9° C.)--iso (2° C./min)

Cooling: Iso (100.6° C.)--SmA (93.1° C.)--Cryst (5° C./min)

2-(4'-heptyloxyphenyl)-6-dodecylthiobenzothiazole! (yield 67%):

¹ H NMR (CDCl₃) δ=0.87 (3H, t, J=7.0 Hz), 0.90 (3H, t, J=6.6 Hz), 1.28-1.46 (26H, m), 1.62(2H, quint, J=7.6 Hz), 1.78 (2H, quint, J=7.6 Hz), 2.97 (2H, t, J=7.6 Hz), 4.02 (2H, t, J=6.6 Hz), 6.97 (2H, d, J=8.6 Hz), 7.42 (1H, dd, J1=2.0 and J2=8.6 Hz), 7.81 (1H, d, J=2.0 Hz), 7.90 (1H, d, J=8.6 Hz), 7.98 (2H, d, J=8.6 Hz)

IR (KBr disc) 571, 812, 841, 967, 1018, 1111, 1178, 1306, 1395, 1474, 1486, 1519, 1607, 2852, 2920, 2956 cm⁻¹

Heating: Cryst (90.0° C.)--SmA (98.0° C.)--iso (2° C./min)

Cooling: Iso (96.1° C.)--SmA (85.7° C.)--Cryst (5° C./min)

UV-VIS λmax=327 nm (10⁻⁶ M in CC1₃)

PL (He--Cd Laser 324 nm) λmax=420, 438 nm

EXAMPLE C Synthesis Example 1 of Intermediate

Synthesis of 2-(4'-heptyloxyphenyl)benzothiazole!

74.2 g (0.34 mol) of 4-heptyloxybenzaldehyde and 54.4 g (0.46 mol) of o-aminobenzenethiol were dissolved in 300 ml of dimethyl sulfoxide, and the temperature of the solution was raised to 140° C. The produced water and the dimethyl sulfoxide were distilled off. After heating for one hr, the residue was cooled, water was added thereto, and the resultant precipitate was collected by filtration and washed with ethanol. The crude crystal thus obtained was recrystallized from ethyl acetate. The yield was 90%.

The above compound exhibited the following peaks in NMR spectrum:

¹ H NMR (CDCl₃) δ=0.90 (3H, t, J=6.6 Hz), 1.25-1.47 (8H, m), 1.81 (2H, quint, J=6.6 Hz), 4.01 (2H, t, J=6.5 Hz), 6.97 (2H, d, J=8.5 Hz), 7.33 (1H, d, J=8.9 Hz), 7.45 (1H, t, J=8.5 Hz), 7.86 (1H, d, J=7.9 Hz), 8.01 (1H, d, J=8.9 Hz), 8.02 (2H, d, J=8.5 Hz)

Further, it exhibited the following peaks in IR (KBr disc) spectrum: 506, 568, 622, 648, 698, 730, 968, 1010, 1037, 1300, 1316, 1394, 1417, 1441, 1470, 1483, 1520, 1603, 2852, 2912 cm⁻¹

Synthesis Example 2 of Intermediate

Synthesis of 2-(4'-heptyloxyphenyl)-6-bromobenzothiazole!

31.0 g (0.095 mol) of 2-(4'-heptyloxyphenyl)benzothiazole was dissolved in 250 ml of acetic acid, and 18.6 g (0.116 mol) of bromine was dropwise added thereto. As soon as bromine was added, a yellow bromine adduct was produced. Subsequently, 150 ml of water was added, and the mixture was stirred at 80° C. for 2 hr. It was then cooled, and the resultant precipitate was collected by filtration and washed with ethanol. The crude product thus obtained was recrystallized from ethyl acetate. The yield was 68%.

The above compound exhibited the following peaks in NMR spectrum:

¹ H NMR (CDCl₃) δ=0.90 (3H, t, J=6.6 Hz), 1.33-1.50 (8H, m), 1.81 (2H, quint, J=6.6 Hz), 4.03 (2H, t, J=6.6 Hz), 6.98 (2H, d, J=8.6 Hz), 7.55 (1H, dd, J1=2.0 and J2=8.6 Hz), 7.85 (1H, d, J=8.6 Hz), 7.98 (1H, d, J=2.0 Hz), 7.99 (2H, d, J=8.6 Hz)

Further, it exhibited the following peaks in IR (KBr disc) spectrum: 520, 563, 622, 666, 695, 723, 748, 859, 1015, 1040, 1090, 1115, 1224, 1393, 1438, 1474, 1488, 1520, 1541, 2855, 2922, 2937 cm⁻¹

EXAMPLES C1 to C4 General process for synthesizing 2-(4'-alkoxyphenyl)-6-alkylthiobenzothiazole derivatives!

A 60% by weight dispersion of 0.8 g (0.02 mol) of sodium hydride in an oil was suspended in 50 ml of ether, 0.022 mol of a corresponding alkanethiol was dropwise added thereto, and the mixture was refluxed for 30 min. Thereafter, the ether was distilled off, 50 ml of N,N'-dimethylimidazolidinone was added to the residue, and the temperature of the system was raised to 60° C. 0.01 mol of 2-(4'-heptyloxyphenyl)-6-bromobenzothiazole was added to the solution, and stirring was continued for one hr. The solution was cooled, water was added thereto, and the resultant precipitate was collected by filtration and washed with ethanol. The crude product thus obtained was recrystallized from hexane.

2-(4'-alkoxyphenyl)-6-alkylthiobenzothiazole, having the same R (heptyl group) and different R', had the following properties.

EXAMPLE C1

2-(4'-heptyloxyphenyl)-6-hexylthiobenzothiazole! (yield 65%):

¹ H NMR (CDCl₃) δ=0.89 (3H, t, J=6.6 Hz), 0.90 (3H, t, J=6.6 Hz), 1.27-1.47 (14H, m), 1.67 (2H, quint, J=7.2 Hz), 1.82 (2H, quint, J=6.6 Hz), 2.98 (2H, t, J=7.2 Hz), 4.02 (2H, t, J=6.6 Hz), 6.98 (2H, d, J=8.6 Hz), 7.43 (1H, dd, J1=1.7 and J2=8.3 Hz), 7.82 (1H, d, J=1.7 Hz), 7.91 (1H, d, J=8.3 Hz), 7.99 (2H, d, J=8.6 Hz)

IR (KBr disc) 520, 570, 621, 701, 727, 966, 1010, 1040, 1112, 1276, 1306, 1396, 1418, 1441, 1474, 1485, 1520, 1543, 1575, 1606, 2855, 2956 cm⁻¹

Heating: Cryst (80.5° C.)--SmA (103.7° C.)--iso (2° C./min)

Cooling: Iso (103.2° C.)--SmA (83.9° C.)--Cryst (5° C./min)

Example C2

2-(4'-heptyloxyphenyl)-6-octylthiobenzothiazole! (yield 54%):

¹ H NMR (CDCl₃) δ=0.87 (3H, t, J=6.9 Hz), 0.90 (3H, t, J=6.6 Hz), 1.18-1.47 (18H, m), 1.67 (2H, quint, J=7.3 Hz), 1.81 (2H, quint, J=6.6 Hz), 2.97 (2H, t, J=7.3 Hz), 4.02 (2H, t, J=6.6 Hz), 6.98 (2H, d, J=8.9 Hz), 7.42 (1H, dd, J1=1.6 and J2=8.6 Hz), 7.81 (1H, d, J=1.6 Hz), 7.90 (1H, d, J=8.6 Hz), 7.98 (2H, d, J=8.9 Hz)

IR (KBr disc) 520, 570, 621, 702, 727, 774, 843, 967, 1017, 1041, 1112, 1176, 1276, 1306, 1396, 1441, 1474, 1486, 1520, 1543, 1575, 1607, 2855, 2956 cm⁻¹

Heating: Cryst (94.0° C.)--SmA (102.0° C.)--iso (2° C./min)

Cooling: Iso (100.3° C.)--SmA (89.8° C.)--Sm? (78.2° C.) -Cryst (5° C./min)

EXAMPLE C3

2-(4'-heptyloxyphenyl)-6-decylthiobenzothiazole! (yield 63%):

¹ H NMR (CDCl₃) δ=0.87 (3H, t, J=6.9 Hz), 0.90 (3H, t, J=6.6 Hz), 1.25-1.47 (22H, m), 1.66 (2H, quint, J=7.3 Hz), 1.81 (2H, quint, J=6.6 Hz), 2.96 (2H, t, J=7.3 Hz), 4.02 (2H, t, J=6.6 Hz), 6.97 (2H, d, J=8.9 Hz), 7.43 (1H, dd, J1=2.0 and J2=8.6 Hz), 7.81 (1H, d, J=2.2 Hz), 7.89 (1H, d, J=8.6 Hz), 7.98 (2H, d, J=8.9 Hz)

IR (KBr disc) 570, 812, 842, 967, 1018, 1041, 1112, 1177, 1306, 1393, 1441, 1474, 1485, 1519,1575, 1607, 2853, 2957 cm⁻¹

Heating: Cryst (95.5° C.)--SmA (100.90° C.)--iso (2° C./min)

Cooling: Iso (100.6° C.)--SmA (93.1° C.)--Cryst (5° C./min)

EXAMPLE C4

2-(4'-heptyloxyphenyl)-6-dodecylthiobenzothiazole! (yield 67%):

¹ H NMR (CDCl₃) δ=0.87 (3H, t, J=7.0 Hz), 0.90 (3H, t, J=6.6 Hz), 1.28-1.46 (26H, m), 1.62(2H, quint, J=7.6 Hz), 1.78 (2H, quint, J=7.6 Hz), 2.97 (2H, t, J=7.6 Hz), 4.02 (2H, t, J=6.6 Hz), 6.97 (2H, d, J=8.6 Hz), 7.42 (1H, dd, J1=2.0 and J2=8.6 Hz), 7.81 (1H, d, J=2.0 Hz), 7.90 (1H, d, J=8.6 Hz), 7.98 (2H, d, J=8.6 Hz)

IR (KBr disc) 571, 812, 841, 967, 1018, 1111, 1178, 1306, 1395, 1474, 1486, 1519, 1607, 2852, 2920, 2956 cm⁻¹

Heating: Cryst (90.0° C.)--SmA (98.0° C.)--iso (2° C./min)

Cooling: Iso (96.1° C.)--SmA (85.7° C.)--Cryst (5° C./min)

UV-VIS λmax=327 nm (10⁻⁶ M in CC1₃)

PL (He--Cd Laser 324 nm) λmax=420, 438 nm

EXAMPLES C5 to C10

Liquid crystalline compounds represented by the above general formula wherein R and R' represent the following groups were prepared in the same manner as in the above examples and comparative examples. All the liquid crystalline compounds thus obtained had the same properties as those prepared in Examples C1 to C4.

    ______________________________________                                         Example       R            R'                                                  ______________________________________                                         Example C5    Hexyl group  Heptyl group                                        Example C6    Octyl group  Nonyl group                                         Example C7    Hexyl group  Undecynyl group                                     Example C8    Decyl group  Tetradecyl group                                    Example C9    Amyl group   Tridecyl group                                      Example C10   Dodecyl group                                                                               Heptyl group                                        ______________________________________                                    

According to the present invention, novel liquid crystalline compounds which exhibit liquid crystallinity and, in addition, photoconductivity and fluorescence. The novel liquid crystalline compounds are useful as materials for liquid crystal displays, photosensitive materials for electrophotography and the like. 

We claim:
 1. A process for producing a liquid crystalline compound represented by the general formula (C), comprising the step of: reacting 2 moles of a compound represented by the general formula (6) with one mole of a compound represented by the general formula (7) to obtain the liquid crystalline compound (C): ##STR127## wherein R₁ is a C₁ -C₂₂ straight-chain or branched saturated or unsaturated alkyl or alkoxy group attached to the aromatic ring through an oxygen or sulfur.
 2. A process for producing a liquid crystalline compound represented by the general formula (D), comprising the step of: reacting two moles of a compound represented by the general formula (8) with one mole of a compound represented by the general formula (9) to obtain the liquid crystalline compound (D): ##STR128## wherein R₁ is a C₁ -C₂₂ straight-chain or branched saturated or unsaturated alkyl or alkoxy group attached to the aromatic ring through an oxygen or sulfur group; and X and Y are respectively groups which are reacted with each other to form Z selected from a --COO--, --OCO--, --N═N--, --CH═N--, --CH₂ S--, --CH═CH--, or --C.tbd.C--group.
 3. A process for producing a liquid crystalline compound represented by the following general formula (I), comprising the steps of: reacting a 4-alkoxybenzaldehyde with o-aminobenzenethiol to synthesize a 2-(4'-alkoxyphenyl)benzothiazole; brominating the 2-(4'-alkoxyphenyl)benzothiazole to synthesize a 2-(4'-alkoxyphenyl)-6-bromobenzothiazole; and reacting the resultant bromide with an alkanethiol to obtain the liquid crystalline compound (I): ##STR129## wherein R represents a C₄ -C₂₀ alkyl group; and R' represents a C₄ -C₂₀ alkyl group, provided that the total number of carbon atoms contained in R and R' is 10 or more.
 4. A liquid crystalline compound represented by the following general formula (II): ##STR130## wherein R represents C₇ H₁₅ and R' represents C₆ H₁₃, C₈ H₁₇, C₁₀ H₂₁ or C₁₂ H₂₅. 